Experimental study of cement-based materials under sulfate attack environment using Electrochemical Impedance Spectroscopy
In this paper, electrochemical impedance spectroscopy tests and compressive strength tests were employed to investigate the sulfate attack process of cement-based materials, and the change law of the electrochemical impedance spectrum with erosion time was analyzed. Based on the typical equivalent c...
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| Published in | International journal of electrochemical science Vol. 18; no. 5; p. 100133 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.05.2023
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| Subjects | |
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| Abstract | In this paper, electrochemical impedance spectroscopy tests and compressive strength tests were employed to investigate the sulfate attack process of cement-based materials, and the change law of the electrochemical impedance spectrum with erosion time was analyzed. Based on the typical equivalent circuit model of cement-based materials and its microstructure equivalent circuit model, the change law of electrochemical parameters and its relationship with compressive strength were analyzed. The experimental results indicate that with increasing erosion time, the electrochemical impedance spectrum shows significant quasi-Randles characteristics, its position moves to the right, and the diameter of the high-frequency semicircle increases. The values of RCP, reflecting disconnected pores, and RCCP, reflecting connected pores, increase continuously during the attack process. The compressive strength of cement-based materials reaches a maximum at a sulfate concentration of 55 g/L. The electrochemical parameter RCCP well reflects the compressive strength of cement-based materials and further characterizes the deterioration of its macro properties. |
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| AbstractList | In this paper, electrochemical impedance spectroscopy tests and compressive strength tests were employed to investigate the sulfate attack process of cement-based materials, and the change law of the electrochemical impedance spectrum with erosion time was analyzed. Based on the typical equivalent circuit model of cement-based materials and its microstructure equivalent circuit model, the change law of electrochemical parameters and its relationship with compressive strength were analyzed. The experimental results indicate that with increasing erosion time, the electrochemical impedance spectrum shows significant quasi-Randles characteristics, its position moves to the right, and the diameter of the high-frequency semicircle increases. The values of RCP, reflecting disconnected pores, and RCCP, reflecting connected pores, increase continuously during the attack process. The compressive strength of cement-based materials reaches a maximum at a sulfate concentration of 55 g/L. The electrochemical parameter RCCP well reflects the compressive strength of cement-based materials and further characterizes the deterioration of its macro properties. |
| ArticleNumber | 100133 |
| Author | Chen, Zhiwei Li, Jindu Chen, MengTing Niu, Shiwei Luo, Jin Wang, Xingyi Bai, Xiangling |
| Author_xml | – sequence: 1 givenname: Shiwei surname: Niu fullname: Niu, Shiwei organization: Yellow River Engineering Consulting Co., Ltd., Zhengzhou 450003, China – sequence: 2 givenname: Jin surname: Luo fullname: Luo, Jin organization: College of Geosciences and Engineering, North China University of Water Resources and Electric Power, Zhengzhou 450003, China – sequence: 3 givenname: MengTing surname: Chen fullname: Chen, MengTing organization: College of Geosciences and Engineering, North China University of Water Resources and Electric Power, Zhengzhou 450003, China – sequence: 4 givenname: Zhiwei surname: Chen fullname: Chen, Zhiwei organization: School of Civil Engineering, Southeast University, Nanjing 210096, China – sequence: 5 givenname: Xingyi surname: Wang fullname: Wang, Xingyi organization: College of Civil Engineering, Taiyuan University of Technology, Taiyuan 030024, China – sequence: 6 givenname: Xiangling surname: Bai fullname: Bai, Xiangling organization: College of Civil Engineering, Taiyuan University of Technology, Taiyuan 030024, China – sequence: 7 givenname: Jindu surname: Li fullname: Li, Jindu email: Lijindu98@163.com organization: Yellow River Engineering Consulting Co., Ltd., Zhengzhou 450003, China |
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| CitedBy_id | crossref_primary_10_1016_j_ijoes_2024_100640 crossref_primary_10_3390_min14010092 crossref_primary_10_1016_j_jobe_2024_110287 crossref_primary_10_1016_j_matpr_2024_02_038 crossref_primary_10_1016_j_jobe_2024_109181 |
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| Issue | 5 |
| Keywords | Cement-based material Compressive strength Sulfate attack Microstructure Electrochemical impedance spectroscopy |
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| SubjectTerms | Cement-based material Compressive strength Electrochemical impedance spectroscopy Microstructure Sulfate attack |
| Title | Experimental study of cement-based materials under sulfate attack environment using Electrochemical Impedance Spectroscopy |
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