Elimination of trichloroanisoles by UV/H2O2: Kinetics, degradation mechanism, water matrix effects and toxicity assessment
The elimination of 2,3,6-trichloroanisole (2,3,6-TCA), which produces a musty-earthy off-odor in water, by an ultraviolet (UV)/H2O2 process was assessed. The removal of 88.1% of 2,3,6-TCA in ultrapure water (UPW) was achieved using an initial 2,3,6-TCA concentration of 1 μg L−1 (4.73 nM), a H2O2 con...
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Published in | Chemosphere (Oxford) Vol. 230; pp. 258 - 267 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier Ltd
01.09.2019
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Abstract | The elimination of 2,3,6-trichloroanisole (2,3,6-TCA), which produces a musty-earthy off-odor in water, by an ultraviolet (UV)/H2O2 process was assessed. The removal of 88.1% of 2,3,6-TCA in ultrapure water (UPW) was achieved using an initial 2,3,6-TCA concentration of 1 μg L−1 (4.73 nM), a H2O2 concentration of 20 mg L−1 (0.588 mM), a UV intensity of 1.44 mW cm−2 and a pH of 8.2. The reaction was found to be pseudo first order with a rate constant (kobs) of 0.0340 min−1. Both the removal efficiency and kobs increased significantly upon increasing the H2O2 concentration from 10 to 50 mg L−1. The second order rate constant (kHO·,2,3,6-TCA) in competition kinetic trials was determined to be 8.17 × 107 M−1s−1. Degradation products generated during both the UV photolysis and UV/H2O2 treatment of 2,3,6-TCA solutions were analyzed using ultrahigh resolution gas chromatography/mass spectrometry, and the degradation mechanism was proposed. The toxicities of water solutions during both processes were assessed via a luminescence method in conjunction with Vibrio fischeri. The pH and Cl−, HCO3− and natural organic matter concentrations of the aqueous medium were all found to significantly affect the removal of 2,3,6-TCA. The degradation rates of trichloroanisoles (TCAs) in real-world water samples demonstrated that UV/H2O2 has significant potential with regard to controlling TCAs as pollutants in water.
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•2,3,6-trichloroanisole as trichloroanisole T&O compound was firstly studied.•UV/H2O2 was of great validity to control trichloroanisole pollution.•Ultrahigh resolution GC/MS facilitated degradation mechanism investigation.•Toxic degradation products generated during both UV photolysis and indirect oxidation. |
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AbstractList | The elimination of 2,3,6-trichloroanisole (2,3,6-TCA), which produces a musty-earthy off-odor in water, by an ultraviolet (UV)/H2O2 process was assessed. The removal of 88.1% of 2,3,6-TCA in ultrapure water (UPW) was achieved using an initial 2,3,6-TCA concentration of 1 μg L−1 (4.73 nM), a H2O2 concentration of 20 mg L−1 (0.588 mM), a UV intensity of 1.44 mW cm−2 and a pH of 8.2. The reaction was found to be pseudo first order with a rate constant (kobs) of 0.0340 min−1. Both the removal efficiency and kobs increased significantly upon increasing the H2O2 concentration from 10 to 50 mg L−1. The second order rate constant (kHO·,2,3,6-TCA) in competition kinetic trials was determined to be 8.17 × 107 M−1s−1. Degradation products generated during both the UV photolysis and UV/H2O2 treatment of 2,3,6-TCA solutions were analyzed using ultrahigh resolution gas chromatography/mass spectrometry, and the degradation mechanism was proposed. The toxicities of water solutions during both processes were assessed via a luminescence method in conjunction with Vibrio fischeri. The pH and Cl−, HCO3− and natural organic matter concentrations of the aqueous medium were all found to significantly affect the removal of 2,3,6-TCA. The degradation rates of trichloroanisoles (TCAs) in real-world water samples demonstrated that UV/H2O2 has significant potential with regard to controlling TCAs as pollutants in water.
[Display omitted]
•2,3,6-trichloroanisole as trichloroanisole T&O compound was firstly studied.•UV/H2O2 was of great validity to control trichloroanisole pollution.•Ultrahigh resolution GC/MS facilitated degradation mechanism investigation.•Toxic degradation products generated during both UV photolysis and indirect oxidation. |
Author | Jia, Ruibao Feng, Guixue Wang, Mingquan Xin, Xiaodong Zhao, Qinghua Sun, Shaohua Zhou, Anran Zhu, Huanhuan |
Author_xml | – sequence: 1 givenname: Huanhuan surname: Zhu fullname: Zhu, Huanhuan organization: School of Water Conservancy and Environment, University of Jinan, Jinan, 250022, PR China – sequence: 2 givenname: Ruibao orcidid: 0000-0003-4583-9179 surname: Jia fullname: Jia, Ruibao email: jiaruibao1968@163.com organization: Shandong Province Water Supply and Drainage Monitoring Center, Jinan, 250101, PR China – sequence: 3 givenname: Shaohua surname: Sun fullname: Sun, Shaohua organization: Shandong Province Water Supply and Drainage Monitoring Center, Jinan, 250101, PR China – sequence: 4 givenname: Guixue surname: Feng fullname: Feng, Guixue organization: Shandong Province Water Supply and Drainage Monitoring Center, Jinan, 250101, PR China – sequence: 5 givenname: Mingquan surname: Wang fullname: Wang, Mingquan organization: Shandong Province Water Supply and Drainage Monitoring Center, Jinan, 250101, PR China – sequence: 6 givenname: Qinghua surname: Zhao fullname: Zhao, Qinghua organization: Shandong Province Water Supply and Drainage Monitoring Center, Jinan, 250101, PR China – sequence: 7 givenname: Xiaodong surname: Xin fullname: Xin, Xiaodong organization: Shandong Province Water Supply and Drainage Monitoring Center, Jinan, 250101, PR China – sequence: 8 givenname: Anran surname: Zhou fullname: Zhou, Anran organization: School of Municipal & Environmental Engineering, Shandong Jianzhu University, Jinan, 250101, PR China |
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Keywords | Water matrix effects Trichloroanisoles Degradation mechanism Kinetics Toxicity assessment Advanced oxidation process |
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Snippet | The elimination of 2,3,6-trichloroanisole (2,3,6-TCA), which produces a musty-earthy off-odor in water, by an ultraviolet (UV)/H2O2 process was assessed. The... |
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SubjectTerms | Advanced oxidation process Degradation mechanism Kinetics Toxicity assessment Trichloroanisoles Water matrix effects |
Title | Elimination of trichloroanisoles by UV/H2O2: Kinetics, degradation mechanism, water matrix effects and toxicity assessment |
URI | https://dx.doi.org/10.1016/j.chemosphere.2019.05.052 |
Volume | 230 |
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