Development of Armillae mellea immobilized nanodiamond for the preconcentrations of Cr(III), Hg(II) and Zn(II)

In this study, we present an environmental friend and easy procedure for simultaneous preconcentration of Cr(III), Hg(II) and Zn(II) by solid-phase extraction before their determination by inductively coupled plasma optical emission spectrometry. Armillae mellea immobilized nanodiamond was used as s...

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Published inAnalytical biochemistry Vol. 617; p. 114122
Main Authors Ozdemir, Sadin, Kılınç, Ersin, Şen, Fatih, Soylak, Mustafa
Format Journal Article
LanguageEnglish
Published United States Elsevier Inc 15.03.2021
Subjects
Food analysis
Metal ions
Preconcentration
Sensitivity enhancement
Solid-phase extraction
Preconcentration
Sensitivity enhancement
Food analysis
Solid-phase extraction
Metal ions
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Abstract In this study, we present an environmental friend and easy procedure for simultaneous preconcentration of Cr(III), Hg(II) and Zn(II) by solid-phase extraction before their determination by inductively coupled plasma optical emission spectrometry. Armillae mellea immobilized nanodiamond was used as sorbent. During the study, critical parameters influencing the extraction performance were investigated in detail. The best parameters were found as pH 5.0, 2.0 mL min−1 of flow rate, 200 mg of Armillae mellea, 300 mL of sample volume. LOD values were found as 0.025, 0.13 and 0.038 ng mL−1, respectively for Cr(III), Hg(II) and Zn(II). By applying the developed procedure, sensitivities of ICP-OES were improved for 60 fold for Cr(III), Hg(II) and Zn(II). Their concentrations in different food samples were measured after microwave digestion and solid-phase extraction. [Display omitted] •A new biosorbent for solid phase extraction is recommended.•Armillae mellea was immobilized on nanodiamond.•Cr(III), Hg(II) and Zn(II) were simultaneously preconcentrated.•The method was validated and applied to real samples.
AbstractList In this study, we present an environmental friend and easy procedure for simultaneous preconcentration of Cr(III), Hg(II) and Zn(II) by solid-phase extraction before their determination by inductively coupled plasma optical emission spectrometry. Armillae mellea immobilized nanodiamond was used as sorbent. During the study, critical parameters influencing the extraction performance were investigated in detail. The best parameters were found as pH 5.0, 2.0 mL min−1 of flow rate, 200 mg of Armillae mellea, 300 mL of sample volume. LOD values were found as 0.025, 0.13 and 0.038 ng mL−1, respectively for Cr(III), Hg(II) and Zn(II). By applying the developed procedure, sensitivities of ICP-OES were improved for 60 fold for Cr(III), Hg(II) and Zn(II). Their concentrations in different food samples were measured after microwave digestion and solid-phase extraction. [Display omitted] •A new biosorbent for solid phase extraction is recommended.•Armillae mellea was immobilized on nanodiamond.•Cr(III), Hg(II) and Zn(II) were simultaneously preconcentrated.•The method was validated and applied to real samples.
In this study, we present an environmental friend and easy procedure for simultaneous preconcentration of Cr(III), Hg(II) and Zn(II) by solid-phase extraction before their determination by inductively coupled plasma optical emission spectrometry. Armillae mellea immobilized nanodiamond was used as sorbent. During the study, critical parameters influencing the extraction performance were investigated in detail. The best parameters were found as pH 5.0, 2.0 mL min of flow rate, 200 mg of Armillae mellea, 300 mL of sample volume. LOD values were found as 0.025, 0.13 and 0.038 ng mL , respectively for Cr(III), Hg(II) and Zn(II). By applying the developed procedure, sensitivities of ICP-OES were improved for 60 fold for Cr(III), Hg(II) and Zn(II). Their concentrations in different food samples were measured after microwave digestion and solid-phase extraction.
ArticleNumber 114122
Author Kılınç, Ersin
Şen, Fatih
Ozdemir, Sadin
Soylak, Mustafa
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Keywords Preconcentration
Sensitivity enhancement
Food analysis
Solid-phase extraction
Metal ions
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Snippet In this study, we present an environmental friend and easy procedure for simultaneous preconcentration of Cr(III), Hg(II) and Zn(II) by solid-phase extraction...
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StartPage 114122
SubjectTerms Food analysis
Metal ions
Preconcentration
Sensitivity enhancement
Solid-phase extraction
Title Development of Armillae mellea immobilized nanodiamond for the preconcentrations of Cr(III), Hg(II) and Zn(II)
URI https://dx.doi.org/10.1016/j.ab.2021.114122
https://www.ncbi.nlm.nih.gov/pubmed/33515499
Volume 617
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