Laser-induced breakdown spectroscopy (LIBS) for carbon single shot analysis of micrometer-sized particles

The purpose of this work is to study the ability of the laser-induced breakdown spectroscopy (LIBS) technique to perform in situ (without sample preparation) detection of graphite particles circulating in a gas loop used to simulate the cooling gas circuit of a helium-cooled nuclear reactor. Results...

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Published inAnalytical and bioanalytical chemistry Vol. 385; no. 2; pp. 281 - 286
Main Authors Vors, E, Salmon, L
Format Journal Article
LanguageEnglish
Published Germany Berlin/Heidelberg : Springer-Verlag 01.05.2006
Springer Nature B.V
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Abstract The purpose of this work is to study the ability of the laser-induced breakdown spectroscopy (LIBS) technique to perform in situ (without sample preparation) detection of graphite particles circulating in a gas loop used to simulate the cooling gas circuit of a helium-cooled nuclear reactor. Results obtained with a laboratory scale set up are presented. The experiments were performed in nitrogen with micrometer-sized particles containing carbon (glucose particles and sodium hydrogenocarbonate particles). Statistical shot to shot analysis was used to determine the concentration of the analyte. The variation of LIBS signal as a function of glucose particle diameter showed an underestimation of the signal of particles of diameters larger than 5 μm. This phenomenon is likely to be correlated to an incomplete vaporization in the laser-induced plasma of particles of sizes above 5 μm. Analytical measurements were performed with glucose particles and sodium hydrogenocarbonate particles, and the concentration-based limit of detection of carbon was evaluated to be about 60 μg m-³.
AbstractList The purpose of this work is to study the ability of the laser-induced breakdown spectroscopy (LIBS) technique to perform in situ (without sample preparation) detection of graphite particles circulating in a gas loop used to simulate the cooling gas circuit of a helium-cooled nuclear reactor. Results obtained with a laboratory scale set up are presented. The experiments were performed in nitrogen with micrometer-sized particles containing carbon (glucose particles and sodium hydrogenocarbonate particles). Statistical shot to shot analysis was used to determine the concentration of the analyte. The variation of LIBS signal as a function of glucose particle diameter showed an underestimation of the signal of particles of diameters larger than 5 microm. This phenomenon is likely to be correlated to an incomplete vaporization in the laser-induced plasma of particles of sizes above 5 microm. Analytical measurements were performed with glucose particles and sodium hydrogenocarbonate particles, and the concentration-based limit of detection of carbon was evaluated to be about 60 microg m(-3).
The purpose of this work is to study the ability of the laser-induced breakdown spectroscopy (LIBS) technique to perform in situ (without sample preparation) detection of graphite particles circulating in a gas loop used to simulate the cooling gas circuit of a helium-cooled nuclear reactor. Results obtained with a laboratory scale set up are presented. The experiments were performed in nitrogen with micrometer-sized particles containing carbon (glucose particles and sodium hydrogenocarbonate particles). Statistical shot to shot analysis was used to determine the concentration of the analyte. The variation of LIBS signal as a function of glucose particle diameter showed an underestimation of the signal of particles of diameters larger than 5 μm. This phenomenon is likely to be correlated to an incomplete vaporization in the laser-induced plasma of particles of sizes above 5 μm. Analytical measurements were performed with glucose particles and sodium hydrogenocarbonate particles, and the concentration-based limit of detection of carbon was evaluated to be about 60 μg m−3.
The purpose of this work is to study the ability of the laser-induced breakdown spectroscopy (LIBS) technique to perform in situ (without sample preparation) detection of graphite particles circulating in a gas loop used to simulate the cooling gas circuit of a helium-cooled nuclear reactor. Results obtained with a laboratory scale set up are presented. The experiments were performed in nitrogen with micrometer-sized particles containing carbon (glucose particles and sodium hydrogenocarbonate particles). Statistical shot to shot analysis was used to determine the concentration of the analyte. The variation of LIBS signal as a function of glucose particle diameter showed an underestimation of the signal of particles of diameters larger than 5 μm. This phenomenon is likely to be correlated to an incomplete vaporization in the laser-induced plasma of particles of sizes above 5 μm. Analytical measurements were performed with glucose particles and sodium hydrogenocarbonate particles, and the concentration-based limit of detection of carbon was evaluated to be about 60 μg m-³.
Author Salmon, L
Vors, E
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Snippet The purpose of this work is to study the ability of the laser-induced breakdown spectroscopy (LIBS) technique to perform in situ (without sample preparation)...
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SubjectTerms Aerosols/particulates
Carbon
Carbon analysis
Circuits
Diameters
Glucose
Helium
Helium cooled nuclear reactors
Laser induced breakdown spectroscopy
Laser plasmas
Lasers
Nuclear reactors
Particle size
Sample preparation
Sodium
Spectroscopy
Spectrum analysis
Vaporization
Title Laser-induced breakdown spectroscopy (LIBS) for carbon single shot analysis of micrometer-sized particles
URI https://www.ncbi.nlm.nih.gov/pubmed/16479369
https://www.proquest.com/docview/2665369267
https://search.proquest.com/docview/67909056
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