Potential application of hydroxypropyl methylcellulose/shellac embedded with graphene oxide/TiO2-Nps as natural packaging film
Graphene oxide (GO), TiO2-NPs, HPMC, and shellac are environmentally green polymers and nanocomposites. This work aimed to create biodegradable composite films made of HPMC/shellac, HPMC/shellac-GO, and HPMC/shellac-GO/TiO2-NPs by film casting. TiO2-HPMC/shellac-GO matrix's dispersibility and m...
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| Published in | International journal of biological macromolecules Vol. 257; p. 128589 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.02.2024
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Graphene oxide (GO), TiO2-NPs, HPMC, and shellac are environmentally green polymers and nanocomposites. This work aimed to create biodegradable composite films made of HPMC/shellac, HPMC/shellac-GO, and HPMC/shellac-GO/TiO2-NPs by film casting. TiO2-HPMC/shellac-GO matrix's dispersibility and mixing ability were characterized and observed using FTIR and XRD. XRD analysis shows that the crystallinity decreased within the composites due to breaking H-bonding. Compared to HPMC/shellac, TGA/DTG demonstrated the composite films' superior thermal stability. TiO2 (0.08–0.16 %) was cast into a composite film comprising HPMC, shellac, and GO. The homogeneity of TiO2 distribution in the composite film was shown using a SEM, which was also used to display the morphology of nanocomposite films. Nanocomposite films' thickness, air permeability, tensile strength, Young's modulus, and burst strength were examined. The results demonstrated that natural films prepared by a combination of shellac/GO with HPMC enhanced the fabricating of films' properties, the tensile strength increased by 231 % (from 16 to 53 MPa) in HPMC and HPSG2 (HPMC 1.9 g/shellac 0.25 g/GO 0.125 g in 100 mL) respectively, whereas the contact angle did not change. And after addition of TiO2-NPs, there were high enhancements in HPMC films' properties, such tensile strength increased by 212 % (from 16 to 50 MPa), burst strength increased by 20.96 % (3.1 to 3.75 Kg/cm2), and the contact angle by 60.86 % (48 to 74°) in HPMC and HPSGT2 respectively. Compared to HPMC films, films exhibited the highest levels of antibacterial activity against E. coli, B. mycoides, and C. albicans. So, the composite films from HPMC/shellac/GO/TiO2-NPs are promising potential packaging materials. |
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| AbstractList | Graphene oxide (GO), TiO2-NPs, HPMC, and shellac are environmentally green polymers and nanocomposites. This work aimed to create biodegradable composite films made of HPMC/shellac, HPMC/shellac-GO, and HPMC/shellac-GO/TiO2-NPs by film casting. TiO2-HPMC/shellac-GO matrix's dispersibility and mixing ability were characterized and observed using FTIR and XRD. XRD analysis shows that the crystallinity decreased within the composites due to breaking H-bonding. Compared to HPMC/shellac, TGA/DTG demonstrated the composite films' superior thermal stability. TiO2 (0.08–0.16 %) was cast into a composite film comprising HPMC, shellac, and GO. The homogeneity of TiO2 distribution in the composite film was shown using a SEM, which was also used to display the morphology of nanocomposite films. Nanocomposite films' thickness, air permeability, tensile strength, Young's modulus, and burst strength were examined. The results demonstrated that natural films prepared by a combination of shellac/GO with HPMC enhanced the fabricating of films' properties, the tensile strength increased by 231 % (from 16 to 53 MPa) in HPMC and HPSG2 (HPMC 1.9 g/shellac 0.25 g/GO 0.125 g in 100 mL) respectively, whereas the contact angle did not change. And after addition of TiO2-NPs, there were high enhancements in HPMC films' properties, such tensile strength increased by 212 % (from 16 to 50 MPa), burst strength increased by 20.96 % (3.1 to 3.75 Kg/cm2), and the contact angle by 60.86 % (48 to 74°) in HPMC and HPSGT2 respectively. Compared to HPMC films, films exhibited the highest levels of antibacterial activity against E. coli, B. mycoides, and C. albicans. So, the composite films from HPMC/shellac/GO/TiO2-NPs are promising potential packaging materials. Graphene oxide (GO), TiO2-NPs, HPMC, and shellac are environmentally green polymers and nanocomposites. This work aimed to create biodegradable composite films made of HPMC/shellac, HPMC/shellac-GO, and HPMC/shellac-GO/TiO2-NPs by film casting. TiO2-HPMC/shellac-GO matrix's dispersibility and mixing ability were characterized and observed using FTIR and XRD. XRD analysis shows that the crystallinity decreased within the composites due to breaking H-bonding. Compared to HPMC/shellac, TGA/DTG demonstrated the composite films' superior thermal stability. TiO2 (0.08-0.16 %) was cast into a composite film comprising HPMC, shellac, and GO. The homogeneity of TiO2 distribution in the composite film was shown using a SEM, which was also used to display the morphology of nanocomposite films. Nanocomposite films' thickness, air permeability, tensile strength, Young's modulus, and burst strength were examined. The results demonstrated that natural films prepared by a combination of shellac/GO with HPMC enhanced the fabricating of films' properties, the tensile strength increased by 231 % (from 16 to 53 MPa) in HPMC and HPSG2 (HPMC 1.9 g/shellac 0.25 g/GO 0.125 g in 100 mL) respectively, whereas the contact angle did not change. And after addition of TiO2-NPs, there were high enhancements in HPMC films' properties, such tensile strength increased by 212 % (from 16 to 50 MPa), burst strength increased by 20.96 % (3.1 to 3.75 Kg/cm2), and the contact angle by 60.86 % (48 to 74°) in HPMC and HPSGT2 respectively. Compared to HPMC films, films exhibited the highest levels of antibacterial activity against E. coli, B. mycoides, and C. albicans. So, the composite films from HPMC/shellac/GO/TiO2-NPs are promising potential packaging materials. |
| ArticleNumber | 128589 |
| Author | Elsayed, Alshaimaa M. El-Sakhawy, Mohamed Kamel, Samir Tohamy, Hebat-Allah S. Mohamed, Salah A.A. |
| Author_xml | – sequence: 1 givenname: Hebat-Allah S. surname: Tohamy fullname: Tohamy, Hebat-Allah S. organization: Cellulose and Paper Department, National Research Centre, Dokki, Giza P.O. 12622, Egypt – sequence: 2 givenname: Salah A.A. surname: Mohamed fullname: Mohamed, Salah A.A. email: salahazhar1@yahoo.com organization: Packing and Packaging Materials Department, National Research Centre, 33 El Bohouth St., Dokki, Giza P.O. 12622, Egypt – sequence: 3 givenname: Mohamed surname: El-Sakhawy fullname: El-Sakhawy, Mohamed organization: Cellulose and Paper Department, National Research Centre, Dokki, Giza P.O. 12622, Egypt – sequence: 4 givenname: Alshaimaa M. surname: Elsayed fullname: Elsayed, Alshaimaa M. organization: Molecular Biology Department, Biotechnology Research Institute, National Research Centre, Dokki, Giza 12622, Egypt – sequence: 5 givenname: Samir surname: Kamel fullname: Kamel, Samir organization: Cellulose and Paper Department, National Research Centre, Dokki, Giza P.O. 12622, Egypt |
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| CitedBy_id | crossref_primary_10_1016_j_ijbiomac_2024_133131 crossref_primary_10_3390_polym16081061 crossref_primary_10_1016_j_tifs_2024_104366 crossref_primary_10_1016_j_ijbiomac_2024_132960 crossref_primary_10_1186_s13065_024_01221_3 |
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| Keywords | Hydroxypropyl methylcellulose/shellac Natural packaging film GO/TiO2-NPs New environmentally friendly biodegradable polymers |
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| SubjectTerms | GO/TiO2-NPs Hydroxypropyl methylcellulose/shellac Natural packaging film New environmentally friendly biodegradable polymers |
| Title | Potential application of hydroxypropyl methylcellulose/shellac embedded with graphene oxide/TiO2-Nps as natural packaging film |
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