First example of a heterobimetallic ‘Pd–Sn’ catalyst for direct activation of alcohol: efficient allylation, benzylation and propargylation of arenes, heteroarenes, active methylenes and allyl-Si nucleophiles
Arenes, heteroarenes, 1,3-dicarbonyls and organosilicon nucleophiles undergo highly efficient alkylation with allylic, propargylic and benzylic alcohols in the presence of a new 'Pd-Sn' bimetallic catalyst in nitromethane; water being the sole byproduct. The plausible mechanism of alkylati...
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| Published in | Organic & biomolecular chemistry Vol. 10; no. 23; pp. 4537 - 4542 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Royal Soc Chemistry
21.06.2012
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| Abstract | Arenes, heteroarenes, 1,3-dicarbonyls and organosilicon nucleophiles undergo highly efficient alkylation with allylic, propargylic and benzylic alcohols in the presence of a new 'Pd-Sn' bimetallic catalyst in nitromethane; water being the sole byproduct. The plausible mechanism of alkylation and the intermediacy of ether has been enumerated. |
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| AbstractList | Arenes, heteroarenes, 1,3-dicarbonyls and organosilicon nucleophiles undergo highly efficient alkylation with allylic, propargylic and benzylic alcohols in the presence of a new 'Pd-Sn' bimetallic catalyst in nitromethane; water being the sole byproduct. The plausible mechanism of alkylation and the intermediacy of ether has been enumerated.Arenes, heteroarenes, 1,3-dicarbonyls and organosilicon nucleophiles undergo highly efficient alkylation with allylic, propargylic and benzylic alcohols in the presence of a new 'Pd-Sn' bimetallic catalyst in nitromethane; water being the sole byproduct. The plausible mechanism of alkylation and the intermediacy of ether has been enumerated. Arenes, heteroarenes, 1,3-dicarbonyls and organosilicon nucleophiles undergo highly efficient alkylation with allylic, propargylic and benzylic alcohols in the presence of a new 'Pd-Sn' bimetallic catalyst in nitromethane; water being the sole byproduct. The plausible mechanism of alkylation and the intermediacy of ether has been enumerated. |
| Author | Roy, Ujjal Kanti Mal, Dipakranjan Roy, Sujit Das, Debjit Pratihar, Sanjay |
| Author_xml | – sequence: 1 givenname: Debjit surname: Das fullname: Das, Debjit – sequence: 2 givenname: Sanjay surname: Pratihar fullname: Pratihar, Sanjay – sequence: 3 givenname: Ujjal Kanti surname: Roy fullname: Roy, Ujjal Kanti – sequence: 4 givenname: Dipakranjan surname: Mal fullname: Mal, Dipakranjan – sequence: 5 givenname: Sujit surname: Roy fullname: Roy, Sujit |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/22580380$$D View this record in MEDLINE/PubMed |
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| Keywords | SUBSTITUTION INSERTION SECONDARY BENZYLATION HETEROGENEOUS ADDITION COMPLEXES ALLENYLATION AROMATICS FRIEDEL-CRAFTS ALKYLATION DERIVATIVES INDOLES |
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| Snippet | Arenes, heteroarenes, 1,3-dicarbonyls and organosilicon nucleophiles undergo highly efficient alkylation with allylic, propargylic and benzylic alcohols in the... |
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| Title | First example of a heterobimetallic ‘Pd–Sn’ catalyst for direct activation of alcohol: efficient allylation, benzylation and propargylation of arenes, heteroarenes, active methylenes and allyl-Si nucleophiles |
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