Investigation of electrochemical copolymerisation of hydroxmethyl substituted 3,4-ethylenedioxythiophene with bithiophene

•Copolymerisation is enhanced by similar oxidation potential of monomers.•High upper potential boundary during electropolymerisation leads to overoxidation of pEDOT_OH.•Increase the upper potential boundary favours incorporation of BTh unit into the copolymer chain. The results of electrochemical co...

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Published inSynthetic metals Vol. 199; pp. 310 - 318
Main Authors Golba, Sylwia, Łężniak, Marta, Gabor, Jadwiga, Tomasz, Flak
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.01.2015
Subjects
Bands
Bithiophene
Boundaries
Chains (polymeric)
Copolymerization
Copolymers
Coupling (molecular)
EDOT functional derivatives
Electrochemical doping
Electroconductivity
MALDI TOF
Molecular conformation
Spectra
MALDI TOF
Electrochemical doping
EDOT functional derivatives
Bithiophene
Electroconductivity
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Abstract •Copolymerisation is enhanced by similar oxidation potential of monomers.•High upper potential boundary during electropolymerisation leads to overoxidation of pEDOT_OH.•Increase the upper potential boundary favours incorporation of BTh unit into the copolymer chain. The results of electrochemical copolymerisation of hydroksymethyl EDOT with bithiophene unit were presented. The obtained copolymers were characterised by FTIR ATR and MALDI TOF techniques. Successful copolymer growth was observed with a wide distribution of the polymer chain length, while increasing the upper potential boundary favours incorporation of BTh unit into the copolymer chain. The FTIR ATR spectra of the homo- and copolymers preset bands indicating α–α′ coupling of radical cations during (co) polymerization. The presence of bithiophene molecules improves stability of the forming polymer matrix. The results confirmed copolymeric layer formation which composition is dependent on the applied potential boundary.
AbstractList •Copolymerisation is enhanced by similar oxidation potential of monomers.•High upper potential boundary during electropolymerisation leads to overoxidation of pEDOT_OH.•Increase the upper potential boundary favours incorporation of BTh unit into the copolymer chain. The results of electrochemical copolymerisation of hydroksymethyl EDOT with bithiophene unit were presented. The obtained copolymers were characterised by FTIR ATR and MALDI TOF techniques. Successful copolymer growth was observed with a wide distribution of the polymer chain length, while increasing the upper potential boundary favours incorporation of BTh unit into the copolymer chain. The FTIR ATR spectra of the homo- and copolymers preset bands indicating α–α′ coupling of radical cations during (co) polymerization. The presence of bithiophene molecules improves stability of the forming polymer matrix. The results confirmed copolymeric layer formation which composition is dependent on the applied potential boundary.
The results of electrochemical copolymerisation of hydroksymethyl EDOT with bithiophene unit were presented. The obtained copolymers were characterised by FTIR ATR and MALDI TOF techniques. Successful copolymer growth was observed with a wide distribution of the polymer chain length, while increasing the upper potential boundary favours incorporation of BTh unit into the copolymer chain. The FTIR ATR spectra of the homo- and copolymers preset bands indicating alpha - alpha ' coupling of radical cations during (co) polymerization. The presence of bithiophene molecules improves stability of the forming polymer matrix. The results confirmed copolymeric layer formation which composition is dependent on the applied potential boundary.
Author Tomasz, Flak
Łężniak, Marta
Golba, Sylwia
Gabor, Jadwiga
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Electrochemical doping
EDOT functional derivatives
Bithiophene
Electroconductivity
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Snippet •Copolymerisation is enhanced by similar oxidation potential of monomers.•High upper potential boundary during electropolymerisation leads to overoxidation of...
The results of electrochemical copolymerisation of hydroksymethyl EDOT with bithiophene unit were presented. The obtained copolymers were characterised by FTIR...
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SubjectTerms Bands
Bithiophene
Boundaries
Chains (polymeric)
Copolymerization
Copolymers
Coupling (molecular)
EDOT functional derivatives
Electrochemical doping
Electroconductivity
MALDI TOF
Molecular conformation
Spectra
Title Investigation of electrochemical copolymerisation of hydroxmethyl substituted 3,4-ethylenedioxythiophene with bithiophene
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