Large specific surface area S-doped Fe–N–C electrocatalysts derived from Metal–Organic frameworks for oxygen reduction reaction

It is highly desired but challenging to develop platinum group metal-free electrocatalysts for oxygen reduction reaction (ORR), which can promote the commercialization of fuel cell technology. To achieve this target, we report a one-step doping method to prepare S-doped Fe–N–C catalysts using zeolit...

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Published inProgress in natural science Vol. 30; no. 6; pp. 896 - 904
Main Authors Yan, Xiaohui, Li, Xiaolin, Fu, Cehuang, Lin, Chen, Hu, Huanming, Shen, Shuiyun, Wei, Guanghua, Zhang, Junliang
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.12.2020
Subjects
Acidic and alkaline medium
Co-doping
Fuel cells
Non-precious metal catalyst
Oxygen reduction reaction
Acidic and alkaline medium
Non-precious metal catalyst
Fuel cells
Oxygen reduction reaction
Co-doping
Online AccessGet full text
ISSN1002-0071
DOI10.1016/j.pnsc.2020.10.018

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Abstract It is highly desired but challenging to develop platinum group metal-free electrocatalysts for oxygen reduction reaction (ORR), which can promote the commercialization of fuel cell technology. To achieve this target, we report a one-step doping method to prepare S-doped Fe–N–C catalysts using zeolite imidazole framework (ZIF-8) and iron (III) thiocyanate (Fe(SCN)3) as precursor. Different from conventional doping approach, i.e. physical mixing, Fe(SCN)3 is in-situ added during ZIF-8 formation which would encapsulate Fe(SCN)3 molecules inside ZIF-8 to avoid structure destruction and create potential replacement of Zn ions by Fe ions to form uniform Fe–N4 complexes. As a result, the prepared S-doped Fe–N–C catalysts own large specific surface areas with a maximum value of 1326 ​m2 ​g−1 and a dual-scale porous structure that benefits mass transport. Significantly, the composition-optimized catalyst exhibits superior ORR activity in both 0.1 ​M HClO4 electrolyte and 0.1 ​M KOH electrolyte, in which the half-wave potential reaches 0.81 ​V and 0.92 ​V (vs. RHE), respectively. Remarkable stability is also attained, which loses 2 ​mV only after 10000 potential cycles in O2-saturated 0.1 ​M HClO4 and remains almost constant in O2-saturated 0.1 ​M KOH, surpassing commercial Pt/C catalyst in both acidic and alkaline medium. [Display omitted] •S-doped Fe–N–C electrocatalysts were prepared via one-step doping method.•Prepared catalysts own ultrahigh specific surface area (1062–1326 ​m2 ​g−1).•The catalysts show good activity and durability in both acidic and alkaline medium.
AbstractList It is highly desired but challenging to develop platinum group metal-free electrocatalysts for oxygen reduction reaction (ORR), which can promote the commercialization of fuel cell technology. To achieve this target, we report a one-step doping method to prepare S-doped Fe–N–C catalysts using zeolite imidazole framework (ZIF-8) and iron (III) thiocyanate (Fe(SCN)3) as precursor. Different from conventional doping approach, i.e. physical mixing, Fe(SCN)3 is in-situ added during ZIF-8 formation which would encapsulate Fe(SCN)3 molecules inside ZIF-8 to avoid structure destruction and create potential replacement of Zn ions by Fe ions to form uniform Fe–N4 complexes. As a result, the prepared S-doped Fe–N–C catalysts own large specific surface areas with a maximum value of 1326 ​m2 ​g−1 and a dual-scale porous structure that benefits mass transport. Significantly, the composition-optimized catalyst exhibits superior ORR activity in both 0.1 ​M HClO4 electrolyte and 0.1 ​M KOH electrolyte, in which the half-wave potential reaches 0.81 ​V and 0.92 ​V (vs. RHE), respectively. Remarkable stability is also attained, which loses 2 ​mV only after 10000 potential cycles in O2-saturated 0.1 ​M HClO4 and remains almost constant in O2-saturated 0.1 ​M KOH, surpassing commercial Pt/C catalyst in both acidic and alkaline medium. [Display omitted] •S-doped Fe–N–C electrocatalysts were prepared via one-step doping method.•Prepared catalysts own ultrahigh specific surface area (1062–1326 ​m2 ​g−1).•The catalysts show good activity and durability in both acidic and alkaline medium.
Author Shen, Shuiyun
Lin, Chen
Fu, Cehuang
Li, Xiaolin
Zhang, Junliang
Yan, Xiaohui
Hu, Huanming
Wei, Guanghua
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Keywords Acidic and alkaline medium
Non-precious metal catalyst
Fuel cells
Oxygen reduction reaction
Co-doping
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Snippet It is highly desired but challenging to develop platinum group metal-free electrocatalysts for oxygen reduction reaction (ORR), which can promote the...
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elsevier
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SubjectTerms Acidic and alkaline medium
Co-doping
Fuel cells
Non-precious metal catalyst
Oxygen reduction reaction
Title Large specific surface area S-doped Fe–N–C electrocatalysts derived from Metal–Organic frameworks for oxygen reduction reaction
URI https://dx.doi.org/10.1016/j.pnsc.2020.10.018
Volume 30
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