Solid-phase combustion synthesis of calcium aluminate with CaAl2O4 nanofiber structures
Calcium aluminate with CaAl2O4 (CA) nanofiber structures was fabricated through a facile solid-phase combustion synthesis method with raw materials of CaO2, CaCO3, Al, and Al2O3 in Ar atomosphere at a pressure of 0.1MPa. The results indicated that the relative content of CA decreased, but that of Ca...
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| Published in | Ceramics international Vol. 44; no. 6; pp. 6186 - 6191 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
15.04.2018
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| Abstract | Calcium aluminate with CaAl2O4 (CA) nanofiber structures was fabricated through a facile solid-phase combustion synthesis method with raw materials of CaO2, CaCO3, Al, and Al2O3 in Ar atomosphere at a pressure of 0.1MPa. The results indicated that the relative content of CA decreased, but that of Ca12Al14O33 (C12A7) increased with the increase of r-value from 0 to 0.5 (r is molar substitution coefficient of CaCO3 for CaO2). Interestingly, CA nanofibers with tens of micrometers in length and about 200nm in diameter were observed in the combustion products with r = 0.2, 0.3, 0.4, respectively. The more nanofibers can be found in the products, as the content of CaCO3 in raw material ratios increased. And the yield of nanofibers in the combustion product with r = 0.4 is the highest. The typical round droplet on head of nanofiber indicated that the growth process of nanofibers was governed by vapor-liquid-solid (VLS) mechanism with base growth mode. It is proposed that both higher reaction temperature and reducing atmosphere are requirements for the growth of CA nanofiber during the process of combustion synthesis. The nanofiber cannot be generated in the samples r0, and r5, because the gaseous Ca is absent due to oxidizing atmosphere and lower reaction temperature, respectively. |
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| AbstractList | Calcium aluminate with CaAl2O4 (CA) nanofiber structures was fabricated through a facile solid-phase combustion synthesis method with raw materials of CaO2, CaCO3, Al, and Al2O3 in Ar atomosphere at a pressure of 0.1MPa. The results indicated that the relative content of CA decreased, but that of Ca12Al14O33 (C12A7) increased with the increase of r-value from 0 to 0.5 (r is molar substitution coefficient of CaCO3 for CaO2). Interestingly, CA nanofibers with tens of micrometers in length and about 200nm in diameter were observed in the combustion products with r = 0.2, 0.3, 0.4, respectively. The more nanofibers can be found in the products, as the content of CaCO3 in raw material ratios increased. And the yield of nanofibers in the combustion product with r = 0.4 is the highest. The typical round droplet on head of nanofiber indicated that the growth process of nanofibers was governed by vapor-liquid-solid (VLS) mechanism with base growth mode. It is proposed that both higher reaction temperature and reducing atmosphere are requirements for the growth of CA nanofiber during the process of combustion synthesis. The nanofiber cannot be generated in the samples r0, and r5, because the gaseous Ca is absent due to oxidizing atmosphere and lower reaction temperature, respectively. |
| Author | Lv, Lihua Yang, Pan Gao, Jianying Ren, Yun Yang, Shoulei Xiao, Guoqing Ding, Donghai |
| Author_xml | – sequence: 1 givenname: Shoulei surname: Yang fullname: Yang, Shoulei organization: College of Materials and Mineral Resources, Xi′an University of Architecture and Technology, Xi′an 710055, China – sequence: 2 givenname: Guoqing surname: Xiao fullname: Xiao, Guoqing organization: College of Materials and Mineral Resources, Xi′an University of Architecture and Technology, Xi′an 710055, China – sequence: 3 givenname: Donghai surname: Ding fullname: Ding, Donghai email: dingdongxauat@163.com organization: College of Materials and Mineral Resources, Xi′an University of Architecture and Technology, Xi′an 710055, China – sequence: 4 givenname: Yun surname: Ren fullname: Ren, Yun organization: College of Materials and Mineral Resources, Xi′an University of Architecture and Technology, Xi′an 710055, China – sequence: 5 givenname: Lihua surname: Lv fullname: Lv, Lihua organization: College of Materials and Mineral Resources, Xi′an University of Architecture and Technology, Xi′an 710055, China – sequence: 6 givenname: Pan surname: Yang fullname: Yang, Pan organization: College of Materials and Mineral Resources, Xi′an University of Architecture and Technology, Xi′an 710055, China – sequence: 7 givenname: Jianying surname: Gao fullname: Gao, Jianying organization: College of Materials and Mineral Resources, Xi′an University of Architecture and Technology, Xi′an 710055, China |
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| Title | Solid-phase combustion synthesis of calcium aluminate with CaAl2O4 nanofiber structures |
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