Properties in aqueous solution of homo- and copolymers of vinylphosphonic acid derivatives obtained by UV-curing
Vinylphosphonic acid is homopolymerized with dimethylvinylphosphonate by radical polymerization using using UV light and photoinitiator Darocur 4265 (3 wt%). The molar ratio between vinylphosphonic acid and dimethylvinylphosphonate is varied between 1:1 and 4:1, respectively. The obtained homopolyme...
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| Published in | Macromolecular research Vol. 25; no. 3; pp. 214 - 221 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Seoul
The Polymer Society of Korea
01.03.2017
Springer Nature B.V 한국고분자학회 |
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| Abstract | Vinylphosphonic acid is homopolymerized with dimethylvinylphosphonate by radical polymerization using using UV light and photoinitiator Darocur 4265 (3 wt%). The molar ratio between vinylphosphonic acid and dimethylvinylphosphonate is varied between 1:1 and 4:1, respectively. The obtained homopolymer of vinylphosphonic acid and copolymers are characterized by Fourier transform infrared spectroscopy (FTIR), thermal analysis and size exclusion chromatography - multi angle laser light scattering. The polymerization by UV light is efficient and an average molar mass of 34,200 g/mol is obtained for poly(vinylphosphonic acid) and in the range from 12,700 to 19,120 g/mol for copolymers, which also have a good thermal stability until 320 °C. The polymers structure allows the formation of random coil conformation. The copolymers are tested as inhibitors against corrosion of iron in NaCl aqueous solution, and, as a result, it was shown that these copolymers exhibit promising anticorrosion properties. |
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| AbstractList | Vinylphosphonic acid is homopolymerized with dimethylvinylphosphonate by radical polymerization using using UV light and photoinitiator Darocur 4265 (3 wt%). The molar ratio between vinylphosphonic acid and dimethylvinylphosphonate is varied between 1:1 and 4:1, respectively. The obtained homopolymer of vinylphosphonic acid and copolymers are characterized by Fourier transform infrared spectroscopy (FTIR), thermal analysis and size exclusion chromatography - multi angle laser light scattering. The polymerization by UV light is efficient and an average molar mass of 34,200 g/mol is obtained for poly(vinylphosphonic acid) and in the range from 12,700 to 19,120 g/mol for copolymers, which also have a good thermal stability until 320 °C. The polymers structure allows the formation of random coil conformation. The copolymers are tested as inhibitors against corrosion of iron in NaCl aqueous solution, and, as a result, it was shown that these copolymers exhibit promising anticorrosion properties. Vinylphosphonic acid is homopolymerized with dimethylvinylphosphonate by radical polymerization using using UV light and photoinitiator Darocur 4265 (3 wt%). The molar ratio between vinylphosphonic acid and dimethylvinylphosphonate is varied between 1:1 and 4:1, respectively. The obtained homopolymer of vinylphosphonic acid and copolymers are characterized by Fourier transform infrared spectroscopy (FTIR), thermal analysis and size exclusion chromatography - multi angle laser light scattering. The polymerization by UV light is efficient and an average molar mass of 34,200 g/mol is obtained for poly(vinylphosphonic acid) and in the range from 12,700 to 19,120 g/mol for copolymers, which also have a good thermal stability until 320 oC. The polymers structure allows the formation of random coil conformation. The copolymers are tested as inhibitors against corrosion of iron in NaCl aqueous solution, and, as a result, it was shown that these copolymers exhibit promising anticorrosion properties. KCI Citation Count: 3 |
| Author | Plesu, Nicoleta Tara-Lunga-Mihali, Milica Iliescu, Smaranda Ilia, Gheorghe Simulescu, Vasile Macarie, Lavinia Pekar, Miloslav |
| Author_xml | – sequence: 1 givenname: Lavinia surname: Macarie fullname: Macarie, Lavinia organization: Institute of Chemistry Timisoara of Romanian Academy – sequence: 2 givenname: Miloslav surname: Pekar fullname: Pekar, Miloslav organization: Materials Research Centre, Faculty of Chemistry, Brno University of Technology – sequence: 3 givenname: Vasile surname: Simulescu fullname: Simulescu, Vasile organization: Institute of Chemistry Timisoara of Romanian Academy, Materials Research Centre, Faculty of Chemistry, Brno University of Technology – sequence: 4 givenname: Nicoleta surname: Plesu fullname: Plesu, Nicoleta organization: Institute of Chemistry Timisoara of Romanian Academy – sequence: 5 givenname: Smaranda surname: Iliescu fullname: Iliescu, Smaranda organization: Institute of Chemistry Timisoara of Romanian Academy – sequence: 6 givenname: Gheorghe surname: Ilia fullname: Ilia, Gheorghe email: ilia@acad-icht.tm.edu.ro organization: Institute of Chemistry Timisoara of Romanian Academy – sequence: 7 givenname: Milica surname: Tara-Lunga-Mihali fullname: Tara-Lunga-Mihali, Milica organization: Institute of Chemistry Timisoara of Romanian Academy |
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| CitedBy_id | crossref_primary_10_3390_polym14030590 crossref_primary_10_3390_ma16082954 crossref_primary_10_3390_gels9090706 crossref_primary_10_3390_batteries10020056 crossref_primary_10_1007_s11696_018_0596_2 crossref_primary_10_1016_j_porgcoat_2019_04_060 crossref_primary_10_3390_ijms24021613 |
| Cites_doi | 10.1016/S0300-5712(98)00061-X 10.1002/macp.201200434 10.1016/j.ijbiomac.2013.12.018 10.1002/app.28626 10.1016/j.polymdegradstab.2015.06.012 10.1021/bm9014182 10.1016/j.porgcoat.2013.10.002 10.1063/1.1746738 10.1016/j.polymdegradstab.2014.12.005 10.1002/marc.200600513 10.1016/j.porgcoat.2004.08.005 10.1016/j.dental.2004.07.014 10.1201/9781420018271 10.1039/9781782624523-00271 10.1016/j.eurpolymj.2011.12.015 10.1021/la981694g 10.1016/0032-3861(79)90298-2 10.1021/la025570m 10.1002/app.20246 10.1016/j.progpolymsci.2010.04.001 10.1021/ma800042m 10.1016/S0141-3910(98)00123-2 10.1021/cr2004212 10.1201/NOE0824727857.ch307 10.1007/s13233-015-3135-9 10.1016/j.ssi.2007.02.007 10.4152/pea.200801047 10.1016/j.corsci.2007.01.010 10.1002/ange.201000804 10.1016/j.electacta.2009.09.023 10.1002/0470011149 10.1016/j.apsusc.2005.07.073 10.1021/ie0607898 |
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| Keywords | copolymers poly(vinylphosphonic acid) anticorrosion SEC-MALLS electrochemical impedance |
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| Snippet | Vinylphosphonic acid is homopolymerized with dimethylvinylphosphonate by radical polymerization using using UV light and photoinitiator Darocur 4265 (3 wt%).... |
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| SubjectTerms | Aqueous solutions Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Complex Fluids and Microfluidics Copolymers Infrared spectroscopy Light scattering Nanochemistry Nanotechnology Physical Chemistry Polymer Sciences Soft and Granular Matter Thermal stability 고분자공학 |
| Title | Properties in aqueous solution of homo- and copolymers of vinylphosphonic acid derivatives obtained by UV-curing |
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