The study of thermal interaction and microstructure of sodium silicate/bentonite composite under microwave radiation
The commercial heating oven usually consumes the power around 2500–3000 Watt and the temperature inside the oven is still below 350 °C. If we need to increase a temperature above 500 °C, a special heating setup with a higher power furnace is required. However, in this work, we propose a composite ma...
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Published in | Materials chemistry and physics Vol. 184; pp. 345 - 350 |
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Main Author | |
Format | Journal Article |
Language | English |
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Lausanne
Elsevier B.V
01.12.2016
Elsevier BV |
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Abstract | The commercial heating oven usually consumes the power around 2500–3000 Watt and the temperature inside the oven is still below 350 °C. If we need to increase a temperature above 500 °C, a special heating setup with a higher power furnace is required. However, in this work, we propose a composite material that interacts with 2.45 GHz 500 Watt microwave and rapidly redeems the thermal energy with the temperature around 600–900 °C. The composite amorphous material easily forms liquid ceramics phase with a high temperature output and responds to the microwave radiation better than that of the solid phase. During the heating process, phase transformation occurs. This method is very effective and can be used to drastically reduce the power consumption of any heating process.
•Amorphous phase transforms to liquid phase by microwave radiation.•Pure sodium silicate and pure bentonite cannot show temperature overshoot.•Silicate-bentonite composite shows a high temperature overshoot above 700 °C.•A rapid heating crucible for the annealing application is fabricated. |
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AbstractList | The subject of this research is to explore the possibility of preparation of nanocomposite material of improved thermo-mechanical and tribological properties, using inorganic fullerene-like tungsten disulfide nanostructures (IF-WS2) as reinforcement in poly(vinyl butyral) (PVB). This paper also reports investigation of the effects of using different solvents in preparation of PVB/IF-WS2 nanocomposite on the thermo-mechanical behavior of the resulting material. PVB was dissolved in ethanol, isopropanol, n-butanol and ethyl acetate. IF-WS2 nanoparticles were added to these PVB solutions and dispersed by different deagglomeration techniques. Samples were dried and thin films were obtained. Their microstructure and the quality of IF-WS2 dispersion and deagglomeration in PVB matrix was analyzed by scanning electron microscope (SEM). The reinforcing effect of IF-WS2 is examined by determining hardness, reduced modulus of elasticity and coefficient of friction, by nanoindentation and nanoscratch test, in terms of the different solvents applied in preparation of the samples, mode of stirring and different contents of IF-WS2. The glass transition temperature (Tg) was determined for the prepared samples using differential scanning calorimetry (DSC) and dynamic mechanical thermal analysis (DMA). Storage modulus and mechanical loss factor were observed in a defined temperature range using DMA. The commercial heating oven usually consumes the power around 2500–3000 Watt and the temperature inside the oven is still below 350 °C. If we need to increase a temperature above 500 °C, a special heating setup with a higher power furnace is required. However, in this work, we propose a composite material that interacts with 2.45 GHz 500 Watt microwave and rapidly redeems the thermal energy with the temperature around 600–900 °C. The composite amorphous material easily forms liquid ceramics phase with a high temperature output and responds to the microwave radiation better than that of the solid phase. During the heating process, phase transformation occurs. This method is very effective and can be used to drastically reduce the power consumption of any heating process. •Amorphous phase transforms to liquid phase by microwave radiation.•Pure sodium silicate and pure bentonite cannot show temperature overshoot.•Silicate-bentonite composite shows a high temperature overshoot above 700 °C.•A rapid heating crucible for the annealing application is fabricated. |
Author | Subannajui, Kittitat |
Author_xml | – sequence: 1 givenname: Kittitat surname: Subannajui fullname: Subannajui, Kittitat email: kittitat.sub@mahidol.ac.th organization: Faculty of Science, Mahidol University, 272 Rama VI Road, Ratchathewi District, Bangkok 10400, Thailand |
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CitedBy_id | crossref_primary_10_1016_j_ceramint_2024_01_348 crossref_primary_10_1016_j_compositesb_2019_106909 |
Cites_doi | 10.1111/j.1551-2916.2010.04286.x 10.1111/j.1151-2916.1992.tb08184.x 10.1111/jace.12393 10.1111/j.1745-4549.1993.tb00230.x 10.1016/j.icheatmasstransfer.2013.09.008 10.1016/j.scriptamat.2007.06.009 10.1346/CCMN.2014.0620303 10.1016/j.matlet.2009.01.086 10.1002/bem.2250160304 10.1039/B610698F 10.1111/j.1151-2916.1995.tb08434.x 10.5714/CL.2014.15.1.015 10.2136/sssaj2005.0067a 10.1016/j.proeng.2013.08.118 10.1016/j.jnoncrysol.2007.08.037 10.1049/ji-3a-1.1946.0188 10.1180/claymin.2012.047.1.31 10.1111/j.1151-2916.1959.tb14076.x 10.1109/27.887755 10.1111/j.1750-3841.2007.00325.x 10.3390/ma9040231 10.1063/1.363824 10.2355/isijinternational.51.1766 10.1007/s00339-003-2329-8 10.1007/s11664-012-2325-x 10.1016/j.jallcom.2010.01.068 10.1021/jf60206a032 10.1179/174328405X51758 10.1039/C4RA13334J 10.1039/C5RA18073B |
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Snippet | The commercial heating oven usually consumes the power around 2500–3000 Watt and the temperature inside the oven is still below 350 °C. If we need to increase... The subject of this research is to explore the possibility of preparation of nanocomposite material of improved thermo-mechanical and tribological properties,... |
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SubjectTerms | Amorphous materials Bentonite Butanol Ceramics Coefficient of friction Composite materials Deagglomeration Dispersion Ethanol Ethyl acetate Glass transition temperature Heat measurement Inorganic fullerenes Mechanical properties Microstructure Modulus of elasticity Nanocomposites Nanoindentation Nanostructured materials Phase transition Polyvinyl butyral Solvents Storage modulus Studies Temperature Thermal analysis Thermomechanical properties Thin films Tribology |
Title | The study of thermal interaction and microstructure of sodium silicate/bentonite composite under microwave radiation |
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