Methanol Steam Reforming over ZrO2-Supported Catalysts in Conventional and Membrane Reactors
Results of a study of the methanol steam reforming (MSR) catalytic process in conventional flow and membrane reactors in the presence of Ni 0.2 –Cu 0.8 and Ru 0.5 –Rh 0.5 catalysts supported on ZrO 2 with a monoclinic, tetragonal, and cubic structure have been described. The cubic structure of zirco...
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Published in | Petroleum chemistry Vol. 57; no. 13; pp. 1219 - 1227 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
Published |
Moscow
Pleiades Publishing
01.12.2017
Springer Nature B.V |
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Abstract | Results of a study of the methanol steam reforming (MSR) catalytic process in conventional flow and membrane reactors in the presence of Ni
0.2
–Cu
0.8
and Ru
0.5
–Rh
0.5
catalysts supported on ZrO
2
with a monoclinic, tetragonal, and cubic structure have been described. The cubic structure of zirconia has been stabilized with ceria. The samples have been characterized by X-ray diffraction analysis, transmission electron microscopy, and the BET method. It has been shown that the catalytic activity of the composites depends on the type of the metals and the structure of the support. It has been found that the Ru–Rh/Ce
0.1
Zr
0.9
O
2–δ
catalyst exhibits the highest activity, whereas Cu–Ni/Ce
0.1
Zr
0.9
O
2–δ
is the most selective. A comparative study of the MSR process in conventional and membrane reactors with Pd–Ru and modified Pd–Ag membranes has been conducted. The membrane process with a membrane based on a Pd–Ag alloy in the presence of the Ru–Rh/Ce
0.1
Zr
0.9
O
2–δ
catalyst provides a ~50% increase in the hydrogen yield. |
---|---|
AbstractList | Results of a study of the methanol steam reforming (MSR) catalytic process in conventional flow and membrane reactors in the presence of Ni
0.2
–Cu
0.8
and Ru
0.5
–Rh
0.5
catalysts supported on ZrO
2
with a monoclinic, tetragonal, and cubic structure have been described. The cubic structure of zirconia has been stabilized with ceria. The samples have been characterized by X-ray diffraction analysis, transmission electron microscopy, and the BET method. It has been shown that the catalytic activity of the composites depends on the type of the metals and the structure of the support. It has been found that the Ru–Rh/Ce
0.1
Zr
0.9
O
2–δ
catalyst exhibits the highest activity, whereas Cu–Ni/Ce
0.1
Zr
0.9
O
2–δ
is the most selective. A comparative study of the MSR process in conventional and membrane reactors with Pd–Ru and modified Pd–Ag membranes has been conducted. The membrane process with a membrane based on a Pd–Ag alloy in the presence of the Ru–Rh/Ce
0.1
Zr
0.9
O
2–δ
catalyst provides a ~50% increase in the hydrogen yield. Results of a study of the methanol steam reforming (MSR) catalytic process in conventional flow and membrane reactors in the presence of Ni0.2–Cu0.8 and Ru0.5–Rh0.5 catalysts supported on ZrO2 with a monoclinic, tetragonal, and cubic structure have been described. The cubic structure of zirconia has been stabilized with ceria. The samples have been characterized by X-ray diffraction analysis, transmission electron microscopy, and the BET method. It has been shown that the catalytic activity of the composites depends on the type of the metals and the structure of the support. It has been found that the Ru–Rh/Ce0.1Zr0.9O2–δ catalyst exhibits the highest activity, whereas Cu–Ni/Ce0.1Zr0.9O2–δ is the most selective. A comparative study of the MSR process in conventional and membrane reactors with Pd–Ru and modified Pd–Ag membranes has been conducted. The membrane process with a membrane based on a Pd–Ag alloy in the presence of the Ru–Rh/Ce0.1Zr0.9O2–δ catalyst provides a ~50% increase in the hydrogen yield. |
Author | Yaroslavtsev, A. B. Baryshev, M. G. Petriev, I. S. Ermilova, M. M. Lytkina, A. A. Orekhova, N. V. |
Author_xml | – sequence: 1 givenname: A. A. surname: Lytkina fullname: Lytkina, A. A. email: lytkina@ips.ac.ru organization: Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences – sequence: 2 givenname: N. V. surname: Orekhova fullname: Orekhova, N. V. organization: Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences – sequence: 3 givenname: M. M. surname: Ermilova fullname: Ermilova, M. M. organization: Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences – sequence: 4 givenname: I. S. surname: Petriev fullname: Petriev, I. S. organization: Kuban State University – sequence: 5 givenname: M. G. surname: Baryshev fullname: Baryshev, M. G. organization: Kuban State University – sequence: 6 givenname: A. B. surname: Yaroslavtsev fullname: Yaroslavtsev, A. B. organization: Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences |
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Cites_doi | 10.1016/j.ijhydene.2011.08.117 10.1016/j.apcata.2013.11.025 10.1002/9783527627806 10.1081/SPM-120006115 10.1016/j.apcatb.2010.06.015 10.1021/cr050198b 10.1016/j.ijhydene.2014.11.082 10.1016/j.apcatb.2016.10.041 10.1016/j.ijhydene.2017.01.229 10.1016/j.jiec.2015.01.007 10.1016/0360-3199(86)90139-4 10.3103/S1062873816060241 10.1039/c0cy00012d 10.1016/j.jiec.2014.06.023 10.1021/ie400679h 10.1016/j.apcatb.2015.11.047 10.1016/S0920-5861(02)00230-4 10.1016/j.cattod.2011.03.068 10.1016/j.fuel.2016.11.058 10.1016/j.jpowsour.2015.01.168 10.1016/j.apsusc.2014.09.017 10.1016/j.ijhydene.2015.05.094 10.1016/j.apcatb.2015.02.039 10.1134/S0036023608030029 10.1016/j.ijhydene.2008.12.058 10.1016/j.ijhydene.2017.05.022 10.1016/j.ijhydene.2011.12.060 10.1016/j.ijhydene.2009.07.063 10.1016/j.rser.2013.08.032 |
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Keywords | Ru–Rh catalysts zirconia methanol steam reforming hydrogen production Ni–Cu catalysts membrane catalysis |
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0.2
–Cu
0.8
and Ru... Results of a study of the methanol steam reforming (MSR) catalytic process in conventional flow and membrane reactors in the presence of Ni0.2–Cu0.8 and... |
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SubjectTerms | Catalysis Catalysts Catalytic activity Cerium oxides Chemistry Chemistry and Materials Science Copper Electron microscopy Industrial Chemistry/Chemical Engineering Membrane reactors Methanol Nickel Palladium base alloys Reactors Reforming Ruthenium Silver base alloys Zirconium dioxide |
Title | Methanol Steam Reforming over ZrO2-Supported Catalysts in Conventional and Membrane Reactors |
URI | https://link.springer.com/article/10.1134/S0965544117130072 https://www.proquest.com/docview/2009642790/abstract/ |
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