Allylation Reactions of Aromatic Aldehydes with Antimony in Aqueous Media Under Ultrasonic Irradiation

The allylation reactions of aromatic aldehydes with allyl bromide were carried out in 89-98% yield with Sb-H 2 O-KF-CH 3 OH under ultrasound irradiation at rt for 2.5 h. The reactions in the same system gave allylic alcohols in 30-69% yield with stirring for 24 h. The main advantages of the present...

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Published inSynthetic communications Vol. 39; no. 13; pp. 2370 - 2377
Main Authors Bian, Yan-Jiang, Zhao, Hong-Mei, Yu, Xu-Guang
Format Journal Article
LanguageEnglish
Published PHILADELPHIA Taylor & Francis Group 09.06.2009
Taylor & Francis
Subjects
Allylation
antimony
Chemistry
Chemistry, Organic
Physical Sciences
Science & Technology
ultrasound irradiation
ORGANIC-SYNTHESIS
antimony
ARYL ALDEHYDES
ORGANOMETALLIC REACTIONS
ultrasound irradiation
CATALYST
CHEMOSELECTIVE ALLYLATION
Allylation
CARBON BOND FORMATION
MAGNESIUM
MANGANESE
BARBIER REACTION
WATER
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Abstract The allylation reactions of aromatic aldehydes with allyl bromide were carried out in 89-98% yield with Sb-H 2 O-KF-CH 3 OH under ultrasound irradiation at rt for 2.5 h. The reactions in the same system gave allylic alcohols in 30-69% yield with stirring for 24 h. The main advantages of the present procedure are shorter reaction time, better yield, and environmental friendliness.
AbstractList The allylation reactions of aromatic aldehydes with allyl bromide were carried out in 89-98% yield with Sb-H2O-KF-CH3OH under ultrasound irradiation at rt for 2.5h. The reactions in the same system gave allylic alcohols in 30-69% yield with stirring for 24h. The main advantages of the present procedure are shorter reaction time, better yield, and environmental friendliness.
The allylation reactions of aromatic aldehydes with allyl bromide were carried out in 89-98% yield with Sb-H 2 O-KF-CH 3 OH under ultrasound irradiation at rt for 2.5 h. The reactions in the same system gave allylic alcohols in 30-69% yield with stirring for 24 h. The main advantages of the present procedure are shorter reaction time, better yield, and environmental friendliness.
ArticleNumber 911867078
Author Bian, Yan-Jiang
Zhao, Hong-Mei
Yu, Xu-Guang
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  givenname: Hong-Mei
  surname: Zhao
  fullname: Zhao, Hong-Mei
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  givenname: Xu-Guang
  surname: Yu
  fullname: Yu, Xu-Guang
  organization: Beijing General Research Institute of Mining and Metallurgy
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10.1016/j.tetlet.2003.12.058
10.1002/cjoc.20020200804
10.1021/jo9901337
10.1016/S0040-4039(00)01961-4
10.1021/jo00274a025
10.1016/S1350-4177(96)00021-1
10.1016/S0040-4039(99)00122-7
10.1002/cjoc.20010190412
10.1021/jo951562h
10.1016/S0040-4039(02)02667-9
10.1016/S0040-4020(99)00371-3
10.1081/SCC-120002400
10.1016/S0040-4039(98)02199-6
10.1021/ol0257326
10.1002/cjoc.20040220512
10.1021/jo982497p
10.1021/om00160a008
10.1016/S0040-4039(02)00995-4
10.1021/jo971914f
10.1081/SCC-120003606
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Issue 13
Keywords ORGANIC-SYNTHESIS
antimony
ARYL ALDEHYDES
ORGANOMETALLIC REACTIONS
ultrasound irradiation
CATALYST
CHEMOSELECTIVE ALLYLATION
Allylation
CARBON BOND FORMATION
MAGNESIUM
MANGANESE
BARBIER REACTION
WATER
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Taylor & Francis
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Snippet The allylation reactions of aromatic aldehydes with allyl bromide were carried out in 89-98% yield with Sb-H 2 O-KF-CH 3 OH under ultrasound irradiation at rt...
The allylation reactions of aromatic aldehydes with allyl bromide were carried out in 89-98% yield with Sb-H2O-KF-CH3OH under ultrasound irradiation at rt for...
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StartPage 2370
SubjectTerms Allylation
antimony
Chemistry
Chemistry, Organic
Physical Sciences
Science & Technology
ultrasound irradiation
Title Allylation Reactions of Aromatic Aldehydes with Antimony in Aqueous Media Under Ultrasonic Irradiation
URI https://www.tandfonline.com/doi/abs/10.1080/00397910802654856
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