Production of jet fuel range hydrocarbons using a magnetic Ni–Fe/SAPO-11 catalyst for solvent-free hydrodeoxygenation of jatropha oil
A novel, multifunctional Nix–Fe/SAPO-11 catalyst was synthesized and characterized, and its activity was evaluated for the solvent-free hydrodeoxygenation of jatropha oil. The catalyst has a spherical structure and moderate acid strength, and exhibited excellent cyclization and deoxidation activity....
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| Published in | Biomass & bioenergy Vol. 177; p. 106927 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.10.2023
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0961-9534 1873-2909 |
| DOI | 10.1016/j.biombioe.2023.106927 |
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| Abstract | A novel, multifunctional Nix–Fe/SAPO-11 catalyst was synthesized and characterized, and its activity was evaluated for the solvent-free hydrodeoxygenation of jatropha oil. The catalyst has a spherical structure and moderate acid strength, and exhibited excellent cyclization and deoxidation activity. The inclusion of iron facilitated the dispersion of active components. Consequently, the iron-nickel alloy particle size remained small, resulting in an optimal distribution of the product. The composition of the products is linear alkanes (59.83%), isoparaffins (4.16%), aromatics (8.41%), and naphthenes (12.03%), where jet fuel components are relatively high, accounting for 55.04% of C8–C16 hydrocarbons. Interestingly, the iron present in the catalyst allowed the use of an external magnetic field for the rapid separation and recycling of the catalyst. Despite multiple uses, the recycled catalyst maintained high activity following five cycles, with hydrocarbon content consistently above 85%. The synergic effect of the metallic and acid sites of the catalyst, let to realize one-pot hydrodeoxygenation, isomerization, aromatization, and cracking of substrate forming bio-jet fuel range hydrocarbons.
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•A low-cost, easily recyclable magnetic Ni–Fe catalyst was prepared.•The presence of Fe promoted the dispersion of Ni in the catalyst.•Bio-jet fuels hydrocarbons containing naphthenes and aromatics were prepared. |
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| AbstractList | A novel, multifunctional Nix–Fe/SAPO-11 catalyst was synthesized and characterized, and its activity was evaluated for the solvent-free hydrodeoxygenation of jatropha oil. The catalyst has a spherical structure and moderate acid strength, and exhibited excellent cyclization and deoxidation activity. The inclusion of iron facilitated the dispersion of active components. Consequently, the iron-nickel alloy particle size remained small, resulting in an optimal distribution of the product. The composition of the products is linear alkanes (59.83%), isoparaffins (4.16%), aromatics (8.41%), and naphthenes (12.03%), where jet fuel components are relatively high, accounting for 55.04% of C8–C16 hydrocarbons. Interestingly, the iron present in the catalyst allowed the use of an external magnetic field for the rapid separation and recycling of the catalyst. Despite multiple uses, the recycled catalyst maintained high activity following five cycles, with hydrocarbon content consistently above 85%. The synergic effect of the metallic and acid sites of the catalyst, let to realize one-pot hydrodeoxygenation, isomerization, aromatization, and cracking of substrate forming bio-jet fuel range hydrocarbons.
[Display omitted]
•A low-cost, easily recyclable magnetic Ni–Fe catalyst was prepared.•The presence of Fe promoted the dispersion of Ni in the catalyst.•Bio-jet fuels hydrocarbons containing naphthenes and aromatics were prepared. A novel, multifunctional Nix-Fe/SAPO-11 catalyst was synthesized and characterized, and its activity was evaluated for the solvent-free hydrodeoxygenation of jatropha oil. The catalyst has a spherical structure and moderate acid strength, and exhibited excellent cyclization and deoxidation activity. The inclusion of iron facilitated the dispersion of active components. Consequently, the iron-nickel alloy particle size remained small, resulting in an optimal distribution of the product. The composition of the products is linear alkanes (59.83%), isoparaffins (4.16%), aromatics (8.41%), and naphthenes (12.03%), where jet fuel components are relatively high, accounting for 55.04% of C8-C16 hydrocarbons. Interestingly, the iron present in the catalyst allowed the use of an external magnetic field for the rapid separation and recycling of the catalyst. Despite multiple uses, the recycled catalyst maintained high activity following five cycles, with hydrocarbon content consistently above 85%. The synergic effect of the metallic and acid sites of the catalyst, let to realize one-pot hydrodeoxygenation, isomerization, aromatization, and cracking of substrate forming bio-jet fuel range hydrocarbons. |
| ArticleNumber | 106927 |
| Author | Wei, Xiaocui Cao, Yang Tang, Hongbiao Jibran, Khalil Wang, Shurong Dai, Qiqi Li, Jin |
| Author_xml | – sequence: 1 givenname: Hongbiao surname: Tang fullname: Tang, Hongbiao organization: College of Chemical Engineering and Technology, Hainan University, Haikou, 570228, China – sequence: 2 givenname: Qiqi surname: Dai fullname: Dai, Qiqi organization: College of Chemical Engineering and Technology, Hainan University, Haikou, 570228, China – sequence: 3 givenname: Yang surname: Cao fullname: Cao, Yang organization: Qiongtai Normal University, Haikou, 571127, China – sequence: 4 givenname: Jin surname: Li fullname: Li, Jin email: lijin@hainanu.edu.cn organization: College of Chemical Engineering and Technology, Hainan University, Haikou, 570228, China – sequence: 5 givenname: Xiaocui surname: Wei fullname: Wei, Xiaocui organization: College of Chemical Engineering and Technology, Hainan University, Haikou, 570228, China – sequence: 6 givenname: Khalil surname: Jibran fullname: Jibran, Khalil organization: College of Chemical Engineering and Technology, Hainan University, Haikou, 570228, China – sequence: 7 givenname: Shurong surname: Wang fullname: Wang, Shurong organization: College of Chemical Engineering and Technology, Hainan University, Haikou, 570228, China |
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| Keywords | One-pot method Ni–Fe/SAPO-11 Hydrodeoxygenation Jatropha oil Jet fuel |
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| Snippet | A novel, multifunctional Nix–Fe/SAPO-11 catalyst was synthesized and characterized, and its activity was evaluated for the solvent-free hydrodeoxygenation of... A novel, multifunctional Nix-Fe/SAPO-11 catalyst was synthesized and characterized, and its activity was evaluated for the solvent-free hydrodeoxygenation of... |
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| SourceType | Aggregation Database Enrichment Source Index Database Publisher |
| StartPage | 106927 |
| SubjectTerms | alloys aromatic compounds aromatization bioenergy biomass catalysts fuels Hydrodeoxygenation iron isomerization Jatropha oil Jet fuel magnetic fields Ni–Fe/SAPO-11 oils One-pot method particle size synergism |
| Title | Production of jet fuel range hydrocarbons using a magnetic Ni–Fe/SAPO-11 catalyst for solvent-free hydrodeoxygenation of jatropha oil |
| URI | https://dx.doi.org/10.1016/j.biombioe.2023.106927 https://www.proquest.com/docview/3153712301 |
| Volume | 177 |
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