Simple and efficient approach to synthesis of [1,2,4]triazolo[4,3-b][1,2,4,6]thiatriazine- 1-oxides from N-triazol-3-ylamidines

A facile method for the synthesis of [1,2,4]triazolo[4,3- ][1,2,4,6]thiatriazine 1-oxides is presented. The approach involves a reaction between -triazol-3-ylamidines and thionyl chloride in the presence of pyridine. The structures of the synthesized compounds were confirmed by spectral studies incl...

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Published inHeterocyclic communications Vol. 23; no. 2; pp. 97 - 100
Main Authors Hajri, Azhar, Marzouki, Mohamed Lamjed
Format Journal Article
LanguageEnglish
Published Berlin De Gruyter 01.04.2017
Walter de Gruyter GmbH
Subjects
[1,2,4]triazole
amidines
iminoester
Infrared radiation
NMR
Nuclear magnetic resonance
oxides
Synthesis
thiatriazine
thionyl chloride
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Abstract A facile method for the synthesis of [1,2,4]triazolo[4,3- ][1,2,4,6]thiatriazine 1-oxides is presented. The approach involves a reaction between -triazol-3-ylamidines and thionyl chloride in the presence of pyridine. The structures of the synthesized compounds were confirmed by spectral studies including IR, H NMR, C NMR, MS and elemental analysis.
AbstractList Abstract A facile method for the synthesis of [1,2,4]triazolo[4,3- b ][1,2,4,6]thiatriazine 1-oxides 3a–h is presented. The approach involves a reaction between N -triazol-3-ylamidines 2a–h and thionyl chloride in the presence of pyridine. The structures of the synthesized compounds were confirmed by spectral studies including IR, 1 H NMR, 13 C NMR, MS and elemental analysis.
A facile method for the synthesis of [1,2,4]triazolo[4,3- ][1,2,4,6]thiatriazine 1-oxides is presented. The approach involves a reaction between -triazol-3-ylamidines and thionyl chloride in the presence of pyridine. The structures of the synthesized compounds were confirmed by spectral studies including IR, H NMR, C NMR, MS and elemental analysis.
A facile method for the synthesis of [1,2,4]triazolo[4,3- b ][1,2,4,6]thiatriazine 1-oxides 3a-h is presented. The approach involves a reaction between N -triazol-3-ylamidines 2a-h and thionyl chloride in the presence of pyridine. The structures of the synthesized compounds were confirmed by spectral studies including IR, 1H NMR, 13C NMR, MS and elemental analysis.
Author Marzouki, Mohamed Lamjed
Hajri, Azhar
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Snippet A facile method for the synthesis of [1,2,4]triazolo[4,3- ][1,2,4,6]thiatriazine 1-oxides is presented. The approach involves a reaction between...
Abstract A facile method for the synthesis of [1,2,4]triazolo[4,3- b ][1,2,4,6]thiatriazine 1-oxides 3a–h is presented. The approach involves a reaction...
A facile method for the synthesis of [1,2,4]triazolo[4,3- b ][1,2,4,6]thiatriazine 1-oxides 3a-h is presented. The approach involves a reaction between N...
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StartPage 97
SubjectTerms [1,2,4]triazole
amidines
iminoester
Infrared radiation
NMR
Nuclear magnetic resonance
oxides
Synthesis
thiatriazine
thionyl chloride
Title Simple and efficient approach to synthesis of [1,2,4]triazolo[4,3-b][1,2,4,6]thiatriazine- 1-oxides from N-triazol-3-ylamidines
URI http://www.degruyter.com/doi/10.1515/hc-2017-0003
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Volume 23
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