A General and Practical Approach for the Synthesis of 1,2,4‐Trioxanes Catalyzed by Silica‐Ferric Chloride
An efficient and practical method has been developed for the facile synthesis of 1,2,4‐trioxanes by the condensation of β‐hydroperoxy alcohols and carbonyl compounds in the presence of a catalytic amount of silica‐supported ferric chloride (FeCl3/SiO2) at room temperature. The method has the benefit...
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| Published in | Advanced synthesis & catalysis Vol. 359; no. 20; pp. 3618 - 3625 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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WEINHEIM
Wiley
25.10.2017
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| Abstract | An efficient and practical method has been developed for the facile synthesis of 1,2,4‐trioxanes by the condensation of β‐hydroperoxy alcohols and carbonyl compounds in the presence of a catalytic amount of silica‐supported ferric chloride (FeCl3/SiO2) at room temperature. The method has the benefits of operational simplicity, high yields and potential large‐scale application. Moreover, the catalyst can be readily recovered by simple filtration and reused up to five times while almost maintaining its catalytic activity. |
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| AbstractList | An efficient and practical method has been developed for the facile synthesis of 1,2,4‐trioxanes by the condensation of β‐hydroperoxy alcohols and carbonyl compounds in the presence of a catalytic amount of silica‐supported ferric chloride (FeCl3/SiO2) at room temperature. The method has the benefits of operational simplicity, high yields and potential large‐scale application. Moreover, the catalyst can be readily recovered by simple filtration and reused up to five times while almost maintaining its catalytic activity. An efficient and practical method has been developed for the facile synthesis of 1,2,4-trioxanes by the condensation of beta-hydroperoxy alcohols and carbonyl compounds in the presence of a catalytic amount of silica-supported ferric chloride (FeCl3/SiO2) at room temperature. The method has the benefits of operational simplicity, high yields and potential large-scale application. Moreover, the catalyst can be readily recovered by simple filtration and reused up to five times while almost maintaining its catalytic activity. An efficient and practical method has been developed for the facile synthesis of 1,2,4‐trioxanes by the condensation of β‐hydroperoxy alcohols and carbonyl compounds in the presence of a catalytic amount of silica‐supported ferric chloride (FeCl 3 /SiO 2 ) at room temperature. The method has the benefits of operational simplicity, high yields and potential large‐scale application. Moreover, the catalyst can be readily recovered by simple filtration and reused up to five times while almost maintaining its catalytic activity. magnified image |
| Author | Han, Yi Zhang, Mo Niu, Jia‐Liang Zhang, Zhan‐Hui |
| Author_xml | – sequence: 1 givenname: Mo surname: Zhang fullname: Zhang, Mo organization: Hebei Normal University – sequence: 2 givenname: Yi surname: Han fullname: Han, Yi organization: Hebei Normal University – sequence: 3 givenname: Jia‐Liang surname: Niu fullname: Niu, Jia‐Liang organization: Hebei Normal University – sequence: 4 givenname: Zhan‐Hui surname: Zhang fullname: Zhang, Zhan‐Hui email: zhanhui@mail.nankai.edu.cn organization: Hebei Normal University |
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| Keywords | CONVENIENT SYNTHESIS 1,2,4-trioxanes ONE-POT SYNTHESIS MAGNETICALLY SEPARABLE CATALYST PROMOTED ONE-POT carbonyl compounds beta-hydroperoxy alcohols silica-supported iron(III) chloride SUPPORTED MOLYBDENUM SPIRO 1,2,4-TRIOXANES DIASTEREOSELECTIVE FORMATION 4-COMPONENT SYNTHESIS RECYCLABLE CATALYST ANTIMALARIAL 1,2,4-TRIOXANES |
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| Snippet | An efficient and practical method has been developed for the facile synthesis of 1,2,4‐trioxanes by the condensation of β‐hydroperoxy alcohols and carbonyl... An efficient and practical method has been developed for the facile synthesis of 1,2,4-trioxanes by the condensation of beta-hydroperoxy alcohols and carbonyl... An efficient and practical method has been developed for the facile synthesis of 1,2,4-trioxanes by the condensation of [beta]-hydroperoxy alcohols and... |
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| SubjectTerms | 1,2,4-trioxanes Alcohols Carbonyl compounds Carbonyls Catalysis Catalytic activity Chemical synthesis Chemistry Chemistry, Applied Chemistry, Organic Ferric chloride Oxidation Physical Sciences Science & Technology silica-supported iron(III) chloride Silicon dioxide β-hydroperoxy alcohols |
| Title | A General and Practical Approach for the Synthesis of 1,2,4‐Trioxanes Catalyzed by Silica‐Ferric Chloride |
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