Evaluation of modified silica nanoparticles in carboxylated nitrile rubber nanocomposites
•We modified silica nanoparticles with a silane agent and with a polymeric shell.•SiO2 nanoparticles induced arrangements in XNBR nanocomposites.•The SDS induced the polymeric macromolecules organization in the nanocomposites.•The silica nanoparticles dispersed in the polymer forming a mass fractal...
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| Published in | Colloids and surfaces. A, Physicochemical and engineering aspects Vol. 462; pp. 45 - 51 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
20.11.2014
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| Subjects | |
| Online Access | Get full text |
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| Abstract | •We modified silica nanoparticles with a silane agent and with a polymeric shell.•SiO2 nanoparticles induced arrangements in XNBR nanocomposites.•The SDS induced the polymeric macromolecules organization in the nanocomposites.•The silica nanoparticles dispersed in the polymer forming a mass fractal system.•The silica nanoparticles and XNBR chains formed three-dimensional network.
Surface-modified silica nanoparticles have a plenty of applications, such as coatings, dyes or biomarkers, catalysts and encapsulated products. When modified with 3-(trimethoxysilyl)propyl methacrylate (SiO2-MPS) or covered with a polymeric shell obtained from a reaction between divinylbenzene and styrene (SiO2-Pol), these SiO2 nanoparticles induced distinct arrangements in polymer nanocomposites (PNC) prepared with commercial carboxylated nitrile rubber (XNBR). The hydrophilicity character of the modified SiO2 nanoparticles was also altered, improving their interaction with the XNBR macromolecules. Consequently, choosing the PNC properties for different conditions and applications became possible due to the adjustment of the nanoparticle surface characteristics. Although the final characteristics of the nanocomposites films varied according to the nanoparticle used, the PNC prepared with SiO2-Pol presented better homogeneity than those with SiO2-MPS. |
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| AbstractList | •We modified silica nanoparticles with a silane agent and with a polymeric shell.•SiO2 nanoparticles induced arrangements in XNBR nanocomposites.•The SDS induced the polymeric macromolecules organization in the nanocomposites.•The silica nanoparticles dispersed in the polymer forming a mass fractal system.•The silica nanoparticles and XNBR chains formed three-dimensional network.
Surface-modified silica nanoparticles have a plenty of applications, such as coatings, dyes or biomarkers, catalysts and encapsulated products. When modified with 3-(trimethoxysilyl)propyl methacrylate (SiO2-MPS) or covered with a polymeric shell obtained from a reaction between divinylbenzene and styrene (SiO2-Pol), these SiO2 nanoparticles induced distinct arrangements in polymer nanocomposites (PNC) prepared with commercial carboxylated nitrile rubber (XNBR). The hydrophilicity character of the modified SiO2 nanoparticles was also altered, improving their interaction with the XNBR macromolecules. Consequently, choosing the PNC properties for different conditions and applications became possible due to the adjustment of the nanoparticle surface characteristics. Although the final characteristics of the nanocomposites films varied according to the nanoparticle used, the PNC prepared with SiO2-Pol presented better homogeneity than those with SiO2-MPS. Surface-modified silica nanoparticles have a plenty of applications, such as coatings, dyes or biomarkers, catalysts and encapsulated products. When modified with 3-(trimethoxysilyl)propyl methacrylate (SiO sub(2)-MPS) or covered with a polymeric shell obtained from a reaction between divinylbenzene and styrene (SiO sub(2)-Pol), these SiO sub(2) nanoparticles induced distinct arrangements in polymer nanocomposites (PNC) prepared with commercial carboxylated nitrile rubber (XNBR). The hydrophilicity character of the modified SiO sub(2) nanoparticles was also altered, improving their interaction with the XNBR macromolecules. Consequently, choosing the PNC properties for different conditions and applications became possible due to the adjustment of the nanoparticle surface characteristics. Although the final characteristics of the nanocomposites films varied according to the nanoparticle used, the PNC prepared with SiO sub(2)-Pol presented better homogeneity than those with SiO sub(2)-MPS. |
| Author | Arantes, Tatiane M. Longo, Elson Paranhos, Caio M. Leite, Edson R. Camargo, Emerson R. Sala, Renata L. |
| Author_xml | – sequence: 1 givenname: Renata L. surname: Sala fullname: Sala, Renata L. email: renata.lang89@gmail.com organization: LIEC – Interdisciplinary Laboratory of Electrochemistry and Ceramics, Department of Chemistry, UFSCar-Federal University of São Carlos, Rod. Washington Luis km 235, CP 676, 13565-9905 São Carlos, SP, Brazil – sequence: 2 givenname: Tatiane M. surname: Arantes fullname: Arantes, Tatiane M. email: tmarantes@yahoo.com.br organization: LIEC – Interdisciplinary Laboratory of Electrochemistry and Ceramics, Department of Chemistry, UFSCar-Federal University of São Carlos, Rod. Washington Luis km 235, CP 676, 13565-9905 São Carlos, SP, Brazil – sequence: 3 givenname: Elson surname: Longo fullname: Longo, Elson email: elson@iq.unesp.br organization: LIEC – Interdisciplinary Laboratory of Electrochemistry and Ceramics, Department of Chemistry, UFSCar-Federal University of São Carlos, Rod. Washington Luis km 235, CP 676, 13565-9905 São Carlos, SP, Brazil – sequence: 4 givenname: Edson R. surname: Leite fullname: Leite, Edson R. email: edson.leite@pq.cnpq.br organization: LIEC – Interdisciplinary Laboratory of Electrochemistry and Ceramics, Department of Chemistry, UFSCar-Federal University of São Carlos, Rod. Washington Luis km 235, CP 676, 13565-9905 São Carlos, SP, Brazil – sequence: 5 givenname: Caio M. surname: Paranhos fullname: Paranhos, Caio M. email: paranhos@ufscar.br organization: Department of Chemistry, UFSCar – Federal University of São Carlos, Rod. Washington Luis km 235, CP 676, São Carlos, SP 13565-9905, Brazil – sequence: 6 givenname: Emerson R. surname: Camargo fullname: Camargo, Emerson R. email: camargo@ufscar.br organization: LIEC – Interdisciplinary Laboratory of Electrochemistry and Ceramics, Department of Chemistry, UFSCar-Federal University of São Carlos, Rod. Washington Luis km 235, CP 676, 13565-9905 São Carlos, SP, Brazil |
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| Snippet | •We modified silica nanoparticles with a silane agent and with a polymeric shell.•SiO2 nanoparticles induced arrangements in XNBR nanocomposites.•The SDS... Surface-modified silica nanoparticles have a plenty of applications, such as coatings, dyes or biomarkers, catalysts and encapsulated products. When modified... |
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| SubjectTerms | Carboxylated Colloidal route Homogeneity Macromolecules Modified surface Nanocomposites Nanoparticles Nitrile rubber Polymer nanocomposites Silica nanoparticles Silicon dioxide Styrenes |
| Title | Evaluation of modified silica nanoparticles in carboxylated nitrile rubber nanocomposites |
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