Insights into influence of nanoparticle size and metal-support interactions of Cu/ZnO catalysts on activity for furfural hydrogenation
Cu/ZnO catalysts primarily derived from aurichalcite with Cu/Zn = 0.4-1.1 (mol/mol) were prepared via "decreased pH" coprecipitation method and introduced in hydrogenation of furfural to furfuryl alcohol. The "precursor effect" was clearly confirmed and the catalyst with a Cu/Zn...
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| Published in | Catalysis science & technology Vol. 7; no. 23; pp. 5625 - 5634 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Cambridge
Royal Society of Chemistry
2017
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| Subjects | |
| Online Access | Get full text |
| ISSN | 2044-4753 2044-4761 |
| DOI | 10.1039/c7cy01284e |
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| Abstract | Cu/ZnO catalysts primarily derived from aurichalcite with Cu/Zn = 0.4-1.1 (mol/mol) were prepared
via
"decreased pH" coprecipitation method and introduced in hydrogenation of furfural to furfuryl alcohol. The "precursor effect" was clearly confirmed and the catalyst with a Cu/Zn = 0.8 provided the best conversion and TOF. Catalysts were characterized
via
XRD, FT-IR, N
2
O titration, TEM, H
2
-TPR, XPS and AES. The size of Cu nanoparticles and Cu-ZnO interactions were systematically investigated and were found to remarkably influence catalytic activity of the catalysts. Consequently, the best catalytic performance for the catalyst with Cu/Zn = 0.8 was due to the suitable Cu particle size (8 nm) and strong metal-support interactions (SMSI), acting as the Cu-ZnO synergy.
Cu/ZnO catalysts primarily derived from aurichalcite with Cu/Zn = 0.4-1.1 (mol/mol) were prepared
via
"decreased pH" coprecipitation method and introduced in hydrogenation of furfural to furfuryl alcohol. |
|---|---|
| AbstractList | Cu/ZnO catalysts primarily derived from aurichalcite with Cu/Zn = 0.4–1.1 (mol/mol) were prepared via “decreased pH” coprecipitation method and introduced in hydrogenation of furfural to furfuryl alcohol. The “precursor effect” was clearly confirmed and the catalyst with a Cu/Zn = 0.8 provided the best conversion and TOF. Catalysts were characterized via XRD, FT-IR, N2O titration, TEM, H2-TPR, XPS and AES. The size of Cu nanoparticles and Cu–ZnO interactions were systematically investigated and were found to remarkably influence catalytic activity of the catalysts. Consequently, the best catalytic performance for the catalyst with Cu/Zn = 0.8 was due to the suitable Cu particle size (8 nm) and strong metal–support interactions (SMSI), acting as the Cu–ZnO synergy. Cu/ZnO catalysts primarily derived from aurichalcite with Cu/Zn = 0.4-1.1 (mol/mol) were prepared via "decreased pH" coprecipitation method and introduced in hydrogenation of furfural to furfuryl alcohol. The "precursor effect" was clearly confirmed and the catalyst with a Cu/Zn = 0.8 provided the best conversion and TOF. Catalysts were characterized via XRD, FT-IR, N 2 O titration, TEM, H 2 -TPR, XPS and AES. The size of Cu nanoparticles and Cu-ZnO interactions were systematically investigated and were found to remarkably influence catalytic activity of the catalysts. Consequently, the best catalytic performance for the catalyst with Cu/Zn = 0.8 was due to the suitable Cu particle size (8 nm) and strong metal-support interactions (SMSI), acting as the Cu-ZnO synergy. Cu/ZnO catalysts primarily derived from aurichalcite with Cu/Zn = 0.4-1.1 (mol/mol) were prepared via "decreased pH" coprecipitation method and introduced in hydrogenation of furfural to furfuryl alcohol. Cu/ZnO catalysts primarily derived from aurichalcite with Cu/Zn = 0.4–1.1 (mol/mol) were prepared via “decreased pH” coprecipitation method and introduced in hydrogenation of furfural to furfuryl alcohol. The “precursor effect” was clearly confirmed and the catalyst with a Cu/Zn = 0.8 provided the best conversion and TOF. Catalysts were characterized via XRD, FT-IR, N 2 O titration, TEM, H 2 -TPR, XPS and AES. The size of Cu nanoparticles and Cu–ZnO interactions were systematically investigated and were found to remarkably influence catalytic activity of the catalysts. Consequently, the best catalytic performance for the catalyst with Cu/Zn = 0.8 was due to the suitable Cu particle size (8 nm) and strong metal–support interactions (SMSI), acting as the Cu–ZnO synergy. |
| Author | Meng, Qingwei Li, Yong Wang Zhu, Yulei Yang, Xiaohai Chen, Hongmei Zheng, Hongyan |
| AuthorAffiliation | State Key Laboratory of Coal Conversion Chinese Academy of Sciences Synfuels China Co. Ltd Institute of Coal Chemistry University of Chinese Academy of Sciences |
| AuthorAffiliation_xml | – name: Institute of Coal Chemistry – name: University of Chinese Academy of Sciences – name: Chinese Academy of Sciences – name: State Key Laboratory of Coal Conversion – name: Synfuels China Co. Ltd |
| Author_xml | – sequence: 1 givenname: Xiaohai surname: Yang fullname: Yang, Xiaohai – sequence: 2 givenname: Hongmei surname: Chen fullname: Chen, Hongmei – sequence: 3 givenname: Qingwei surname: Meng fullname: Meng, Qingwei – sequence: 4 givenname: Hongyan surname: Zheng fullname: Zheng, Hongyan – sequence: 5 givenname: Yulei surname: Zhu fullname: Zhu, Yulei – sequence: 6 givenname: Yong Wang surname: Li fullname: Li, Yong Wang |
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| Snippet | Cu/ZnO catalysts primarily derived from aurichalcite with Cu/Zn = 0.4-1.1 (mol/mol) were prepared
via
"decreased pH" coprecipitation method and introduced in... Cu/ZnO catalysts primarily derived from aurichalcite with Cu/Zn = 0.4–1.1 (mol/mol) were prepared via “decreased pH” coprecipitation method and introduced in... Cu/ZnO catalysts primarily derived from aurichalcite with Cu/Zn = 0.4–1.1 (mol/mol) were prepared via “decreased pH” coprecipitation method and introduced in... |
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| SubjectTerms | Catalysis Catalysts Catalytic activity Copper Furfural Furfuryl alcohol Hydrogenation Nanoparticles Nitrous oxide Titration X ray photoelectron spectroscopy Zinc oxide |
| Title | Insights into influence of nanoparticle size and metal-support interactions of Cu/ZnO catalysts on activity for furfural hydrogenation |
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