Catalyst-free visible-light-initiated oxidative coupling of aryldiazo sulfones with thiols leading to unsymmetrical sulfoxides in air

A facile and efficient visible-light-driven method has been developed to construct sulfoxides via oxidative coupling of aryldiazo sulfones with thiols using the O 2 in air as the oxidant. This reaction could be performed at room temperature under catalyst- and additive-free conditions. The present m...

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Published inGreen chemistry : an international journal and green chemistry resource : GC Vol. 21; no. 7; pp. 169 - 1613
Main Authors Liu, Qishun, Wang, Leilei, Yue, Huilan, Li, Jiang-Sheng, Luo, Zidan, Wei, Wei
Format Journal Article
LanguageEnglish
Published CAMBRIDGE Royal Soc Chemistry 01.04.2019
Royal Society of Chemistry
Subjects
air
Air temperature
ambient temperature
Catalysis
Catalysts
Chemistry
Chemistry, Multidisciplinary
Coupling
Functional groups
Green & Sustainable Science & Technology
Green chemistry
moieties
oxidants
Oxidizing agents
oxygen
Physical Sciences
Science & Technology
Science & Technology - Other Topics
Sulfones
Sulfoxides
sustainable technology
Thiols
SULFINIC ACIDS
ALKENES
SELECTIVE OXIDATION
SULFIDES
STRATEGY
SINGLET OXYGEN
METAL
ALKYNES
HIGHLY EFFICIENT
PHOTOREDOX CATALYSIS
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Abstract A facile and efficient visible-light-driven method has been developed to construct sulfoxides via oxidative coupling of aryldiazo sulfones with thiols using the O 2 in air as the oxidant. This reaction could be performed at room temperature under catalyst- and additive-free conditions. The present methodology offers a mild and environmentally benign approach to obtain a library of sulfoxides in good yields with favorable functional group tolerance. A facile visible-light-driven method has been developed to construct sulfoxides from aryldiazo sulfones and thiols in air under photocatalyst-free conditions.
AbstractList A facile and efficient visible-light-driven method has been developed to construct sulfoxides via oxidative coupling of aryldiazo sulfones with thiols using the O2 in air as the oxidant. This reaction could be performed at room temperature under catalyst- and additive-free conditions. The present methodology offers a mild and environmentally benign approach to obtain a library of sulfoxides in good yields with favorable functional group tolerance.
A facile and efficient visible-light-driven method has been developed to construct sulfoxides via oxidative coupling of aryldiazo sulfones with thiols using the O 2 in air as the oxidant. This reaction could be performed at room temperature under catalyst- and additive-free conditions. The present methodology offers a mild and environmentally benign approach to obtain a library of sulfoxides in good yields with favorable functional group tolerance. A facile visible-light-driven method has been developed to construct sulfoxides from aryldiazo sulfones and thiols in air under photocatalyst-free conditions.
A facile and efficient visible-light-driven method has been developed to construct sulfoxides via oxidative coupling of aryldiazo sulfones with thiols using the O-2 in air as the oxidant. This reaction could be performed at room temperature under catalyst- and additive-free conditions. The present methodology offers a mild and environmentally benign approach to obtain a library of sulfoxides in good yields with favorable functional group tolerance.
A facile and efficient visible-light-driven method has been developed to construct sulfoxides via oxidative coupling of aryldiazo sulfones with thiols using the O 2 in air as the oxidant. This reaction could be performed at room temperature under catalyst- and additive-free conditions. The present methodology offers a mild and environmentally benign approach to obtain a library of sulfoxides in good yields with favorable functional group tolerance.
A facile and efficient visible-light-driven method has been developed to construct sulfoxides via oxidative coupling of aryldiazo sulfones with thiols using the O₂ in air as the oxidant. This reaction could be performed at room temperature under catalyst- and additive-free conditions. The present methodology offers a mild and environmentally benign approach to obtain a library of sulfoxides in good yields with favorable functional group tolerance.
Author Wei, Wei
Luo, Zidan
Li, Jiang-Sheng
Wang, Leilei
Yue, Huilan
Liu, Qishun
AuthorAffiliation Qufu Normal University
Chinese Academy of Sciences
School of Chemistry and food Engineering
Qinghai Provincial Key Laboratory of Tibetan Medicine Research and Key Laboratory of Tibetan Medicine Research
Changsha University of Science and Technology
Hunan University of Science and Technology
School of Chemistry and Chemical Engineering
Northwest Institute of Plateau Biology
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  name: Northwest Institute of Plateau Biology
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  name: Qufu Normal University
– sequence: 0
  name: Chinese Academy of Sciences
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  name: Changsha University of Science and Technology
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  name: School of Chemistry and food Engineering
– sequence: 0
  name: Qinghai Provincial Key Laboratory of Tibetan Medicine Research and Key Laboratory of Tibetan Medicine Research
Author_xml – sequence: 1
  givenname: Qishun
  surname: Liu
  fullname: Liu, Qishun
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  givenname: Leilei
  surname: Wang
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  givenname: Huilan
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  surname: Li
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  surname: Luo
  fullname: Luo, Zidan
– sequence: 6
  givenname: Wei
  surname: Wei
  fullname: Wei, Wei
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Keywords SULFINIC ACIDS
ALKENES
SELECTIVE OXIDATION
SULFIDES
STRATEGY
SINGLET OXYGEN
METAL
ALKYNES
HIGHLY EFFICIENT
PHOTOREDOX CATALYSIS
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PublicationDecade 2010
PublicationPlace CAMBRIDGE
PublicationPlace_xml – name: CAMBRIDGE
– name: Cambridge
PublicationTitle Green chemistry : an international journal and green chemistry resource : GC
PublicationTitleAbbrev GREEN CHEM
PublicationYear 2019
Publisher Royal Soc Chemistry
Royal Society of Chemistry
Publisher_xml – name: Royal Soc Chemistry
– name: Royal Society of Chemistry
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Snippet A facile and efficient visible-light-driven method has been developed to construct sulfoxides via oxidative coupling of aryldiazo sulfones with thiols using...
A facile and efficient visible-light-driven method has been developed to construct sulfoxides via oxidative coupling of aryldiazo sulfones with thiols using...
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SubjectTerms air
Air temperature
ambient temperature
Catalysis
Catalysts
Chemistry
Chemistry, Multidisciplinary
Coupling
Functional groups
Green & Sustainable Science & Technology
Green chemistry
moieties
oxidants
Oxidizing agents
oxygen
Physical Sciences
Science & Technology
Science & Technology - Other Topics
Sulfones
Sulfoxides
sustainable technology
Thiols
Title Catalyst-free visible-light-initiated oxidative coupling of aryldiazo sulfones with thiols leading to unsymmetrical sulfoxides in air
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