Ultrafast high-temperature sintering of gadolinia-doped ceria
Ultrafast high-temperature sintering (UHS) is a rapidly growing research area of material science and engineering. Herein we present UHS of gadolinia-doped ceria (GDC) powders in single and multi-step approaches. The sintered ceramics were characterized from a physical and electrochemical point of v...
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| Published in | Journal of the European Ceramic Society Vol. 43; no. 11; pp. 4837 - 4843 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.09.2023
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0955-2219 1873-619X |
| DOI | 10.1016/j.jeurceramsoc.2023.04.025 |
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| Abstract | Ultrafast high-temperature sintering (UHS) is a rapidly growing research area of material science and engineering. Herein we present UHS of gadolinia-doped ceria (GDC) powders in single and multi-step approaches. The sintered ceramics were characterized from a physical and electrochemical point of view. When the power is applied gradually during the multistep UHS process crack-free GDC ceramics can be obtained with 95 % bulk density using commercial powder. Oxalate converted GDC powder gave 86 % bulk density with the same multistep sintering process. Additionally, it is shown that multistep UHS is also suitable for multilayer co-sintering necessary for solid oxide fuel cells (SOFC), as demonstrated by the production of dense GDC electrolyte in tight contact with porous electrodes.
•Ultrafast high-temperature sintering was used to prepare Gd-doped ceria ceramics.•Single and multi-step sintering cycles were developed to improve the final compacts.•Electrochemical performance of the final ceramics was studied.•Co-sintering of SOFC layered systems by UHS was successfully developed. |
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| AbstractList | Ultrafast high-temperature sintering (UHS) is a rapidly growing research area of material science and engineering. Herein we present UHS of gadolinia-doped ceria (GDC) powders in single and multi-step approaches. The sintered ceramics were characterized from a physical and electrochemical point of view. When the power is applied gradually during the multistep UHS process crack-free GDC ceramics can be obtained with 95 % bulk density using commercial powder. Oxalate converted GDC powder gave 86 % bulk density with the same multistep sintering process. Additionally, it is shown that multistep UHS is also suitable for multilayer co-sintering necessary for solid oxide fuel cells (SOFC), as demonstrated by the production of dense GDC electrolyte in tight contact with porous electrodes.
•Ultrafast high-temperature sintering was used to prepare Gd-doped ceria ceramics.•Single and multi-step sintering cycles were developed to improve the final compacts.•Electrochemical performance of the final ceramics was studied.•Co-sintering of SOFC layered systems by UHS was successfully developed. |
| Author | Tkach, Alexander Biesuz, Mattia Javan, Kimia Y. Sglavo, Vincenzo M. Tyrpekl, Václav Alemayehu, Adam Vilarinho, Paula M. |
| Author_xml | – sequence: 1 givenname: Adam surname: Alemayehu fullname: Alemayehu, Adam organization: Department of Inorganic Chemistry, Faculty of Science, Charles University, Hlavova 2030/8, 128 43 Prague, Czech Republic – sequence: 2 givenname: Mattia orcidid: 0000-0002-4338-4177 surname: Biesuz fullname: Biesuz, Mattia email: mattia.biesuz@unitn.it organization: Department of Industrial Engineering, University of Trento, via Sommarive 9, 38123 Trento, Italy – sequence: 3 givenname: Kimia Y. surname: Javan fullname: Javan, Kimia Y. organization: Department of Industrial Engineering, University of Trento, via Sommarive 9, 38123 Trento, Italy – sequence: 4 givenname: Alexander orcidid: 0000-0002-0318-9262 surname: Tkach fullname: Tkach, Alexander organization: CICECO-Aveiro Institute of Materials, Department of Materials and Ceramic Engineering, University of Aveiro, 3810-193 Aveiro, Portugal – sequence: 5 givenname: Paula M. surname: Vilarinho fullname: Vilarinho, Paula M. organization: CICECO-Aveiro Institute of Materials, Department of Materials and Ceramic Engineering, University of Aveiro, 3810-193 Aveiro, Portugal – sequence: 6 givenname: Vincenzo M. surname: Sglavo fullname: Sglavo, Vincenzo M. organization: Department of Industrial Engineering, University of Trento, via Sommarive 9, 38123 Trento, Italy – sequence: 7 givenname: Václav surname: Tyrpekl fullname: Tyrpekl, Václav email: vaclav.tyrpekl@natur.cuni.cz organization: Department of Inorganic Chemistry, Faculty of Science, Charles University, Hlavova 2030/8, 128 43 Prague, Czech Republic |
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| Keywords | Oxygen conductor Gadolinia Ultrafast sintering Ceria |
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| Title | Ultrafast high-temperature sintering of gadolinia-doped ceria |
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