Graphene oxide-monohydrated manganese phosphate composites: Preparation via modified Hummers method
[Display omitted] A modified Hummers method was established to prepare graphene oxide-MnPO4·H2O (denoted as GO-MnPO4·H2O) composites. Findings indicate that the as-formed GO-MnPO4·H2O particles are of a petal-shape and exhibit a uniform size of ∼1.2 μm, and they are stable and remain nearly unchange...
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| Published in | Colloids and surfaces. A, Physicochemical and engineering aspects Vol. 547; pp. 56 - 63 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
20.06.2018
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| Subjects | |
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| Abstract | [Display omitted]
A modified Hummers method was established to prepare graphene oxide-MnPO4·H2O (denoted as GO-MnPO4·H2O) composites. Findings indicate that the as-formed GO-MnPO4·H2O particles are of a petal-shape and exhibit a uniform size of ∼1.2 μm, and they are stable and remain nearly unchanged after 2 day of standing at 30 ℃ in air. The formation mechanism was investigated by computer simulations in combination with experimental explorations. The Mn2+ ions obtained by oxidation reaction can be distributed around the oxygen-containing functional groups of GO (especially for hydroxyl) and interact with them via electrostatic forces or coordination bonds. The as-formed GO-Mn2+ dipolar pair can further act as the anchor sites to facilitate the growth of MnPO4·H2O. During the formation of GO-MnPO4·H2O composites, MnPO4·H2O species contributes to promoting the exfoliation of GO sheets. Moreover, the polycrystalline structure of GO-MnPO4·H2O aggregates is destroyed heavily under 450 °C, and they can be decomposed to generate reduced GO-Mn2P2O7 (denoted as rGO-Mn2P2O7) after 900 ℃ treatment in N2 atmosphere. This methodology made the synthesis of GO-MnPO4·H2O and rGO-Mn2P2O7 composites possible and may be further extended to prepare more complicated nanocomposites based on GO sheets for technological applications. |
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| AbstractList | [Display omitted]
A modified Hummers method was established to prepare graphene oxide-MnPO4·H2O (denoted as GO-MnPO4·H2O) composites. Findings indicate that the as-formed GO-MnPO4·H2O particles are of a petal-shape and exhibit a uniform size of ∼1.2 μm, and they are stable and remain nearly unchanged after 2 day of standing at 30 ℃ in air. The formation mechanism was investigated by computer simulations in combination with experimental explorations. The Mn2+ ions obtained by oxidation reaction can be distributed around the oxygen-containing functional groups of GO (especially for hydroxyl) and interact with them via electrostatic forces or coordination bonds. The as-formed GO-Mn2+ dipolar pair can further act as the anchor sites to facilitate the growth of MnPO4·H2O. During the formation of GO-MnPO4·H2O composites, MnPO4·H2O species contributes to promoting the exfoliation of GO sheets. Moreover, the polycrystalline structure of GO-MnPO4·H2O aggregates is destroyed heavily under 450 °C, and they can be decomposed to generate reduced GO-Mn2P2O7 (denoted as rGO-Mn2P2O7) after 900 ℃ treatment in N2 atmosphere. This methodology made the synthesis of GO-MnPO4·H2O and rGO-Mn2P2O7 composites possible and may be further extended to prepare more complicated nanocomposites based on GO sheets for technological applications. |
| Author | Ju, Pengfei Ji, Li Wu, Yanping Li, Hongxuan Zhou, Huidi Chen, Lei Yuan, Rui Chen, Jianmin Yuan, Jing |
| Author_xml | – sequence: 1 givenname: Rui surname: Yuan fullname: Yuan, Rui organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China – sequence: 2 givenname: Jing surname: Yuan fullname: Yuan, Jing organization: College of Physics Electronic Information Engineering, Qinghai University for Nationalities, Xining, Qinghai 810007, PR China – sequence: 3 givenname: Yanping surname: Wu fullname: Wu, Yanping organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China – sequence: 4 givenname: Pengfei surname: Ju fullname: Ju, Pengfei organization: Shanghai Aerospace Equipment Manufacturer, Shanghai, 200245, PR China – sequence: 5 givenname: Li surname: Ji fullname: Ji, Li organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China – sequence: 6 givenname: Hongxuan surname: Li fullname: Li, Hongxuan organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China – sequence: 7 givenname: Lei surname: Chen fullname: Chen, Lei email: chenlei@licp.cas.cn organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China – sequence: 8 givenname: Huidi surname: Zhou fullname: Zhou, Huidi organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China – sequence: 9 givenname: Jianmin surname: Chen fullname: Chen, Jianmin email: chenjm@licp.cas.cn organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, PR China |
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A modified Hummers method was established to prepare graphene oxide-MnPO4·H2O (denoted as GO-MnPO4·H2O) composites. Findings indicate that... |
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| SubjectTerms | Computer simulation Graphene oxide-MnPO4·H2O Reduced GO-Mn2P2O7 |
| Title | Graphene oxide-monohydrated manganese phosphate composites: Preparation via modified Hummers method |
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