Novel graphite-like carbon nitride/organic aluminum diethylhypophosphites nanohybrid: Preparation and enhancement on thermal stability and flame retardancy of polystyrene
Graphite-like carbon nitride (g-C3N4) was innovatively modified by diethylphosphinic acid through hydrogen bonding; g-C3N4/organic aluminum diethylhypophosphites (g-C3N4/DAHPi) hybrid (denoted as CDAHPi) was synthesized by salification reactions, and subsequently incorporated into PS matrix to prepa...
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| Published in | Composites. Part A, Applied science and manufacturing Vol. 99; pp. 149 - 156 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
01.08.2017
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| Subjects | |
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| Abstract | Graphite-like carbon nitride (g-C3N4) was innovatively modified by diethylphosphinic acid through hydrogen bonding; g-C3N4/organic aluminum diethylhypophosphites (g-C3N4/DAHPi) hybrid (denoted as CDAHPi) was synthesized by salification reactions, and subsequently incorporated into PS matrix to prepare composites through melt blending method. Thermal data showed that g-C3N4 could protect DAHPi from external heat, leading to improved thermal stability of DAHPi. Moreover, it was found that the introduction of the hybrid reduced the values of heat release rate (HRR) and total heat release (THR) of the composites. Compared with those of pure PS, the HRR and THR of PS/CDAPHi4 decreasing by 43% and 21% respectively were observed at loadings as low as 4.0wt%. The PS/CDAHPi exhibited an additional advantage in suppression of pyrolysis gas production in comparison with neat PS. In addition, the additive showed higher interfacial adhesion with PS. |
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| AbstractList | Graphite-like carbon nitride (g-C3N4) was innovatively modified by diethylphosphinic acid through hydrogen bonding; g-C3N4/organic aluminum diethylhypophosphites (g-C3N4/DAHPi) hybrid (denoted as CDAHPi) was synthesized by salification reactions, and subsequently incorporated into PS matrix to prepare composites through melt blending method. Thermal data showed that g-C3N4 could protect DAHPi from external heat, leading to improved thermal stability of DAHPi. Moreover, it was found that the introduction of the hybrid reduced the values of heat release rate (HRR) and total heat release (THR) of the composites. Compared with those of pure PS, the HRR and THR of PS/CDAPHi4 decreasing by 43% and 21% respectively were observed at loadings as low as 4.0wt%. The PS/CDAHPi exhibited an additional advantage in suppression of pyrolysis gas production in comparison with neat PS. In addition, the additive showed higher interfacial adhesion with PS. |
| Author | Huang, Zheng-Qi Tai, Qilong Hu, Yuan Zhu, Yulu Duan, Lijin Shi, Yongqian |
| Author_xml | – sequence: 1 givenname: Yulu surname: Zhu fullname: Zhu, Yulu organization: State Key Laboratory of Fire Science, University of Science and Technology of China, 96 Jinzhai Road, Hefei, Anhui 230026, PR China – sequence: 2 givenname: Yongqian surname: Shi fullname: Shi, Yongqian organization: State Key Laboratory of Fire Science, University of Science and Technology of China, 96 Jinzhai Road, Hefei, Anhui 230026, PR China – sequence: 3 givenname: Zheng-Qi surname: Huang fullname: Huang, Zheng-Qi organization: State Key Laboratory of Fire Science, University of Science and Technology of China, 96 Jinzhai Road, Hefei, Anhui 230026, PR China – sequence: 4 givenname: Lijin surname: Duan fullname: Duan, Lijin organization: State Key Laboratory of Fire Science, University of Science and Technology of China, 96 Jinzhai Road, Hefei, Anhui 230026, PR China – sequence: 5 givenname: Qilong surname: Tai fullname: Tai, Qilong email: qltai@ustc.edu.cn organization: State Key Laboratory of Fire Science, University of Science and Technology of China, 96 Jinzhai Road, Hefei, Anhui 230026, PR China – sequence: 6 givenname: Yuan surname: Hu fullname: Hu, Yuan email: yuanhu@ustc.edu.cn organization: State Key Laboratory of Fire Science, University of Science and Technology of China, 96 Jinzhai Road, Hefei, Anhui 230026, PR China |
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| SubjectTerms | adhesion aluminum carbon nitride composite materials Flame retardancy g-C3N4/organic aluminum diethylhypophosphites hybrid heat Hydrogen bond hydrogen bonding Mechanism melting mixing nanohybrids polystyrenes pyrolysis Thermal stability |
| Title | Novel graphite-like carbon nitride/organic aluminum diethylhypophosphites nanohybrid: Preparation and enhancement on thermal stability and flame retardancy of polystyrene |
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