Role of lamellar thickening in thick lamellae formation in isotactic polypropylene when crystallizing under flow and pressure
Lamellar thickening of semicrystalline polymers is a fascinating subject in the realm of polymer physics as lamellar thickness plays a vital role in deciding the performance of polymer products. Whereas, regarding the processing of semicrystalline polymers where both the flow and pressure exist, the...
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| Published in | Polymer (Guilford) Vol. 179; p. 121641 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
28.09.2019
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| Abstract | Lamellar thickening of semicrystalline polymers is a fascinating subject in the realm of polymer physics as lamellar thickness plays a vital role in deciding the performance of polymer products. Whereas, regarding the processing of semicrystalline polymers where both the flow and pressure exist, the mystery of lamellar thickening has not been revealed yet. Here, the lamellar thickening of isotactic polypropylene (iPP) crystallizing under flow (30 s−1) and pressure (100 MPa) is studied by using a custom pressuring and shearing device (PSD). IPP crystallizing under flow and pressure has manifested a large lamellar thickening rate, where the lamellar thickness increases from 24 to 31 nm within a very short period of time (3000 s). The increased portion of lamellar thickness (7 nm) is more than one quarter of the original lamellae. The fast lamellar thickening behavior of iPP is shown to be occurred only under the coexistence of flow and pressure. Conversely, the lamellar thicknesses for both the iPP crystallized under the sole effect of flow (7.0 nm) and pressure (7.5 nm) remain unchanged within the same period of time. Furthermore, the activation energy of lamellar thickening for iPP crystallizing under flow and pressure is 180.1 kJ/mol, substantially below that for iPP quiescently crystallizing at atmosphere pressure (460.7 kJ/mol). The fast lamellar thickening behavior for iPP crystallizing under flow and pressure is shown to be related with the flow-induced oriented α-parent lamellae, which are composed by regularly arranged polymer chains and have a low energy barrier for molecular chains translating along the chain axis. The current study pioneers the probing into lamellar thickening of iPP crystallizing under the coexistence of flow and pressure, and suggests a promising method to fabricate high performance polymer products with thick lamellae.
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•Flow and pressure jointly induced α-form thick lamellae in iPP.•Lamellar thickening played a key role in the formation of α-form thick lamellae.•iPP crystallization under flow and pressure showed a fast lamellar thickening. |
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| AbstractList | Lamellar thickening of semicrystalline polymers is a fascinating subject in the realm of polymer physics as lamellar thickness plays a vital role in deciding the performance of polymer products. Whereas, regarding the processing of semicrystalline polymers where both the flow and pressure exist, the mystery of lamellar thickening has not been revealed yet. Here, the lamellar thickening of isotactic polypropylene (iPP) crystallizing under flow (30 s−1) and pressure (100 MPa) is studied by using a custom pressuring and shearing device (PSD). IPP crystallizing under flow and pressure has manifested a large lamellar thickening rate, where the lamellar thickness increases from 24 to 31 nm within a very short period of time (3000 s). The increased portion of lamellar thickness (7 nm) is more than one quarter of the original lamellae. The fast lamellar thickening behavior of iPP is shown to be occurred only under the coexistence of flow and pressure. Conversely, the lamellar thicknesses for both the iPP crystallized under the sole effect of flow (7.0 nm) and pressure (7.5 nm) remain unchanged within the same period of time. Furthermore, the activation energy of lamellar thickening for iPP crystallizing under flow and pressure is 180.1 kJ/mol, substantially below that for iPP quiescently crystallizing at atmosphere pressure (460.7 kJ/mol). The fast lamellar thickening behavior for iPP crystallizing under flow and pressure is shown to be related with the flow-induced oriented α-parent lamellae, which are composed by regularly arranged polymer chains and have a low energy barrier for molecular chains translating along the chain axis. The current study pioneers the probing into lamellar thickening of iPP crystallizing under the coexistence of flow and pressure, and suggests a promising method to fabricate high performance polymer products with thick lamellae.
[Display omitted]
•Flow and pressure jointly induced α-form thick lamellae in iPP.•Lamellar thickening played a key role in the formation of α-form thick lamellae.•iPP crystallization under flow and pressure showed a fast lamellar thickening. |
| ArticleNumber | 121641 |
| Author | Lei, Jun Yang, Shu-Gui Li, Zhong-Ming Xu, Jia-Zhuang Zhong, Gan-Ji |
| Author_xml | – sequence: 1 givenname: Shu-Gui surname: Yang fullname: Yang, Shu-Gui – sequence: 2 givenname: Jun orcidid: 0000-0001-6803-5216 surname: Lei fullname: Lei, Jun email: leijun@scu.edu.cn – sequence: 3 givenname: Gan-Ji orcidid: 0000-0002-8540-7293 surname: Zhong fullname: Zhong, Gan-Ji – sequence: 4 givenname: Jia-Zhuang orcidid: 0000-0001-9888-7014 surname: Xu fullname: Xu, Jia-Zhuang – sequence: 5 givenname: Zhong-Ming surname: Li fullname: Li, Zhong-Ming email: zmli@scu.edu.cn |
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| CitedBy_id | crossref_primary_10_1016_j_compscitech_2024_110961 crossref_primary_10_1016_j_ijimpeng_2023_104634 crossref_primary_10_1016_j_compscitech_2022_109285 crossref_primary_10_1016_j_polymer_2021_123565 crossref_primary_10_1016_j_ijmecsci_2024_109622 crossref_primary_10_1016_j_polymer_2024_127912 crossref_primary_10_1016_j_chemosphere_2025_144151 crossref_primary_10_1002_adsu_202400711 crossref_primary_10_1016_j_polymer_2025_128122 crossref_primary_10_1016_j_ijfatigue_2024_108517 crossref_primary_10_1021_acs_macromol_3c01846 crossref_primary_10_3390_polym14214745 crossref_primary_10_1016_j_cej_2022_136205 crossref_primary_10_1016_j_tca_2025_179948 crossref_primary_10_1007_s10118_022_2672_x crossref_primary_10_1016_j_addma_2024_104188 |
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| Title | Role of lamellar thickening in thick lamellae formation in isotactic polypropylene when crystallizing under flow and pressure |
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