Design of 2D/2D heterojunction of Ti3C2/BiOClxBr1−x for enhancing photocatalytic performance

Newly emerged 2D metallic Ti3C2 is highly spotlighted for its unique properties and ubiquitous compounding compatibility. Herein we pioneeringly demonstrate a heterojunction photocatalyst of Ti3C2/BiOClxBr1−x. X-ray diffraction, scanning electron microscope, transmission electron scope, and X-ray ph...

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Published inColloids and surfaces. A, Physicochemical and engineering aspects Vol. 663; p. 131010
Main Authors Wu, Danni, Zeng, Liya, Liu, Yuwei, Yuan, Changlai, Xue, Xiaogang, Zhang, Xiaowen
Format Journal Article
LanguageEnglish
Published Elsevier B.V 20.04.2023
Subjects
absorbance
BiOClxBr1−x
electric current
electrochemistry
electron paramagnetic resonance spectroscopy
energy
Fourier transform infrared spectroscopy
Heterojunction
nanosheets
photocatalysis
Photocatalyst
photocatalysts
photoluminescence
photolysis
RhB photodegradation
species
synergism
Ti3C2
X-ray diffraction
X-ray photoelectron spectroscopy
BiOClxBr1−x
Photocatalyst
Ti3C2
Heterojunction
RhB photodegradation
Online AccessGet full text
ISSN0927-7757
1873-4359
DOI10.1016/j.colsurfa.2023.131010

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Abstract Newly emerged 2D metallic Ti3C2 is highly spotlighted for its unique properties and ubiquitous compounding compatibility. Herein we pioneeringly demonstrate a heterojunction photocatalyst of Ti3C2/BiOClxBr1−x. X-ray diffraction, scanning electron microscope, transmission electron scope, and X-ray photoelectron spectroscopy analysis indicates that BiOClxBr1−x is successfully in-situ grown upon Ti3C2 nanosheets. Visible light photocatalytic performance of 7 %-Ti3C2/BiOCl0.25Br0.75 is overwhelmingly superior to BiOClxBr1−x with an increment of 11.9 times in the reaction rate constant of RhB photodegradation, owing to the distinctive Schottky heterojunction between Ti3C2 and BiOClxBr1−x. UV–vis absorbance, photoluminescence, Fourier transform infrared spectra, Raman, electrochemical impedance spectra, and transient photocurrent response account for the improved utilization of visible light, effective separation of photogenerated carriers, and more photogenerated electron acceptors, which elucidate the superior photocatalytic performance and good stability of Ti3C2/BiOClxBr1−x. Trapping experiments and electron paramagnetic resonance tests verify that the dominant active species of·O2- and h+ are responsible for the rapid degradation of RhB. The reasonable photocatalytic mechanism of Ti3C2/BiOClxBr1−x is clarified based on the energy band structure and synergistic effect of the heterojunction. This work provides some novel insights into designing 2D layered heterojunction photocatalysts, boosting photocatalytic performance, and advancing Ti3C2 application. [Display omitted] •2D/2D Ti3C2/BiOClxBr1-x heterojunctions were constructed via in-situ growth.•Carriers dynamics investigations suggest that Schottky junctions are formed between two materials.•Optimized heterojunction of 7 %-TB0.25 exhibits enhanced RhB degradation rate, 11.9 times higher than that of TB0.25.•The in-built electric field and band bending accelerate carriers’ separation and accumulation.
AbstractList Newly emerged 2D metallic Ti₃C₂ is highly spotlighted for its unique properties and ubiquitous compounding compatibility. Herein we pioneeringly demonstrate a heterojunction photocatalyst of Ti₃C₂/BiOClₓBr₁₋ₓ. X-ray diffraction, scanning electron microscope, transmission electron scope, and X-ray photoelectron spectroscopy analysis indicates that BiOClₓBr₁₋ₓ is successfully in-situ grown upon Ti₃C₂ nanosheets. Visible light photocatalytic performance of 7 %-Ti₃C₂/BiOCl₀.₂₅Br₀.₇₅ is overwhelmingly superior to BiOClₓBr₁₋ₓ with an increment of 11.9 times in the reaction rate constant of RhB photodegradation, owing to the distinctive Schottky heterojunction between Ti₃C₂ and BiOClₓBr₁₋ₓ. UV–vis absorbance, photoluminescence, Fourier transform infrared spectra, Raman, electrochemical impedance spectra, and transient photocurrent response account for the improved utilization of visible light, effective separation of photogenerated carriers, and more photogenerated electron acceptors, which elucidate the superior photocatalytic performance and good stability of Ti₃C₂/BiOClₓBr₁₋ₓ. Trapping experiments and electron paramagnetic resonance tests verify that the dominant active species of·O²⁻ and h⁺ are responsible for the rapid degradation of RhB. The reasonable photocatalytic mechanism of Ti₃C₂/BiOClₓBr₁₋ₓ is clarified based on the energy band structure and synergistic effect of the heterojunction. This work provides some novel insights into designing 2D layered heterojunction photocatalysts, boosting photocatalytic performance, and advancing Ti₃C₂ application.
Newly emerged 2D metallic Ti3C2 is highly spotlighted for its unique properties and ubiquitous compounding compatibility. Herein we pioneeringly demonstrate a heterojunction photocatalyst of Ti3C2/BiOClxBr1−x. X-ray diffraction, scanning electron microscope, transmission electron scope, and X-ray photoelectron spectroscopy analysis indicates that BiOClxBr1−x is successfully in-situ grown upon Ti3C2 nanosheets. Visible light photocatalytic performance of 7 %-Ti3C2/BiOCl0.25Br0.75 is overwhelmingly superior to BiOClxBr1−x with an increment of 11.9 times in the reaction rate constant of RhB photodegradation, owing to the distinctive Schottky heterojunction between Ti3C2 and BiOClxBr1−x. UV–vis absorbance, photoluminescence, Fourier transform infrared spectra, Raman, electrochemical impedance spectra, and transient photocurrent response account for the improved utilization of visible light, effective separation of photogenerated carriers, and more photogenerated electron acceptors, which elucidate the superior photocatalytic performance and good stability of Ti3C2/BiOClxBr1−x. Trapping experiments and electron paramagnetic resonance tests verify that the dominant active species of·O2- and h+ are responsible for the rapid degradation of RhB. The reasonable photocatalytic mechanism of Ti3C2/BiOClxBr1−x is clarified based on the energy band structure and synergistic effect of the heterojunction. This work provides some novel insights into designing 2D layered heterojunction photocatalysts, boosting photocatalytic performance, and advancing Ti3C2 application. [Display omitted] •2D/2D Ti3C2/BiOClxBr1-x heterojunctions were constructed via in-situ growth.•Carriers dynamics investigations suggest that Schottky junctions are formed between two materials.•Optimized heterojunction of 7 %-TB0.25 exhibits enhanced RhB degradation rate, 11.9 times higher than that of TB0.25.•The in-built electric field and band bending accelerate carriers’ separation and accumulation.
ArticleNumber 131010
Author Liu, Yuwei
Zhang, Xiaowen
Xue, Xiaogang
Zeng, Liya
Yuan, Changlai
Wu, Danni
Author_xml – sequence: 1
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  givenname: Liya
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  givenname: Yuwei
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  givenname: Changlai
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  givenname: Xiaogang
  surname: Xue
  fullname: Xue, Xiaogang
  email: liangzixue@163.com
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  givenname: Xiaowen
  surname: Zhang
  fullname: Zhang, Xiaowen
  email: zhang-xiaowen@163.com
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Keywords BiOClxBr1−x
Photocatalyst
Ti3C2
Heterojunction
RhB photodegradation
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Snippet Newly emerged 2D metallic Ti3C2 is highly spotlighted for its unique properties and ubiquitous compounding compatibility. Herein we pioneeringly demonstrate a...
Newly emerged 2D metallic Ti₃C₂ is highly spotlighted for its unique properties and ubiquitous compounding compatibility. Herein we pioneeringly demonstrate a...
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SubjectTerms absorbance
BiOClxBr1−x
electric current
electrochemistry
electron paramagnetic resonance spectroscopy
energy
Fourier transform infrared spectroscopy
Heterojunction
nanosheets
photocatalysis
Photocatalyst
photocatalysts
photoluminescence
photolysis
RhB photodegradation
species
synergism
Ti3C2
X-ray diffraction
X-ray photoelectron spectroscopy
Title Design of 2D/2D heterojunction of Ti3C2/BiOClxBr1−x for enhancing photocatalytic performance
URI https://dx.doi.org/10.1016/j.colsurfa.2023.131010
https://www.proquest.com/docview/3242049396
Volume 663
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