Triphenylene based metal-pyridine cages
[Display omitted] •We prepared three tris-pyridine containing triphenylene polydentate ligands.•Coordination with Pd(II) or Pt(II) metal corners led to different assemblies.•19F NMR was fundamental to monitor the formation of clear M3L2 aggregates.•M3L2 cage was confirmed by 2D-DOSY and semi-empiric...
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Published in | Tetrahedron letters Vol. 60; no. 43; pp. 151202 - 151208 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
Published |
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Elsevier Ltd
24.10.2019
Elsevier |
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Abstract | [Display omitted]
•We prepared three tris-pyridine containing triphenylene polydentate ligands.•Coordination with Pd(II) or Pt(II) metal corners led to different assemblies.•19F NMR was fundamental to monitor the formation of clear M3L2 aggregates.•M3L2 cage was confirmed by 2D-DOSY and semi-empirical calculations.•The stereochemistry of the assemblies was considered as well.
C3-symmetric pyridine containing tris-benzyl-O-substituted hexahydroxytriphenylene derivatives were prepared and used in combination with square-planar Pd(II) and Pt(II) complexes for the self-assembly of molecular cages in solution. The formation of a trigonal bipyramid M3L2 cage was demonstrated by multinuclear NMR analyses and pseudo 2D DOSY experiments and supported by semi-empirical calculations. |
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AbstractList | C-3-symmetric pyridine containing tris-benzyl-O-substituted hexahydroxytriphenylene derivatives were prepared and used in combination with square-planar Pd(II) and Pt(II) complexes for the self-assembly of molecular cages in solution. The formation of a trigonal bipyramid M3L2 cage was demonstrated by multinuclear NMR analyses and pseudo 2D DOSY experiments and supported by semi-empirical calculations. (C) 2019 Elsevier Ltd. All rights reserved. [Display omitted] •We prepared three tris-pyridine containing triphenylene polydentate ligands.•Coordination with Pd(II) or Pt(II) metal corners led to different assemblies.•19F NMR was fundamental to monitor the formation of clear M3L2 aggregates.•M3L2 cage was confirmed by 2D-DOSY and semi-empirical calculations.•The stereochemistry of the assemblies was considered as well. C3-symmetric pyridine containing tris-benzyl-O-substituted hexahydroxytriphenylene derivatives were prepared and used in combination with square-planar Pd(II) and Pt(II) complexes for the self-assembly of molecular cages in solution. The formation of a trigonal bipyramid M3L2 cage was demonstrated by multinuclear NMR analyses and pseudo 2D DOSY experiments and supported by semi-empirical calculations. |
ArticleNumber | 151202 |
Author | Sgarbossa, Paolo Santo, Claudio Berton, Giacomo Fabris, Fabrizio Lorenzetto, Tommaso Visentin, Fabiano Borsato, Giuseppe Scarso, Alessandro |
Author_xml | – sequence: 1 givenname: Giacomo surname: Berton fullname: Berton, Giacomo organization: Dipartimento di Scienze Molecolari e Nanosistemi, Università Ca’ Foscari di Venezia, Via Torino 155, 30172 Venezia Mestre, Italy – sequence: 2 givenname: Tommaso surname: Lorenzetto fullname: Lorenzetto, Tommaso organization: Dipartimento di Scienze Molecolari e Nanosistemi, Università Ca’ Foscari di Venezia, Via Torino 155, 30172 Venezia Mestre, Italy – sequence: 3 givenname: Giuseppe surname: Borsato fullname: Borsato, Giuseppe organization: Dipartimento di Scienze Molecolari e Nanosistemi, Università Ca’ Foscari di Venezia, Via Torino 155, 30172 Venezia Mestre, Italy – sequence: 4 givenname: Paolo surname: Sgarbossa fullname: Sgarbossa, Paolo organization: Dipartimento di Ingegneria Industriale, Università degli Studi di Padova, via Marzolo 9, 35131 Padova, Italy – sequence: 5 givenname: Claudio surname: Santo fullname: Santo, Claudio organization: Dipartimento di Scienze Molecolari e Nanosistemi, Università Ca’ Foscari di Venezia, Via Torino 155, 30172 Venezia Mestre, Italy – sequence: 6 givenname: Fabiano surname: Visentin fullname: Visentin, Fabiano organization: Dipartimento di Scienze Molecolari e Nanosistemi, Università Ca’ Foscari di Venezia, Via Torino 155, 30172 Venezia Mestre, Italy – sequence: 7 givenname: Fabrizio surname: Fabris fullname: Fabris, Fabrizio organization: Dipartimento di Scienze Molecolari e Nanosistemi, Università Ca’ Foscari di Venezia, Via Torino 155, 30172 Venezia Mestre, Italy – sequence: 8 givenname: Alessandro surname: Scarso fullname: Scarso, Alessandro email: alesca@unive.it organization: Dipartimento di Scienze Molecolari e Nanosistemi, Università Ca’ Foscari di Venezia, Via Torino 155, 30172 Venezia Mestre, Italy |
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Keywords | Platinum C3-symmetry Coordination cage Palladium Triphenylene Supramolecular chemistry Exchange process M12L24 NANOSPHERES CATALYSIS C-3-symmetry STABILIZATION COMPLEXES ENCAPSULATION DRIVEN M3L2 CAGES COORDINATION CAGES LIGANDS DISCRETE |
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•We prepared three tris-pyridine containing triphenylene polydentate ligands.•Coordination with Pd(II) or Pt(II) metal corners led to... C-3-symmetric pyridine containing tris-benzyl-O-substituted hexahydroxytriphenylene derivatives were prepared and used in combination with square-planar Pd(II)... |
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SubjectTerms | C3-symmetry Chemistry Chemistry, Organic Coordination cage Exchange process Palladium Physical Sciences Platinum Science & Technology Supramolecular chemistry Triphenylene |
Title | Triphenylene based metal-pyridine cages |
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