Metal‐Free C3 Hydroxylation of Quinoxalin‐2(1H)‐ones in Water

A practical protocol for the preparation of quinoxaline‐2,3(1H,4H)‐diones through direct C(sp2)−H hydroxylation of quinoxalin‐2(1H)‐ones in recyclable DL‐α‐Tocopherol methoxypolyethylene glycol succinate solution (2 wt% in water) (TPGS‐750‐M/H2O) was developed. The target products were exclusively g...

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Published inAdvanced synthesis & catalysis Vol. 361; no. 24; pp. 5721 - 5726
Main Authors Peng, Sha, Hu, Die, Hu, Jia‐Li, Lin, Ying‐Wu, Tang, Shan‐Shan, Tang, Hai‐Shan, He, Jun‐Yi, Cao, Zhong, He, Wei‐Min
Format Journal Article
LanguageEnglish
Published WEINHEIM Wiley 17.12.2019
Wiley Subscription Services, Inc
Subjects
Chemistry
Chemistry, Applied
Chemistry, Organic
green chemistry
Hydroxylation
in water
Physical Sciences
quinoxalin-2(1H)-one
Quinoxalines
Recrystallization
Science & Technology
Tocopherol
TPGS-750-M
in water
DESIGN
DIRECT ARYLATION
hydroxylation
VISIBLE-LIGHT PHOTOREDOX
quinoxalin-2(1H)-one
green chemistry
SALTS
H HYDROXYLATION
ALCOHOLS
MILD
TPGS-750-M
QUINOXALIN-2(H)-ONES
FACILE
EFFICIENT
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Abstract A practical protocol for the preparation of quinoxaline‐2,3(1H,4H)‐diones through direct C(sp2)−H hydroxylation of quinoxalin‐2(1H)‐ones in recyclable DL‐α‐Tocopherol methoxypolyethylene glycol succinate solution (2 wt% in water) (TPGS‐750‐M/H2O) was developed. The target products were exclusively generated and could be collected through extraction and recrystallization.
AbstractList A practical protocol for the preparation of quinoxaline‐2,3(1H,4H)‐diones through direct C(sp2)−H hydroxylation of quinoxalin‐2(1H)‐ones in recyclable DL‐α‐Tocopherol methoxypolyethylene glycol succinate solution (2 wt% in water) (TPGS‐750‐M/H2O) was developed. The target products were exclusively generated and could be collected through extraction and recrystallization.
A practical protocol for the preparation of quinoxaline-2,3(1H,4H)-diones through direct C(sp(2))-H hydroxylation of quinoxalin-2(1H)-ones in recyclable DL-alpha-Tocopherol methoxypolyethylene glycol succinate solution (2 wt% in water) (TPGS-750-M/H2O) was developed. The target products were exclusively generated and could be collected through extraction and recrystallization.
A practical protocol for the preparation of quinoxaline‐2,3(1 H ,4 H )‐diones through direct C( sp 2 )−H hydroxylation of quinoxalin‐2(1 H )‐ones in recyclable DL‐α‐Tocopherol methoxypolyethylene glycol succinate solution (2 wt% in water) (TPGS‐750‐M/H 2 O) was developed. The target products were exclusively generated and could be collected through extraction and recrystallization. magnified image
Author Hu, Jia‐Li
Tang, Hai‐Shan
He, Wei‐Min
Tang, Shan‐Shan
He, Jun‐Yi
Hu, Die
Lin, Ying‐Wu
Cao, Zhong
Peng, Sha
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  surname: Peng
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  organization: Hunan University of Science and Engineering
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  givenname: Die
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  fullname: Hu, Die
  organization: Hunan University of Science and Engineering
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  givenname: Jia‐Li
  surname: Hu
  fullname: Hu, Jia‐Li
  organization: Hunan University of Science and Engineering
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  organization: University of South China
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  surname: Tang
  fullname: Tang, Shan‐Shan
  organization: Hunan University of Science and Engineering
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  surname: Tang
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  organization: Hunan University of Science and Engineering
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  surname: He
  fullname: He, Jun‐Yi
  organization: Changsha University of Science and Technology
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  givenname: Zhong
  surname: Cao
  fullname: Cao, Zhong
  organization: Changsha University of Science and Technology
– sequence: 9
  givenname: Wei‐Min
  surname: He
  fullname: He, Wei‐Min
  email: weiminhe2016@yeah.net
  organization: Changsha University of Science and Technology
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Keywords in water
DESIGN
DIRECT ARYLATION
hydroxylation
VISIBLE-LIGHT PHOTOREDOX
quinoxalin-2(1H)-one
green chemistry
SALTS
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ALCOHOLS
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FACILE
EFFICIENT
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Snippet A practical protocol for the preparation of quinoxaline‐2,3(1H,4H)‐diones through direct C(sp2)−H hydroxylation of quinoxalin‐2(1H)‐ones in recyclable...
A practical protocol for the preparation of quinoxaline‐2,3(1 H ,4 H )‐diones through direct C( sp 2 )−H hydroxylation of quinoxalin‐2(1 H )‐ones in recyclable...
A practical protocol for the preparation of quinoxaline-2,3(1H,4H)-diones through direct C(sp(2))-H hydroxylation of quinoxalin-2(1H)-ones in recyclable...
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SubjectTerms Chemistry
Chemistry, Applied
Chemistry, Organic
green chemistry
Hydroxylation
in water
Physical Sciences
quinoxalin-2(1H)-one
Quinoxalines
Recrystallization
Science & Technology
Tocopherol
TPGS-750-M
Title Metal‐Free C3 Hydroxylation of Quinoxalin‐2(1H)‐ones in Water
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fadsc.201901163
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