Microstructure, fractal geometry and corrosion properties of CrN thin films: The effect of shot number and angular position

The effect of different plasma focus shots and angular positions (0° and 30°) on the properties of chromium nitride (CrN) coatings, deposited by a plasma focus (PF) device on stainless steel substrates, have been systematically investigated in this paper. The structural and morphological properties...

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Published inMaterials today communications Vol. 32; p. 104072
Main Authors Habibi, Maryam, Mirzaei, Saeed, Arman, Ali, Jurečka, Stanislav, Sadeghi, Mohammad, Zelati, Amir, Shakoury, Reza, Tanhaee, Ehsan, Ghobadi, Nader, Ehteram, Hamid, Ţălu, Ştefan
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.08.2022
Subjects
AFM
Angular positions
Atomic-force-microscopy
Chromium alloys
Chromium compounds
Chromium nitride
Chromium nitride coatings
Corrosion properties
Corrosion property
Corrosion resistance
Corrosion resistant coatings
Corrosive effects
CrN coating
Crystallinity
Film preparation
Fractals
Nitride thin films
Plasma focus
Stainless steel
Stainless steel substrates
Steel corrosion
Substrates
Thin films
X ray diffraction
X- ray diffractions
XRD
AFM
Plasma focus
XRD
CrN coating
Corrosion properties
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Abstract The effect of different plasma focus shots and angular positions (0° and 30°) on the properties of chromium nitride (CrN) coatings, deposited by a plasma focus (PF) device on stainless steel substrates, have been systematically investigated in this paper. The structural and morphological properties of CrN thin films were characterized by X-ray diffraction (XRD) and atomic force microscopy (AFM). Moreover, the corrosion behavior of the CrN thin films was investigated using the ‘c’ method. The XRD patterns demonstrated the growth of the polycrystalline structure composed of CrN/Cr2N nanograins and the enhanced crystallinity of the CrN coatings upon increasing the shot numbers. In addition, AFM results showed enhanced multifractal properties of the sample prepared at 0° angular position and a reducing trend in these properties for the layers prepared at 30° angular position. Moreover, they exhibited sharp hillock-like features on the surface, corresponding to the columnar growth of the CrN coatings, which further protruded as the number of shots increased. The results of the corrosion test showed that the resistance of stainless-steel substrate was improved by depositing the CrN coatings due to the formation of a passive and protective layer on its surface. Notably, ceramic CrN film, prepared through 10 shots at 30° angular position, showed the best corrosion resistance. Our strategy is advantageous for designing and manufacturing novel devices and instruments based on CrN corrosion resistant coating. [Display omitted] •CrN/SS films have been deposited at different plasma focus shots and angular positions by plasma focus (PF) instruments.•The effect of shot number and angular position on the surface microtexture, and corrosion features of the films was studied.•The 3-D surface analysis of the samples was performed using an atomic force microscope operating in tapping mode.
AbstractList The effect of different plasma focus shots and angular positions (0° and 30°) on the properties of chromium nitride (CrN) coatings, deposited by a plasma focus (PF) device on stainless steel substrates, have been systematically investigated in this paper. The structural and morphological properties of CrN thin films were characterized by X-ray diffraction (XRD) and atomic force microscopy (AFM). Moreover, the corrosion behavior of the CrN thin films was investigated using the ‘c’ method. The XRD patterns demonstrated the growth of the polycrystalline structure composed of CrN/Cr2N nanograins and the enhanced crystallinity of the CrN coatings upon increasing the shot numbers. In addition, AFM results showed enhanced multifractal properties of the sample prepared at 0° angular position and a reducing trend in these properties for the layers prepared at 30° angular position. Moreover, they exhibited sharp hillock-like features on the surface, corresponding to the columnar growth of the CrN coatings, which further protruded as the number of shots increased. The results of the corrosion test showed that the resistance of stainless-steel substrate was improved by depositing the CrN coatings due to the formation of a passive and protective layer on its surface. Notably, ceramic CrN film, prepared through 10 shots at 30° angular position, showed the best corrosion resistance. Our strategy is advantageous for designing and manufacturing novel devices and instruments based on CrN corrosion resistant coating.
The effect of different plasma focus shots and angular positions (0° and 30°) on the properties of chromium nitride (CrN) coatings, deposited by a plasma focus (PF) device on stainless steel substrates, have been systematically investigated in this paper. The structural and morphological properties of CrN thin films were characterized by X-ray diffraction (XRD) and atomic force microscopy (AFM). Moreover, the corrosion behavior of the CrN thin films was investigated using the ‘c’ method. The XRD patterns demonstrated the growth of the polycrystalline structure composed of CrN/Cr2N nanograins and the enhanced crystallinity of the CrN coatings upon increasing the shot numbers. In addition, AFM results showed enhanced multifractal properties of the sample prepared at 0° angular position and a reducing trend in these properties for the layers prepared at 30° angular position. Moreover, they exhibited sharp hillock-like features on the surface, corresponding to the columnar growth of the CrN coatings, which further protruded as the number of shots increased. The results of the corrosion test showed that the resistance of stainless-steel substrate was improved by depositing the CrN coatings due to the formation of a passive and protective layer on its surface. Notably, ceramic CrN film, prepared through 10 shots at 30° angular position, showed the best corrosion resistance. Our strategy is advantageous for designing and manufacturing novel devices and instruments based on CrN corrosion resistant coating. [Display omitted] •CrN/SS films have been deposited at different plasma focus shots and angular positions by plasma focus (PF) instruments.•The effect of shot number and angular position on the surface microtexture, and corrosion features of the films was studied.•The 3-D surface analysis of the samples was performed using an atomic force microscope operating in tapping mode.
ArticleNumber 104072
Author Sadeghi, Mohammad
Tanhaee, Ehsan
Habibi, Maryam
Shakoury, Reza
Ţălu, Ştefan
Mirzaei, Saeed
Jurečka, Stanislav
Zelati, Amir
Ghobadi, Nader
Arman, Ali
Ehteram, Hamid
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  givenname: Ali
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  givenname: Ştefan
  surname: Ţălu
  fullname: Ţălu, Ştefan
  email: stefan.talu@auto.utcluj.ro
  organization: The Directorate of Research, Development and Innovation Management (DMCDI), Technical University of Cluj-Napoca, Constantin Daicoviciu St., no. 15, Cluj-Napoca 400020, Cluj County, Romania
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Snippet The effect of different plasma focus shots and angular positions (0° and 30°) on the properties of chromium nitride (CrN) coatings, deposited by a plasma focus...
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SubjectTerms AFM
Angular positions
Atomic-force-microscopy
Chromium alloys
Chromium compounds
Chromium nitride
Chromium nitride coatings
Corrosion properties
Corrosion property
Corrosion resistance
Corrosion resistant coatings
Corrosive effects
CrN coating
Crystallinity
Film preparation
Fractals
Nitride thin films
Plasma focus
Stainless steel
Stainless steel substrates
Steel corrosion
Substrates
Thin films
X ray diffraction
X- ray diffractions
XRD
Title Microstructure, fractal geometry and corrosion properties of CrN thin films: The effect of shot number and angular position
URI https://dx.doi.org/10.1016/j.mtcomm.2022.104072
https://urn.kb.se/resolve?urn=urn:nbn:se:mdh:diva-59614
Volume 32
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