Synthesis and Characterization of Lead Zirconate Titanate Nanofibers Obtained by Electrospinning
In this study, lead zirconate titanate (PZT) nanofibers were synthesized by electrospinning method using polyvinylpyrrolidone (PVP) as a viscosity controller and were characterized the crystallinity and the chemical composition of PZT nanofibers obtained by different postannealing methods. From the...
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| Published in | Bulletin of the Korean Chemical Society Vol. 36; no. 6; pp. 1594 - 1598 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Wiley-VCH Verlag GmbH & Co. KGaA
01.06.2015
Wiley‐VCH Verlag GmbH & Co. KGaA 대한화학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1229-5949 0253-2964 1229-5949 |
| DOI | 10.1002/bkcs.10303 |
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| Abstract | In this study, lead zirconate titanate (PZT) nanofibers were synthesized by electrospinning method using polyvinylpyrrolidone (PVP) as a viscosity controller and were characterized the crystallinity and the chemical composition of PZT nanofibers obtained by different postannealing methods. From the X‐ray photoelectron spectroscopy results, the formation of PZT nanofibers was confirmed. The diameter of PZT nanofibers was a few hundreds of nanometers. And the diameter of PZT‐D (directly annealed to the target temperature) nanofibers decreased as the annealing temperature increased while the diameter of PZT‐S (stepwisely annealed to the target temperature) nanofibers increased which were confirmed by SEM. According to the results of X‐ray diffraction, as the annealing temperature increased, the crystallinity of PZT nanofibers changed from pyrochlore to perovskite structure and the perovskite phase of PZT was observed from the PZT nanofibers annealed at 823 K. |
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| AbstractList | In this study, lead zirconate titanate (PZT) nanofibers were synthesized by electrospinning method using polyvinylpyrrolidone (PVP) as a viscosity controller and were characterized the crystallinity and the chemical composition of PZT nanofibers obtained by different postannealing methods. From the X‐ray photoelectron spectroscopy results, the formation of PZT nanofibers was confirmed. The diameter of PZT nanofibers was a few hundreds of nanometers. And the diameter of PZT‐D (directly annealed to the target temperature) nanofibers decreased as the annealing temperature increased while the diameter of PZT‐S (stepwisely annealed to the target temperature) nanofibers increased which were confirmed by SEM. According to the results of X‐ray diffraction, as the annealing temperature increased, the crystallinity of PZT nanofibers changed from pyrochlore to perovskite structure and the perovskite phase of PZT was observed from the PZT nanofibers annealed at 823 K. In this study, lead zirconate titanate (PZT) nanofibers were synthesized by electrospinning method using polyvinylpyrrolidone (PVP) as a viscosity controller and were characterized the crystallinity and the chemical composition of PZT nanofibers obtained by different postannealing methods. From the X-ray photoelectron spectroscopy results, the formation of PZT nanofibers was confirmed. The diameter of PZT nanofibers was a few hundreds of nanometers. And the diameter of PZT-D (directly annealed to the target temperature) nanofibers decreased as the annealing temperature increased while the diameter of PZT-S (stepwisely annealed to the target temperature) nanofibers increased which were confirmed by SEM. According to the results of X-ray diffraction, as the annealing temperature increased, the crystallinity of PZT nanofibers changed from pyrochlore to perovskite structure and the perovskite phase of PZT was observed from the PZT nanofibers annealed at 823 K. KCI Citation Count: 6 In this study, lead zirconate titanate ( PZT ) nanofibers were synthesized by electrospinning method using polyvinylpyrrolidone ( PVP ) as a viscosity controller and were characterized the crystallinity and the chemical composition of PZT nanofibers obtained by different postannealing methods. From the X‐ray photoelectron spectroscopy results, the formation of PZT nanofibers was confirmed. The diameter of PZT nanofibers was a few hundreds of nanometers. And the diameter of PZT ‐D (directly annealed to the target temperature) nanofibers decreased as the annealing temperature increased while the diameter of PZT ‐S (stepwisely annealed to the target temperature) nanofibers increased which were confirmed by SEM . According to the results of X‐ray diffraction, as the annealing temperature increased, the crystallinity of PZT nanofibers changed from pyrochlore to perovskite structure and the perovskite phase of PZT was observed from the PZT nanofibers annealed at 823 K . |
| Author | Park, Juyun Koh, Sung-Wi Kang, Yong-Cheol Choi, Sujin Kang, Jisoo |
| Author_xml | – sequence: 1 givenname: Sujin surname: Choi fullname: Choi, Sujin organization: Department of Chemistry, Pukyong National University, 608-737, Busan, Korea – sequence: 2 givenname: Juyun surname: Park fullname: Park, Juyun organization: Department of Chemistry, Pukyong National University, 608-737, Busan, Korea – sequence: 3 givenname: Jisoo surname: Kang fullname: Kang, Jisoo organization: Nano/Bio Interface Center, University of Pennsylvania, PA, 19104, Philadelphia, USA – sequence: 4 givenname: Sung-Wi surname: Koh fullname: Koh, Sung-Wi organization: Department of Mechanical System Engineering, Pukyong National University, 608-739, Busan, Korea – sequence: 5 givenname: Yong-Cheol surname: Kang fullname: Kang, Yong-Cheol email: yckang@pknu.ac.kr organization: Department of Chemistry, Pukyong National University, 608-737, Busan, Korea |
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| CitedBy_id | crossref_primary_10_1016_j_physb_2020_412257 crossref_primary_10_3390_nano15050409 crossref_primary_10_1016_j_apsusc_2019_144883 crossref_primary_10_1016_j_ceramint_2025_02_211 crossref_primary_10_1002_sia_6630 crossref_primary_10_1016_j_ceramint_2022_05_003 crossref_primary_10_1016_j_jhazmat_2021_126792 crossref_primary_10_1002_pssa_202400618 crossref_primary_10_1007_s10854_019_01197_0 crossref_primary_10_1016_j_cej_2024_154913 crossref_primary_10_1016_j_mseb_2023_116702 crossref_primary_10_1002_pssa_202100148 |
| Cites_doi | 10.1063/1.1631750 10.1080/10584587.2010.491726 10.1016/S0169-4332(01)00027-7 10.1021/cm500381g 10.1002/crat.201100409 10.1088/0957-4484/17/17/036 10.1111/j.1151-2916.1998.tb02420.x 10.1111/j.1151-2916.1998.tb02300.x 10.1063/1.2837185 10.1016/S0040-6090(00)01013-0 10.1002/adma.200400998 10.1016/j.apsusc.2013.05.103 10.1016/j.jallcom.2013.07.099 10.1016/S0169-4332(98)00577-7 10.1016/j.matlet.2005.05.040 10.1016/j.apsusc.2011.01.056 10.1016/j.apsusc.2013.11.041 10.1016/j.matlet.2012.01.082 10.1016/S0167-577X(99)00190-1 10.1111/j.1151-2916.1999.tb01840.x 10.1016/j.apsusc.2005.03.168 10.1088/0964-1726/12/3/303 10.1007/s00339-003-2152-2 10.1016/j.mee.2012.07.026 10.1016/S0955-2219(97)00027-7 10.1016/j.msea.2005.04.036 |
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| Snippet | In this study, lead zirconate titanate (PZT) nanofibers were synthesized by electrospinning method using polyvinylpyrrolidone (PVP) as a viscosity controller... In this study, lead zirconate titanate ( PZT ) nanofibers were synthesized by electrospinning method using polyvinylpyrrolidone ( PVP ) as a viscosity... |
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| SubjectTerms | Lead zirconate titanate Nanofiber Perovskite X-ray diffraction X-ray photoelectron spectroscopy 화학 |
| Title | Synthesis and Characterization of Lead Zirconate Titanate Nanofibers Obtained by Electrospinning |
| URI | https://api.istex.fr/ark:/67375/WNG-FR1D6KZ0-9/fulltext.pdf https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fbkcs.10303 https://www.kci.go.kr/kciportal/ci/sereArticleSearch/ciSereArtiView.kci?sereArticleSearchBean.artiId=ART001996461 |
| Volume | 36 |
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| ispartofPNX | Bulletin of the Korean Chemical Society, 2015, 36(6), , pp.1594-1598 |
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