Ca-P Conversion Coating on AZ60 Magnesium Alloy for Biomedical Application
To improve the anti-corrosion behaviors of magnesium alloy in the inner environment of human body,a bioactive Ca-P coating was deposited on the AZ60 magnesium alloy by a novel simple method.The morphologies of the Ca-P coatings formed under different treatment time were studied by scanning electron...
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| Published in | Chemical research in Chinese universities Vol. 30; no. 4; pp. 543 - 548 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Heidelberg
Jilin University and The Editorial Department of Chemical Research in Chinese Universities
01.08.2014
Key Laboratory of Automobile Materials, Ministry of Education, College of Materials Science and Engineering,Jilin University, Changchun 130022, P.R.China |
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| Abstract | To improve the anti-corrosion behaviors of magnesium alloy in the inner environment of human body,a bioactive Ca-P coating was deposited on the AZ60 magnesium alloy by a novel simple method.The morphologies of the Ca-P coatings formed under different treatment time were studied by scanning electron microscopy（SEM）.The corrosion behaviors of Ca-P coating were investigated by electrochemical polarization test and electrochemical impedance spectroscopy in both 3％（mass fraction） NaCl solution and simulated body fluid（SBF）.Immersion test in SBF was performed to evaluate the corrosion rate of Ca-P coated magnesium alloy.X-Ray diffraction（XRD） analysis result shows that the coating mentioned above mainly consists of dicalcium phosphate dehydrate（CaHPO4·2H2O,DCPD） and β-tricalcium phosphate dehydrate[β-TCP,Ca3（PO4）2],which exhibits good corrosion resistance.After magnesium alloy was immersed in 1 mol/L NaOH solution at 80 ℃ for 2 h,hydroxyapatite [Ca10（PO4）6（OH）2,HA]appeared on the magnesium alloy substrate,which can further decrease the corrosion rate of AZ60 magnesium alloy in SBF. |
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| AbstractList | To improve the anti-corrosion behaviors of magnesium alloy in the inner environment of human body, a bioactive Ca-P coating was deposited on the AZ60 magnesium alloy by a novel simple method. The morphologies of the Ca-P coatings formed under different treatment time were studied by scanning electron microscopy(SEM). The corrosion behaviors of Ca-P coating were investigated by electrochemical polarization test and electrochemical impedance spectroscopy in both 3%(mass fraction) NaCl solution and simulated body fluid(SBF). Immersion test in SBF was performed to evaluate the corrosion rate of Ca-P coated magnesium alloy. X-Ray diffraction(XRD) analysis result shows that the coating mentioned above mainly consists of dicalcium phosphate dehydrate(CaHPO
4
·2H
2
O, DCPD) and
β
-tricalcium phosphate dehydrate[
β
-TCP, Ca
3
(PO
4
)
2
], which exhibits good corrosion resistance. After magnesium alloy was immersed in 1 mol/L NaOH solution at 80 °C for 2 h, hydroxyapatite [Ca
10
(PO
4
)
6
(OH)
2
, HA] appeared on the magnesium alloy substrate, which can further decrease the corrosion rate of AZ60 magnesium alloy in SBF. To improve the anti-corrosion behaviors of magnesium alloy in the inner environment of human body,a bioactive Ca-P coating was deposited on the AZ60 magnesium alloy by a novel simple method.The morphologies of the Ca-P coatings formed under different treatment time were studied by scanning electron microscopy（SEM）.The corrosion behaviors of Ca-P coating were investigated by electrochemical polarization test and electrochemical impedance spectroscopy in both 3％（mass fraction） NaCl solution and simulated body fluid（SBF）.Immersion test in SBF was performed to evaluate the corrosion rate of Ca-P coated magnesium alloy.X-Ray diffraction（XRD） analysis result shows that the coating mentioned above mainly consists of dicalcium phosphate dehydrate（CaHPO4·2H2O,DCPD） and β-tricalcium phosphate dehydrate[β-TCP,Ca3（PO4）2],which exhibits good corrosion resistance.After magnesium alloy was immersed in 1 mol/L NaOH solution at 80 ℃ for 2 h,hydroxyapatite [Ca10（PO4）6（OH）2,HA]appeared on the magnesium alloy substrate,which can further decrease the corrosion rate of AZ60 magnesium alloy in SBF. |
| Author | CHENG Zhongji LIAN Jianshe HU Xiaoli YANG Xiaohong LI Guangyu |
| AuthorAffiliation | Key Laboratory of Automobile Materials, Ministry of Education, College of Materials Science and Engineering, Jilin University, Changchun 130022, P. R. China |
| AuthorAffiliation_xml | – name: Key Laboratory of Automobile Materials, Ministry of Education, College of Materials Science and Engineering,Jilin University, Changchun 130022, P.R.China |
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| CitedBy_id | crossref_primary_10_1016_j_surfcoat_2021_127093 crossref_primary_10_3390_ma15238676 crossref_primary_10_1016_j_ceramint_2018_09_258 crossref_primary_10_1039_C6RA19531H |
| Cites_doi | 10.1016/j.electacta.2009.07.033 10.1016/j.apsusc.2008.09.078 10.2320/matertrans.42.1317 10.1016/j.actbio.2009.12.013 10.1016/j.surfcoat.2006.03.006 10.1016/S0010-938X(98)00078-X 10.1016/j.mser.2009.05.001 10.1016/j.apsusc.2012.03.158 10.1007/BF02013247 10.1016/j.surfcoat.2008.06.035 10.1016/S0257-8972(01)01710-8 10.1016/j.actbio.2008.06.020 10.1098/rsif.2008.0151 10.1016/j.biomaterials.2006.01.017 10.1016/j.biomaterials.2010.11.017 10.1007/s40242-013-2314-5 10.1016/S1672-6529(13)60210-3 10.1016/j.actbio.2009.12.009 10.1021/cr0782574 10.1016/S0022-0728(98)00107-7 10.1016/j.biomaterials.2008.12.001 10.1016/j.msec.2010.03.016 10.1016/j.surfcoat.2004.10.119 10.1016/S0010-938X(98)00121-8 10.1016/j.biomaterials.2005.07.037 10.1016/j.biomaterials.2005.10.003 10.1002/(SICI)1527-2648(199909)1:1<11::AID-ADEM11>3.0.CO;2-N 10.1002/adem.200500013 10.1016/j.actamat.2010.09.041 10.1016/j.biomaterials.2006.12.027 10.3866/PKU.WHXB20061010 10.1007/s11998-011-9382-6 10.1149/2.036311jes 10.1016/S0142-9612(01)00180-6 10.1016/j.matlet.2008.02.048 |
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| Copyright | Jilin University, The Editorial Department of Chemical Research in Chinese Universities and Springer-Verlag GmbH 2014 Copyright © Wanfang Data Co. Ltd. All Rights Reserved. |
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| Keywords | Deposited method Corrosion rate Ca-P coating Magnesium alloy Simulated body fluid(SBF) |
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| Notes | To improve the anti-corrosion behaviors of magnesium alloy in the inner environment of human body,a bioactive Ca-P coating was deposited on the AZ60 magnesium alloy by a novel simple method.The morphologies of the Ca-P coatings formed under different treatment time were studied by scanning electron microscopy（SEM）.The corrosion behaviors of Ca-P coating were investigated by electrochemical polarization test and electrochemical impedance spectroscopy in both 3％（mass fraction） NaCl solution and simulated body fluid（SBF）.Immersion test in SBF was performed to evaluate the corrosion rate of Ca-P coated magnesium alloy.X-Ray diffraction（XRD） analysis result shows that the coating mentioned above mainly consists of dicalcium phosphate dehydrate（CaHPO4·2H2O,DCPD） and β-tricalcium phosphate dehydrate[β-TCP,Ca3（PO4）2],which exhibits good corrosion resistance.After magnesium alloy was immersed in 1 mol/L NaOH solution at 80 ℃ for 2 h,hydroxyapatite [Ca10（PO4）6（OH）2,HA]appeared on the magnesium alloy substrate,which can further decrease the corrosion rate of AZ60 magnesium alloy in SBF. 22-1183/06 Ca-P coating; Deposited method; Magnesium alloy; Corrosion rate; Simulated body fluid（SBF） |
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| PublicationYear | 2014 |
| Publisher | Jilin University and The Editorial Department of Chemical Research in Chinese Universities Key Laboratory of Automobile Materials, Ministry of Education, College of Materials Science and Engineering,Jilin University, Changchun 130022, P.R.China |
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| Snippet | To improve the anti-corrosion behaviors of magnesium alloy in the inner environment of human body,a bioactive Ca-P coating was deposited on the AZ60 magnesium... To improve the anti-corrosion behaviors of magnesium alloy in the inner environment of human body, a bioactive Ca-P coating was deposited on the AZ60 magnesium... |
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| SubjectTerms | Analytical Chemistry Chemistry Chemistry and Materials Science Chemistry/Food Science Inorganic Chemistry NaCl溶液 Organic Chemistry Physical Chemistry 二水磷酸氢钙 涂层沉积 生物医学应用 生物活性钙 电化学阻抗谱 转化膜 镁合金 |
| Title | Ca-P Conversion Coating on AZ60 Magnesium Alloy for Biomedical Application |
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