Dechlorination of zinc dross by microwave roasting
Traditional treatments of zinc dross have many disadvantages, such as complicated recovering process and serious environmental pollution. In this work, a new process of chlorine removal from zinc dross by microwave was proposed for solving problem of recycling the zinc dross. With better ability of...
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| Published in | Journal of Central South University Vol. 21; no. 7; pp. 2627 - 2632 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Heidelberg
Central South University
01.07.2014
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| Subjects | |
| Online Access | Get full text |
| ISSN | 2095-2899 2227-5223 |
| DOI | 10.1007/s11771-014-2222-y |
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| Abstract | Traditional treatments of zinc dross have many disadvantages, such as complicated recovering process and serious environmental pollution. In this work, a new process of chlorine removal from zinc dross by microwave was proposed for solving problem of recycling the zinc dross. With better ability of absorbing the microwave than zinc oxide, the main material in zinc dross, chlorides, can be heated and evaporated rapidly during microwave roasting. Various parameters including roasting temperature, duration time and stirring speed were optimized. The microstructure of roasted materials was characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM). The content of the chloride was analyzed by the method of chlorine ion selective electrode. The experiments indicate that the best duration time is 60 min with a stirring speed of 15 r/min during the microwave roasting process. The dechlorination rate reaches peak value of 88% at 700 °C. The chlorine is removed as HCl gas when water vapor is used as activating agent, which means that it can be recovered into hydrochloride acid. |
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| AbstractList | Traditional treatments of zinc dross have many disadvantages, such as complicated recovering process and serious environmental pollution. In this work, a new process of chlorine removal from zinc dross by microwave was proposed for solving problem of recycling the zinc dross. With better ability of absorbing the microwave than zinc oxide, the main material in zinc dross, chlorides, can be heated and evaporated rapidly during microwave roasting. Various parameters including roasting temperature, duration time and stirring speed were optimized. The microstructure of roasted materials was characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM). The content of the chloride was analyzed by the method of chlorine ion selective electrode. The experiments indicate that the best duration time is 60 min with a stirring speed of 15 r/min during the microwave roasting process. The dechlorination rate reaches peak value of 88% at 700 °C. The chlorine is removed as HCl gas when water vapor is used as activating agent, which means that it can be recovered into hydrochloride acid. |
| Author | Zheng, Qin Zhang, Li-bo Ju, Shao-hua Wang, Ya-jian Xia, Yi Wei, Ya-qian Peng, Jin-hui |
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| CitedBy_id | crossref_primary_10_1016_j_seppur_2021_120221 crossref_primary_10_1515_htmp_2014_0206 crossref_primary_10_1016_j_jallcom_2015_08_120 crossref_primary_10_3390_met11121922 crossref_primary_10_1515_htmp_2014_0177 crossref_primary_10_3390_met8121025 crossref_primary_10_1590_0104_6632_20160331s00003530 crossref_primary_10_1016_j_cep_2015_03_024 crossref_primary_10_1016_j_jece_2023_109362 crossref_primary_10_1515_gps_2015_0041 |
| Cites_doi | 10.1016/j.hydromet.2008.02.008 10.1016/j.mineng.2004.01.007 10.1007/s11771-014-2065-6 10.1016/S0921-3449(01)00088-X 10.1016/j.fuproc.2012.01.031 10.1016/S0921-3449(00)00095-1 10.1016/j.minpro.2009.09.001 10.1016/S0304-386X(98)00012-7 10.1016/j.jhazmat.2010.05.098 10.1016/j.chemosphere.2010.10.074 10.1134/S1064229311020177 10.1007/s11661-011-1056-6 10.1016/S1003-6326(09)60204-1 10.1016/S0301-7516(99)00009-5 10.1034/j.1600-0692.2000.d01-26.x 10.1016/j.mineng.2009.02.015 10.1016/j.seppur.2005.11.003 10.1016/j.jhazmat.2007.01.143 10.1016/S1003-6326(11)60700-0 10.1016/j.jtice.2009.08.012 10.1016/S1003-6326(08)60167-3 |
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| Keywords | zinc dross dechlorination resources recovery microwave roasting |
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