Three-dimensionally ordered macroporous La0.6Sr0.4MnO3 with high surface areas: Active catalysts for the combustion of methane
Rhombohedrally crystallized3DOM La0.6Sr0.4MnO3 (LSMO) catalysts with a high surface area of 32–42m2/g were prepared by the PMMA-templating method. The 3DOM LSMO-DP3 catalyst derived with 3.0mL of dimethoxytetraethylene glycol and 5.0mL of polyethylene glycol shows excellent activity for the combusti...
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| Published in | Journal of catalysis Vol. 307; pp. 327 - 339 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier Inc
01.11.2013
Elsevier Elsevier BV |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Rhombohedrally crystallized3DOM La0.6Sr0.4MnO3 (LSMO) catalysts with a high surface area of 32–42m2/g were prepared by the PMMA-templating method. The 3DOM LSMO-DP3 catalyst derived with 3.0mL of dimethoxytetraethylene glycol and 5.0mL of polyethylene glycol shows excellent activity for the combustion of methane. [Display omitted]
•High-surface-area 3DOM La0.6Sr0.4MnO3 is prepared by the PMMA-templating method.•Surfactant addition is critical in 3DOM structure formation with nanovoid-like walls.•The calcination procedure is a key step in the formation of 3DOM structure.•3DOM La0.6Sr0.4MnO3-DP3 performs best in the combustion of methane.•Surface area, Oads, and reducibility determine the activity of 3DOM La0.6Sr0.4MnO3.
Three-dimensionally ordered macroporous rhombohedral La0.6Sr0.4MnO3 (3DOM LSMO) with nanovoids was prepared using polymethyl methacrylate (PMMA) microspheres as a hard template and dimethoxytetraethylene glycol (DMOTEG), ethylene glycol, polyethylene glycol (PEG400), l-lysine, or triblock copolymer (Pluronic P123) as a surfactant. Physicochemical properties of the materials were characterized by a number of analytical techniques, and their catalytic activities for the combustion of methane were evaluated. It is shown that the morphology of the sample depended strongly on the nature of the surfactant added during the fabrication process. The macropore sizes and surface areas of the 3DOM LSMO materials were 165–214nm and 32–40m2/g, respectively. It is found that addition of appropriate amounts of DMOTEG and PEG400 was beneficial for the generation of high-quality 3DOM-structured La0.6Sr0.4MnO3 (denoted as LSMO-DP1, LSMO-DP3, LSMO-DP5, derived with a DMOTEG /PEG400 ratio of 0.2, 0.6, and 1.0, respectively). The LSMO-DP3 catalyst derived with 3.0mL of DMOTEG and 5.0mL of PEG400 possessed the highest oxygen species concentration and surface area and best low-temperature reducibility, and hence exhibited a good catalytic activity (T10%=437°C, T50%=566°C, andT90%=661°C at GHSV=30,000mL/(gh)) for methane combustion. The apparent activation energies of the 3DOM LSMO samples were estimated to be 56.5–75.2kJ/mol, with the LSMO-DP3 sample showing the lowest apparent activation energy (56.6kJ/mol). |
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| AbstractList | Rhombohedrally crystallized3DOM La0.6Sr0.4MnO3 (LSMO) catalysts with a high surface area of 32–42m2/g were prepared by the PMMA-templating method. The 3DOM LSMO-DP3 catalyst derived with 3.0mL of dimethoxytetraethylene glycol and 5.0mL of polyethylene glycol shows excellent activity for the combustion of methane. [Display omitted]
•High-surface-area 3DOM La0.6Sr0.4MnO3 is prepared by the PMMA-templating method.•Surfactant addition is critical in 3DOM structure formation with nanovoid-like walls.•The calcination procedure is a key step in the formation of 3DOM structure.•3DOM La0.6Sr0.4MnO3-DP3 performs best in the combustion of methane.•Surface area, Oads, and reducibility determine the activity of 3DOM La0.6Sr0.4MnO3.
Three-dimensionally ordered macroporous rhombohedral La0.6Sr0.4MnO3 (3DOM LSMO) with nanovoids was prepared using polymethyl methacrylate (PMMA) microspheres as a hard template and dimethoxytetraethylene glycol (DMOTEG), ethylene glycol, polyethylene glycol (PEG400), l-lysine, or triblock copolymer (Pluronic P123) as a surfactant. Physicochemical properties of the materials were characterized by a number of analytical techniques, and their catalytic activities for the combustion of methane were evaluated. It is shown that the morphology of the sample depended strongly on the nature of the surfactant added during the fabrication process. The macropore sizes and surface areas of the 3DOM LSMO materials were 165–214nm and 32–40m2/g, respectively. It is found that addition of appropriate amounts of DMOTEG and PEG400 was beneficial for the generation of high-quality 3DOM-structured La0.6Sr0.4MnO3 (denoted as LSMO-DP1, LSMO-DP3, LSMO-DP5, derived with a DMOTEG /PEG400 ratio of 0.2, 0.6, and 1.0, respectively). The LSMO-DP3 catalyst derived with 3.0mL of DMOTEG and 5.0mL of PEG400 possessed the highest oxygen species concentration and surface area and best low-temperature reducibility, and hence exhibited a good catalytic activity (T10%=437°C, T50%=566°C, andT90%=661°C at GHSV=30,000mL/(gh)) for methane combustion. The apparent activation energies of the 3DOM LSMO samples were estimated to be 56.5–75.2kJ/mol, with the LSMO-DP3 sample showing the lowest apparent activation energy (56.6kJ/mol). Three-dimensionally ordered macroporous rhombohedral La₀.₆Sr₀.₄MnO₃ (3DOM LSMO) with nanovoids was prepared using polymethyl methacrylate (PMMA) microspheres as a hard template and dimethoxytetraethylene glycol (DMOTEG), ethylene glycol, polyethylene glycol (PEG400), l-lysine, or triblock copolymer (Pluronic P123) as a surfactant. Physicochemical properties of the materials were characterized by a number of analytical techniques, and their catalytic activities for the combustion of methane were evaluated. It is shown that the morphology of the sample depended strongly on the nature of the surfactant added during the fabrication process. The macropore sizes and surface areas of the 3DOM LSMO materials were 165–214nm and 32–40m²/g, respectively. It is found that addition of appropriate amounts of DMOTEG and PEG400 was beneficial for the generation of high-quality 3DOM-structured La₀.₆Sr₀.₄MnO₃ (denoted as LSMO-DP1, LSMO-DP3, LSMO-DP5, derived with a DMOTEG /PEG400 ratio of 0.2, 0.6, and 1.0, respectively). The LSMO-DP3 catalyst derived with 3.0mL of DMOTEG and 5.0mL of PEG400 possessed the highest oxygen species concentration and surface area and best low-temperature reducibility, and hence exhibited a good catalytic activity (T₁₀%=437°C, T₅₀%=566°C, andT₉₀%=661°C at GHSV=30,000mL/(gh)) for methane combustion. The apparent activation energies of the 3DOM LSMO samples were estimated to be 56.5–75.2kJ/mol, with the LSMO-DP3 sample showing the lowest apparent activation energy (56.6kJ/mol). Graphical abstract Rhombohedrally crystallized3DOM La0.6 Sr0.4 MnO3 (LSMO) catalysts with a high surface area of 32-42m2 /g were prepared by the PMMA-templating method. The 3DOM LSMO-DP3 catalyst derived with 3.0mL of dimethoxytetraethylene glycol and 5.0mL of polyethylene glycol shows excellent activity for the combustion of methane. Display Omitted Three-dimensionally ordered macroporous rhombohedral La0.6 Sr0.4 MnO3 (3DOM LSMO) with nanovoids was prepared using polymethyl methacrylate (PMMA) microspheres as a hard template and dimethoxytetraethylene glycol (DMOTEG), ethylene glycol, polyethylene glycol (PEG400), l-lysine, or triblock copolymer (Pluronic P123) as a surfactant. Physicochemical properties of the materials were characterized by a number of analytical techniques, and their catalytic activities for the combustion of methane were evaluated. It is shown that the morphology of the sample depended strongly on the nature of the surfactant added during the fabrication process. The macropore sizes and surface areas of the 3DOM LSMO materials were 165-214nm and 32-40m2 /g, respectively. It is found that addition of appropriate amounts of DMOTEG and PEG400 was beneficial for the generation of high-quality 3DOM-structured La0.6 Sr0.4 MnO3 (denoted as LSMO-DP1, LSMO-DP3, LSMO-DP5, derived with a DMOTEG /PEG400 ratio of 0.2, 0.6, and 1.0, respectively). The LSMO-DP3 catalyst derived with 3.0mL of DMOTEG and 5.0mL of PEG400 possessed the highest oxygen species concentration and surface area and best low-temperature reducibility, and hence exhibited a good catalytic activity (T 10% =437°C, T 50% =566°C, and T 90% =661°C at GHSV=30,000mL/(gh)) for methane combustion. The apparent activation energies of the 3DOM LSMO samples were estimated to be 56.5-75.2kJ/mol, with the LSMO-DP3 sample showing the lowest apparent activation energy (56.6kJ/mol). [PUBLICATION ABSTRACT] |
| Author | Xie, Shaohua Dai, Hongxing Deng, Jiguang Li, Junhua Arandiyan, Hamidreza Bai, Bingyang Wang, Yuan Liu, Yuxi Li, Xinwei |
| Author_xml | – sequence: 1 givenname: Hamidreza surname: Arandiyan fullname: Arandiyan, Hamidreza organization: State Key Joint Laboratory of Environment Simulation and Pollution Control (SKLESPC), School of Environment, Tsinghua University, Beijing 100084, People’s Republic of China – sequence: 2 givenname: Hongxing surname: Dai fullname: Dai, Hongxing email: hxdai@bjut.edu.cn organization: Laboratory of Catalysis Chemistry and Nanoscience, Department of Chemistry and Chemical Engineering, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100124, People’s Republic of China – sequence: 3 givenname: Jiguang surname: Deng fullname: Deng, Jiguang organization: Laboratory of Catalysis Chemistry and Nanoscience, Department of Chemistry and Chemical Engineering, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100124, People’s Republic of China – sequence: 4 givenname: Yuxi surname: Liu fullname: Liu, Yuxi organization: Laboratory of Catalysis Chemistry and Nanoscience, Department of Chemistry and Chemical Engineering, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100124, People’s Republic of China – sequence: 5 givenname: Bingyang surname: Bai fullname: Bai, Bingyang organization: State Key Joint Laboratory of Environment Simulation and Pollution Control (SKLESPC), School of Environment, Tsinghua University, Beijing 100084, People’s Republic of China – sequence: 6 givenname: Yuan surname: Wang fullname: Wang, Yuan organization: Laboratory of Catalysis Chemistry and Nanoscience, Department of Chemistry and Chemical Engineering, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100124, People’s Republic of China – sequence: 7 givenname: Xinwei surname: Li fullname: Li, Xinwei organization: Laboratory of Catalysis Chemistry and Nanoscience, Department of Chemistry and Chemical Engineering, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100124, People’s Republic of China – sequence: 8 givenname: Shaohua surname: Xie fullname: Xie, Shaohua organization: Laboratory of Catalysis Chemistry and Nanoscience, Department of Chemistry and Chemical Engineering, College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100124, People’s Republic of China – sequence: 9 givenname: Junhua surname: Li fullname: Li, Junhua email: lijunhua@tsinghua.edu.cn organization: State Key Joint Laboratory of Environment Simulation and Pollution Control (SKLESPC), School of Environment, Tsinghua University, Beijing 100084, People’s Republic of China |
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| Keywords | Low-temperature reducibility Polymethyl methacrylate-templating preparation Surfactant-mediated fabrication Methane combustion Three-dimensionally ordered macroporous La0.6Sr0.4MnO3 Methane Reducibility Lanthanum Oxides Methyl methacrylate polymer Combustion Surfactant Porous material Three-dimensionally ordered macroporous Template La Low temperature Transition element compounds MnO Heterogeneous catalysis Quaternary compound Preparation Manganese Oxides Surface area Strontium Oxides Catalyst Macroporosity Sr |
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| Snippet | Rhombohedrally crystallized3DOM La0.6Sr0.4MnO3 (LSMO) catalysts with a high surface area of 32–42m2/g were prepared by the PMMA-templating method. The 3DOM... Three-dimensionally ordered macroporous rhombohedral La₀.₆Sr₀.₄MnO₃ (3DOM LSMO) with nanovoids was prepared using polymethyl methacrylate (PMMA) microspheres... Graphical abstract Rhombohedrally crystallized3DOM La0.6 Sr0.4 MnO3 (LSMO) catalysts with a high surface area of 32-42m2 /g were prepared by the... |
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| SubjectTerms | activation energy analytical methods Catalysis Catalysts catalytic activity Chemical synthesis Chemistry Colloidal state and disperse state combustion composite polymers ethylene glycol Exact sciences and technology General and physical chemistry glycols Low-temperature reducibility lysine Methane Methane combustion oxygen physicochemical properties polyethylene glycol Polymethyl methacrylate-templating preparation polymethylmethacrylate Porous materials surface area Surfactant-mediated fabrication surfactants Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry Three-dimensionally ordered macroporous La0.6Sr0.4MnO3 |
| Title | Three-dimensionally ordered macroporous La0.6Sr0.4MnO3 with high surface areas: Active catalysts for the combustion of methane |
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