Ultrasonic synthesis, characterization and formation mechanism of aggregated nanorings of EuF3
The aggregated nanorings of EuF3 were synthesized via ultrasonic irritation in aqueous solution. The products were characterized by X-ray powder diffraction （XRD）, scanning electron microscopy （SEM）, and transmission electron microscopy （TEM）. XRD pattern proved that the crystalline phase of the EuF...
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| Published in | Journal of rare earths Vol. 26; no. 5; pp. 684 - 687 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Chemistry and Environmental College,Henan Normal University,Xinxiang 453007,China
01.10.2008
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| Online Access | Get full text |
| ISSN | 1002-0721 2509-4963 |
| DOI | 10.1016/S1002-0721(08)60163-5 |
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| Abstract | The aggregated nanorings of EuF3 were synthesized via ultrasonic irritation in aqueous solution. The products were characterized by X-ray powder diffraction （XRD）, scanning electron microscopy （SEM）, and transmission electron microscopy （TEM）. XRD pattern proved that the crystalline phase of the EuF3 rings was hexagonal. The SEM and TEM images indicated that the as-prepared EuF3 nanocrystals had ring-like morphology and were aggregated by numerous small crystallites （about 10-15 nm in diameter）; the outer diameter of the rings was in the range of 200--300 nm, while the inner diameter was in the range of 50-80 nm with a thickness of 30-40 nm. Moreover, the time-depend experiments were carried out to disclose the formation mechanism of the as-prepared ring-like nanostructures. |
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| AbstractList | The aggregated nanorings of EuF3 were synthesized via ultrasonic irritation in aqueous solution. The products were characterized by X-ray powder diffraction （XRD）, scanning electron microscopy （SEM）, and transmission electron microscopy （TEM）. XRD pattern proved that the crystalline phase of the EuF3 rings was hexagonal. The SEM and TEM images indicated that the as-prepared EuF3 nanocrystals had ring-like morphology and were aggregated by numerous small crystallites （about 10-15 nm in diameter）; the outer diameter of the rings was in the range of 200--300 nm, while the inner diameter was in the range of 50-80 nm with a thickness of 30-40 nm. Moreover, the time-depend experiments were carried out to disclose the formation mechanism of the as-prepared ring-like nanostructures. O6; The aggregated nanorings of EuF3 were synthesized via ultrasonic irritation in aqueous solution. The products were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). XRD pattern proved that the crystalline phase of the EuF3 rngs was hexagonal. The SEM and TEM images indicated that the as-prepared EuF3 nanocrys-tals had ring-like morphology and were aggregated by numerous small crystallites (about 10-15 nm in diameter); the outer diameter of the rings was in the range of 200-300 nm, while the inner diameter was in the range of 50-80 nm with a thickness of 30-40 nm. Moreover, the time-depend experiments were carried out to disclose the formation mechanism of the as-prepared ring-like nanostructures. The aggregated nanorings of EuF3 were synthesized via ultrasonic irritation in aqueous solution. The products were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). XRD pattern proved that the crystalline phase of the EuF3 rings was hexagonal. The SEM and TEM images indicated that the as-prepared EuF3 nanocrystals had ring-like morphology and were aggregated by numerous small crystallites (about 10-15 nm in diameter); the outer diameter of the rings was in the range of 200-300 nm, while the inner diameter was in the range of 50-80 nm with a thickness of 30-40 nm. Moreover, the time-depend experiments were carried out to disclose the formation mechanism of the as-prepared ring-like nanostructures. |
| Author | 武大鹏 王新军 白正宇 蒋凯 |
| AuthorAffiliation | Chemistry and Environmental College, Henan Normal University, Xinxiang 453007, China |
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| CitedBy_id | crossref_primary_10_1016_j_ceramint_2014_12_071 crossref_primary_10_1016_j_colsurfa_2011_01_034 crossref_primary_10_1016_j_dyepig_2017_04_058 crossref_primary_10_1142_S1793292014500829 crossref_primary_10_1016_j_jfluchem_2013_01_035 crossref_primary_10_1016_j_jlumin_2018_05_002 |
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| Snippet | The aggregated nanorings of EuF3 were synthesized via ultrasonic irritation in aqueous solution. The products were characterized by X-ray powder diffraction... O6; The aggregated nanorings of EuF3 were synthesized via ultrasonic irritation in aqueous solution. The products were characterized by X-ray powder... |
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| Title | Ultrasonic synthesis, characterization and formation mechanism of aggregated nanorings of EuF3 |
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