Characterization of nanocomposite laminates fabricated from aqueous dispersion of polyvinylpyrrolidone and l-leucine amino acid modified-montmorillonite

This study presents a favorable, simple, safe, fast, and facile approach for the synthesis of potentially ecofriendly biodegradable polymer nanocomposites (NC)s with amino acid modified-montmorillonite (AA-MMT). At first, positively charged chiral amino acid l -leucine was incorporated into the unmo...

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Published inPolymer bulletin (Berlin, Germany) Vol. 73; no. 10; pp. 2677 - 2688
Main Authors Mallakpour, Shadpour, Khani, Marziyeh
Format Journal Article
LanguageEnglish
Published Berlin/Heidelberg Springer Berlin Heidelberg 01.10.2016
Springer Nature B.V
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Abstract This study presents a favorable, simple, safe, fast, and facile approach for the synthesis of potentially ecofriendly biodegradable polymer nanocomposites (NC)s with amino acid modified-montmorillonite (AA-MMT). At first, positively charged chiral amino acid l -leucine was incorporated into the unmodified Cloisite-Na + montmorillonite (MMT) for organo-modification of MMT by cation-exchange method. Fourier transform infrared spectroscopy (FT-IR) showed the presence of the organic segment in the modified clay product. Then the dispersion characteristics of AA-MMT in the aforementioned NCs were determined based on polyvinylpyrrolidone (PVP). The obtained NCs were characterized by different analytical tools including FT-IR, powder X-ray diffraction (XRD), thermogravimetric analysis (TGA), transmission electron microscopy (TEM), and field emission scanning electron microscopy (FE-SEM). The XRD patterns, FE-SEM, and TEM results proposed that the AA-MMT platelets were intercalated with PVP during the process. As evidenced by TGA analysis of the obtained NCs, heat stability was slightly improved as compared with the pure PVP.
AbstractList This study presents a favorable, simple, safe, fast, and facile approach for the synthesis of potentially ecofriendly biodegradable polymer nanocomposites (NC)s with amino acid modified-montmorillonite (AA-MMT). At first, positively charged chiral amino acid l -leucine was incorporated into the unmodified Cloisite-Na + montmorillonite (MMT) for organo-modification of MMT by cation-exchange method. Fourier transform infrared spectroscopy (FT-IR) showed the presence of the organic segment in the modified clay product. Then the dispersion characteristics of AA-MMT in the aforementioned NCs were determined based on polyvinylpyrrolidone (PVP). The obtained NCs were characterized by different analytical tools including FT-IR, powder X-ray diffraction (XRD), thermogravimetric analysis (TGA), transmission electron microscopy (TEM), and field emission scanning electron microscopy (FE-SEM). The XRD patterns, FE-SEM, and TEM results proposed that the AA-MMT platelets were intercalated with PVP during the process. As evidenced by TGA analysis of the obtained NCs, heat stability was slightly improved as compared with the pure PVP.
This study presents a favorable, simple, safe, fast, and facile approach for the synthesis of potentially ecofriendly biodegradable polymer nanocomposites (NC)s with amino acid modified-montmorillonite (AA-MMT). At first, positively charged chiral amino acid l-leucine was incorporated into the unmodified Cloisite-Na+ montmorillonite (MMT) for organo-modification of MMT by cation-exchange method. Fourier transform infrared spectroscopy (FT-IR) showed the presence of the organic segment in the modified clay product. Then the dispersion characteristics of AA-MMT in the aforementioned NCs were determined based on polyvinylpyrrolidone (PVP). The obtained NCs were characterized by different analytical tools including FT-IR, powder X-ray diffraction (XRD), thermogravimetric analysis (TGA), transmission electron microscopy (TEM), and field emission scanning electron microscopy (FE-SEM). The XRD patterns, FE-SEM, and TEM results proposed that the AA-MMT platelets were intercalated with PVP during the process. As evidenced by TGA analysis of the obtained NCs, heat stability was slightly improved as compared with the pure PVP.
Author Mallakpour, Shadpour
Khani, Marziyeh
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Keywords Amino acid modified-montmorillonite
Polymer–clay nanocomposites
Morphology study
Polyvinylpyrrolidone
Solution intercalation process
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Snippet This study presents a favorable, simple, safe, fast, and facile approach for the synthesis of potentially ecofriendly biodegradable polymer nanocomposites...
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springer
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Publisher
StartPage 2677
SubjectTerms Amino acids
Carbon
Cation exchanging
Characterization and Evaluation of Materials
Chemical synthesis
Chemistry
Chemistry and Materials Science
Complex Fluids and Microfluidics
Dispersion
Emission analysis
Field emission microscopy
Fourier transforms
Infrared spectroscopy
Laminates
Leucine
Montmorillonite
Nanocomposites
Organic Chemistry
Original Paper
Physical Chemistry
Polymer Sciences
Polymers
Polyvinylpyrrolidone
R&D
Research & development
Scanning electron microscopy
Soft and Granular Matter
Spectrum analysis
Stability analysis
Surfactants
Thermogravimetric analysis
Transmission electron microscopy
X ray powder diffraction
X-ray diffraction
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Title Characterization of nanocomposite laminates fabricated from aqueous dispersion of polyvinylpyrrolidone and l-leucine amino acid modified-montmorillonite
URI https://link.springer.com/article/10.1007/s00289-016-1614-6
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