Synthesis and crystal structure of a highly selective colorimetric and fluorometric sensor for hydrogen sulfide
A novel Cu(II) complex chemosensor for hydrogen sulfide with azo as the colorimetric group has been synthesized. The complex and ligand crystals were obtained and the molecular structures were characterized by X‐ray diffraction and Electrospray ionization High resolution mass spectrometer (ESI‐HRMS)...
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| Published in | Luminescence (Chichester, England) Vol. 32; no. 5; pp. 765 - 771 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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England
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01.08.2017
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| Abstract | A novel Cu(II) complex chemosensor for hydrogen sulfide with azo as the colorimetric group has been synthesized. The complex and ligand crystals were obtained and the molecular structures were characterized by X‐ray diffraction and Electrospray ionization High resolution mass spectrometer (ESI‐HRMS). The photophysical and recognition properties were examined. The complex can recognize S2−, with an obvious color change from yellow to red based on a copper ion complex displacement mechanism. By contrast, no obvious changes were observed in the presence of other anions (AcO−, H2PO4−, F−, Cl−, Br− and I−). We present a simple, easily prepared, yet efficient, inorganic reaction‐based sensor for the detection of S2−. The complex should have many chemical and analytical applications in the sensing of hydrogen sulfide. |
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| AbstractList | Abstract
A novel Cu(II) complex chemosensor for hydrogen sulfide with azo as the colorimetric group has been synthesized. The complex and ligand crystals were obtained and the molecular structures were characterized by X‐ray diffraction and Electrospray ionization High resolution mass spectrometer (ESI‐HRMS). The photophysical and recognition properties were examined. The complex can recognize S
2
−
, with an obvious color change from yellow to red based on a copper ion complex displacement mechanism. By contrast, no obvious changes were observed in the presence of other anions (AcO
−
, H
2
PO
4
−
, F
−
, Cl
−
, Br
−
and I
−
). We present a simple, easily prepared, yet efficient, inorganic reaction‐based sensor for the detection of S
2
−
. The complex should have many chemical and analytical applications in the sensing of hydrogen sulfide. A novel Cu(II) complex chemosensor for hydrogen sulfide with azo as the colorimetric group has been synthesized. The complex and ligand crystals were obtained and the molecular structures were characterized by X‐ray diffraction and Electrospray ionization High resolution mass spectrometer (ESI‐HRMS). The photophysical and recognition properties were examined. The complex can recognize S2−, with an obvious color change from yellow to red based on a copper ion complex displacement mechanism. By contrast, no obvious changes were observed in the presence of other anions (AcO−, H2PO4−, F−, Cl−, Br− and I−). We present a simple, easily prepared, yet efficient, inorganic reaction‐based sensor for the detection of S2−. The complex should have many chemical and analytical applications in the sensing of hydrogen sulfide. A novel Cu(II) complex chemosensor for hydrogen sulfide with azo as the colorimetric group has been synthesized. The complex and ligand crystals were obtained and the molecular structures were characterized by X-ray diffraction and Electrospray ionization High resolution mass spectrometer (ESI-HRMS). The photophysical and recognition properties were examined. The complex can recognize S2-, with an obvious color change from yellow to red based on a copper ion complex displacement mechanism. By contrast, no obvious changes were observed in the presence of other anions (AcO-, H2PO4-, F-, Cl-, Br- and I-). We present a simple, easily prepared, yet efficient, inorganic reaction-based sensor for the detection of S2-. The complex should have many chemical and analytical applications in the sensing of hydrogen sulfide. A novel Cu(II) complex chemosensor for hydrogen sulfide with azo as the colorimetric group has been synthesized. The complex and ligand crystals were obtained and the molecular structures were characterized by X-ray diffraction and Electrospray ionization High resolution mass spectrometer (ESI-HRMS). The photophysical and recognition properties were examined. The complex can recognize S2- , with an obvious color change from yellow to red based on a copper ion complex displacement mechanism. By contrast, no obvious changes were observed in the presence of other anions (AcO- , H2 PO4- , F- , Cl- , Br- and I- ). We present a simple, easily prepared, yet efficient, inorganic reaction-based sensor for the detection of S2- . The complex should have many chemical and analytical applications in the sensing of hydrogen sulfide. A novel Cu(II) complex chemosensor for hydrogen sulfide with azo as the colorimetric group has been synthesized. The complex and ligand crystals were obtained and the molecular structures were characterized by X-ray diffraction and Electrospray ionization High resolution mass spectrometer (ESI-HRMS). The photophysical and recognition properties were examined. The complex can recognize S , with an obvious color change from yellow to red based on a copper ion complex displacement mechanism. By contrast, no obvious changes were observed in the presence of other anions (AcO , H PO , F , Cl , Br and I ). We present a simple, easily prepared, yet efficient, inorganic reaction-based sensor for the detection of S . The complex should have many chemical and analytical applications in the sensing of hydrogen sulfide. |
| Author | Chen, Yanmei Fu, Jiajia Shang, Xuefang Ren, Kui Zhang, Xueli Zhao, Peipei Zhang, Jinlian |
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| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/28026099$$D View this record in MEDLINE/PubMed |
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| CitedBy_id | crossref_primary_10_1016_j_microc_2023_109035 crossref_primary_10_1021_acs_analchem_9b04990 crossref_primary_10_1039_C7OB02881D crossref_primary_10_1016_j_talanta_2019_04_067 crossref_primary_10_1021_acs_chemrev_3c00683 crossref_primary_10_1002_bio_4097 crossref_primary_10_1080_10610278_2019_1590573 crossref_primary_10_1016_j_jece_2022_109150 crossref_primary_10_1021_acsomega_3c08573 |
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Neurochem. contributor: fullname: Abe K. |
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| Snippet | A novel Cu(II) complex chemosensor for hydrogen sulfide with azo as the colorimetric group has been synthesized. The complex and ligand crystals were obtained... Abstract A novel Cu(II) complex chemosensor for hydrogen sulfide with azo as the colorimetric group has been synthesized. The complex and ligand crystals were... |
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| SubjectTerms | Anions Chemical synthesis Chlorides Color colorimetric chemosensor Colorimetry Colorimetry - methods Colour Coordination Complexes - chemical synthesis Coordination Complexes - chemistry Coordination compounds Copper Copper - chemistry copper complex crystal Crystal structure Crystallography, X-Ray Crystals Detection Dimethyl Sulfoxide - chemistry Fluorescent Dyes - chemical synthesis Fluorescent Dyes - chemistry Fluorometry - methods High resolution Hydrogen Hydrogen sulfide Hydrogen Sulfide - analysis Hydrogen sulphide Ionization Ions Sensors Spectrometry, Mass, Electrospray Ionization Spectrophotometry, Ultraviolet Sulfide Sulfides - analysis Sulphides X-Ray Diffraction |
| Title | Synthesis and crystal structure of a highly selective colorimetric and fluorometric sensor for hydrogen sulfide |
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