The study of thermal interaction and microstructure of sodium silicate/bentonite composite under microwave radiation

The commercial heating oven usually consumes the power around 2500–3000 Watt and the temperature inside the oven is still below 350 °C. If we need to increase a temperature above 500 °C, a special heating setup with a higher power furnace is required. However, in this work, we propose a composite ma...

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Published inMaterials chemistry and physics Vol. 184; pp. 345 - 350
Main Author Subannajui, Kittitat
Format Journal Article
LanguageEnglish
Published Lausanne Elsevier B.V 01.12.2016
Elsevier BV
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Abstract The commercial heating oven usually consumes the power around 2500–3000 Watt and the temperature inside the oven is still below 350 °C. If we need to increase a temperature above 500 °C, a special heating setup with a higher power furnace is required. However, in this work, we propose a composite material that interacts with 2.45 GHz 500 Watt microwave and rapidly redeems the thermal energy with the temperature around 600–900 °C. The composite amorphous material easily forms liquid ceramics phase with a high temperature output and responds to the microwave radiation better than that of the solid phase. During the heating process, phase transformation occurs. This method is very effective and can be used to drastically reduce the power consumption of any heating process. •Amorphous phase transforms to liquid phase by microwave radiation.•Pure sodium silicate and pure bentonite cannot show temperature overshoot.•Silicate-bentonite composite shows a high temperature overshoot above 700 °C.•A rapid heating crucible for the annealing application is fabricated.
AbstractList The subject of this research is to explore the possibility of preparation of nanocomposite material of improved thermo-mechanical and tribological properties, using inorganic fullerene-like tungsten disulfide nanostructures (IF-WS2) as reinforcement in poly(vinyl butyral) (PVB). This paper also reports investigation of the effects of using different solvents in preparation of PVB/IF-WS2 nanocomposite on the thermo-mechanical behavior of the resulting material. PVB was dissolved in ethanol, isopropanol, n-butanol and ethyl acetate. IF-WS2 nanoparticles were added to these PVB solutions and dispersed by different deagglomeration techniques. Samples were dried and thin films were obtained. Their microstructure and the quality of IF-WS2 dispersion and deagglomeration in PVB matrix was analyzed by scanning electron microscope (SEM). The reinforcing effect of IF-WS2 is examined by determining hardness, reduced modulus of elasticity and coefficient of friction, by nanoindentation and nanoscratch test, in terms of the different solvents applied in preparation of the samples, mode of stirring and different contents of IF-WS2. The glass transition temperature (Tg) was determined for the prepared samples using differential scanning calorimetry (DSC) and dynamic mechanical thermal analysis (DMA). Storage modulus and mechanical loss factor were observed in a defined temperature range using DMA.
The commercial heating oven usually consumes the power around 2500–3000 Watt and the temperature inside the oven is still below 350 °C. If we need to increase a temperature above 500 °C, a special heating setup with a higher power furnace is required. However, in this work, we propose a composite material that interacts with 2.45 GHz 500 Watt microwave and rapidly redeems the thermal energy with the temperature around 600–900 °C. The composite amorphous material easily forms liquid ceramics phase with a high temperature output and responds to the microwave radiation better than that of the solid phase. During the heating process, phase transformation occurs. This method is very effective and can be used to drastically reduce the power consumption of any heating process. •Amorphous phase transforms to liquid phase by microwave radiation.•Pure sodium silicate and pure bentonite cannot show temperature overshoot.•Silicate-bentonite composite shows a high temperature overshoot above 700 °C.•A rapid heating crucible for the annealing application is fabricated.
Author Subannajui, Kittitat
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CitedBy_id crossref_primary_10_1016_j_ceramint_2024_01_348
crossref_primary_10_1016_j_compositesb_2019_106909
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Snippet The commercial heating oven usually consumes the power around 2500–3000 Watt and the temperature inside the oven is still below 350 °C. If we need to increase...
The subject of this research is to explore the possibility of preparation of nanocomposite material of improved thermo-mechanical and tribological properties,...
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SubjectTerms Amorphous materials
Bentonite
Butanol
Ceramics
Coefficient of friction
Composite materials
Deagglomeration
Dispersion
Ethanol
Ethyl acetate
Glass transition temperature
Heat measurement
Inorganic fullerenes
Mechanical properties
Microstructure
Modulus of elasticity
Nanocomposites
Nanoindentation
Nanostructured materials
Phase transition
Polyvinyl butyral
Solvents
Storage modulus
Studies
Temperature
Thermal analysis
Thermomechanical properties
Thin films
Tribology
Title The study of thermal interaction and microstructure of sodium silicate/bentonite composite under microwave radiation
URI https://dx.doi.org/10.1016/j.matchemphys.2016.09.061
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