THERMALLY STABLE POLYMERS BASED ON 1,3,4-OXADIAZOLE RINGS
In the present work, new thermally stable polymers containing 1,3,4-oxadiazole units have been synthesized through Huisgen reaction of the aromatic bis-tetrazole compounds with the aromatic/aliphatic bis-acid chlorides in pyridine as solvent. The obtained polymers are insoluble or slightly soluble i...
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| Published in | Chinese journal of polymer science Vol. 28; no. 1; pp. 21 - 28 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Heidelberg
Chinese Chemical Society and Institute of Chemistry, CAS
2010
Department of Applied Chemistry,College of Science,University of Mohaghegh Ardabili, Ardabil,Iran,56199-11367 |
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| Abstract | In the present work, new thermally stable polymers containing 1,3,4-oxadiazole units have been synthesized through Huisgen reaction of the aromatic bis-tetrazole compounds with the aromatic/aliphatic bis-acid chlorides in pyridine as solvent. The obtained polymers are insoluble or slightly soluble in polar aprotic solvents such as DMSO and DMF. Thermal analyses of the polymers using DSC and TGA techniques showed that the polymers had improved thermal stabilities. The model reaction was also investigated and the resulting bis-1,3,4-oxadiazole compounds were characterized by conventional spectroscopic methods. |
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| AbstractList | In the present work, new thermally stable polymers containing 1,3,4-oxadiazole units have been synthesized through Huisgen reaction of the aromatic bis-tetrazole compounds with the aromatic/aliphatic bis-acid chlorides in pyridine as solvent. The obtained polymers are insoluble or slightly soluble in polar aprotic solvents such as DMSO and DMF. Thermal analyses of the polymers using DSC and TGA techniques showed that the polymers had improved thermal stabilities. The model reaction was also investigated and the resulting bis-1,3,4-oxadiazole compounds were characterized by conventional spectroscopic methods. O6; In the present work,new thermally stable polymers containing 1,3,4-oxadiazole units have been synthesized through Huisgen reaction of the aromatic bis-tetrazole compounds with the aromatic/aliphatic bis-acid chlorides in pyridine as solvent.The obtained polymers are insoluble or slightly soluble in polar aprotic solvents such as DMSO and DMF.Thermal analyses of the polymers using DSC and TGA techniques showed that the polymers had improved thermal Stabilities.The model reaction was also investigated and the resulting bis-1,3,4-oxadiazole compounds were characterized by conventional spectroscopic methods. |
| Author | Yagoub Mansoori Raana Sarvari |
| AuthorAffiliation | Mohammad Reza Zamanloo and Gholam Hassan Imanzadeh Department of Applied Chemistry, College of Science, University of Mohaghegh Ardabili, Ardabil, Iran, 56199-11367 |
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| Cites_doi | 10.1557/PROC-558-433 10.1134/S1070428009010229 10.1002/macp.200350066 10.1021/cm000794g 10.1002/pola.20975 10.1021/ma011093n 10.1016/j.polymer.2005.05.074 10.1016/S0014-3057(02)00295-1 10.1002/app.20601 10.1002/pola.1204 10.1002/pola.10187 10.1002/1521-4095(200106)13:11<810::AID-ADMA810>3.0.CO;2-C 10.1016/S0379-6779(00)01320-5 10.3184/030823400103168010 10.1002/macp.1961.020440132 10.1038/347539a0 10.1023/A:1013947228772 10.1002/adma.200400963 10.1002/1521-3935(20011201)202:18<3579::AID-MACP3579>3.0.CO;2-O 10.1002/app.20201 10.1002/masy.200450868 10.1016/S0143-7208(02)00028-1 |
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| Keywords | Bis-tetrazole Thermally stable polymers 1,3,4-Oxadiazole Huisgen reaction |
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| Notes | 1,3,4-Oxadiazole; Thermally stable polymers; Bis-tetrazole; Huisgen reaction. TE357.46 Bis-tetrazole TQ453.22 1,3,4-Oxadiazole Thermally stable polymers Huisgen reaction. 11-2015/O6 |
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| Snippet | In the present work, new thermally stable polymers containing 1,3,4-oxadiazole units have been synthesized through Huisgen reaction of the aromatic... O6; In the present work,new thermally stable polymers containing 1,3,4-oxadiazole units have been synthesized through Huisgen reaction of the aromatic... |
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| Title | THERMALLY STABLE POLYMERS BASED ON 1,3,4-OXADIAZOLE RINGS |
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