Crystal Structure of the Lanthanum Nitrate Complex with N-(2-Amino-4-methylpyridinyl)benzoylacetamide

A solid complex of lanthanum nitrate with a β-diketonate-type ligand, N-(2-amino-4-methylpyridinyl)benzoylacetamide, was synthesized. The title complex was crystallized in the monoclinic system, space group C2/c with a = 25.005(5)Å, b = 11.636(2)Å, c = 17.706(3)Å, β = 124.837(1)°, V = 4228.35(1)Å3,...

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Published inAnalytical Sciences ; X-ray Structure and Analysis Online Vol. 23; pp. x71 - x72
Main Authors XU, Li, TANG, Kuan-Zhen, TANG, Yu, TAN, Min-Yu
Format Journal Article
LanguageEnglish
Published Tokyo The Japan Society for Analytical Chemistry 2007
Japan Science and Technology Agency
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Abstract A solid complex of lanthanum nitrate with a β-diketonate-type ligand, N-(2-amino-4-methylpyridinyl)benzoylacetamide, was synthesized. The title complex was crystallized in the monoclinic system, space group C2/c with a = 25.005(5)Å, b = 11.636(2)Å, c = 17.706(3)Å, β = 124.837(1)°, V = 4228.35(1)Å3, Z = 4. The complex has a symmetry of C2, and the geometry of La(III) is a distorted bicapped square antiprism. In the structure of the title complex, a 3D supramolecular network is formed by hydrogen-bond interactions.
AbstractList A solid complex of lanthanum nitrate with a β-diketonate-type ligand, N-(2-amino-4-methylpyridinyl)benzoylacetamide, was synthesized. The title complex was crystallized in the monoclinic system, space group C2/c with a = 25.005(5)Å, b = 11.636(2)Å, c = 17.706(3)Å, β = 124.837(1)°, V = 4228.35(1)Å3, Z = 4. The complex has a symmetry of C2, and the geometry of La(III) is a distorted bicapped square antiprism. In the structure of the title complex, a 3D supramolecular network is formed by hydrogen-bond interactions.
A solid complex of lanthanum nitrate with a β-diketonate-type ligand, N-(2-amino-4-methylpyridinyl)benzoylacetamide, was synthesized. The title complex was crystallized in the monoclinic system, space group C2/c with a = 25.005(5)Å, b = 11.636(2)Å, c = 17.706(3)Å, β = 124.837(1)[Degree], V = 4228.35(1)Å3, Z = 4. The complex has a symmetry of C2, and the geometry of La(III) is a distorted bicapped square antiprism. In the structure of the title complex, a 3D supramolecular network is formed by hydrogen-bond interactions.
Author TANG, Yu
TAN, Min-Yu
XU, Li
TANG, Kuan-Zhen
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10.1016/0022-2860(95)09164-5
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Title Crystal Structure of the Lanthanum Nitrate Complex with N-(2-Amino-4-methylpyridinyl)benzoylacetamide
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