Three-dimensionally ordered macroporous WO3 supported Ag3PO4 with enhanced photocatalytic activity and durability
[Display omitted] •Ag3PO4/3DOM-WO3 photocatalysts were firstly reported.•Ag3PO4/3DOM-WO3 exhibited super high activity in degradation of organic contaminants.•Ag3PO4/3DOM-WO3 was highly active and durable in water splitting for oxygen evolution.•Slow photon effect of 3DOM-WO3 could notably improve t...
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| Published in | Applied catalysis. B, Environmental Vol. 176-177; pp. 363 - 373 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.10.2015
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Ag3PO4/3DOM-WO3 photocatalysts were firstly reported.•Ag3PO4/3DOM-WO3 exhibited super high activity in degradation of organic contaminants.•Ag3PO4/3DOM-WO3 was highly active and durable in water splitting for oxygen evolution.•Slow photon effect of 3DOM-WO3 could notably improve the catalytic efficiency.•The notably enhanced durability was mainly due to the efficient transfer of electrons.
Ag3PO4 nanoparticles were firstly deposited into the three-dimensionally ordered macroporous WO3 (3DOM-WO3) with different pore sizes. The resulted Ag3PO4/3DOM-WO3 composites were characterized by XRD, SEM, TEM and DR UV–vis. These composite photocatalysts showed extraordinarily excellent efficiencies in the visible light degradation of organic contaminants and water splitting for oxygen evolution, which were mainly due to the synergic effect of Ag3PO4 and 3DOM-WO3 as well as the periodic macroporous structure of 3DOM-WO3. Especially, the catalyst A5W5 with Ag3PO4:WO3 mass ratio of 5:5 exhibited the highest catalytic activity, and complete degradation could be achieved within 4min for phenol and three typical dyes investigated in this work. In addition, the slow photon effect in Ag3PO4/3DOM-WO3 was demonstrated, and the pore size of 3DOM-WO3 was found to have a significant influence on the catalytic performance. The catalyst A5W5(270) showed notably higher photocatalytic activity than A5W5(150) and A5W5 (420), which was mainly attributed to the exact overlap between the stop-band of 3DOM-WO3(270) and the electronic absorption band of Ag3PO4/3DOM-WO3 composite. Moreover, these composite catalysts were very stable and could be recycled ten times without any loss in photocatalytic activity for RhB degradation. More excitingly, remarkably improved activity and durability were also obtained over Ag3PO4/3DOM-WO3 in water splitting for oxygen evolution. According to the XPS and HRTEM characterizations of used catalyst, the enhanced durability was mainly attributed to the effective transfer of photogenerated electrons from Ag3PO4 to 3DOM-WO3. |
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| AbstractList | [Display omitted]
•Ag3PO4/3DOM-WO3 photocatalysts were firstly reported.•Ag3PO4/3DOM-WO3 exhibited super high activity in degradation of organic contaminants.•Ag3PO4/3DOM-WO3 was highly active and durable in water splitting for oxygen evolution.•Slow photon effect of 3DOM-WO3 could notably improve the catalytic efficiency.•The notably enhanced durability was mainly due to the efficient transfer of electrons.
Ag3PO4 nanoparticles were firstly deposited into the three-dimensionally ordered macroporous WO3 (3DOM-WO3) with different pore sizes. The resulted Ag3PO4/3DOM-WO3 composites were characterized by XRD, SEM, TEM and DR UV–vis. These composite photocatalysts showed extraordinarily excellent efficiencies in the visible light degradation of organic contaminants and water splitting for oxygen evolution, which were mainly due to the synergic effect of Ag3PO4 and 3DOM-WO3 as well as the periodic macroporous structure of 3DOM-WO3. Especially, the catalyst A5W5 with Ag3PO4:WO3 mass ratio of 5:5 exhibited the highest catalytic activity, and complete degradation could be achieved within 4min for phenol and three typical dyes investigated in this work. In addition, the slow photon effect in Ag3PO4/3DOM-WO3 was demonstrated, and the pore size of 3DOM-WO3 was found to have a significant influence on the catalytic performance. The catalyst A5W5(270) showed notably higher photocatalytic activity than A5W5(150) and A5W5 (420), which was mainly attributed to the exact overlap between the stop-band of 3DOM-WO3(270) and the electronic absorption band of Ag3PO4/3DOM-WO3 composite. Moreover, these composite catalysts were very stable and could be recycled ten times without any loss in photocatalytic activity for RhB degradation. More excitingly, remarkably improved activity and durability were also obtained over Ag3PO4/3DOM-WO3 in water splitting for oxygen evolution. According to the XPS and HRTEM characterizations of used catalyst, the enhanced durability was mainly attributed to the effective transfer of photogenerated electrons from Ag3PO4 to 3DOM-WO3. |
| Author | Chang, Yue Li, Rui Liu, Shuangxi Zhang, Chenxi Lou, Lan-Lan Zhao, Peiyuan Yu, Kai |
| Author_xml | – sequence: 1 givenname: Yue surname: Chang fullname: Chang, Yue organization: Institute of New Catalytic Materials Science and Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), College of Chemistry, Nankai University, Tianjin 300071, People’s Republic of China – sequence: 2 givenname: Kai orcidid: 0000-0001-7569-3276 surname: Yu fullname: Yu, Kai email: kaiyu@nankai.edu.cn organization: College of Environmental Science and Engineering, Nankai University, Tianjin 300071, People’s Republic of China – sequence: 3 givenname: Chenxi surname: Zhang fullname: Zhang, Chenxi organization: Institute of New Catalytic Materials Science and Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), College of Chemistry, Nankai University, Tianjin 300071, People’s Republic of China – sequence: 4 givenname: Rui surname: Li fullname: Li, Rui organization: College of Environmental Science and Engineering, Nankai University, Tianjin 300071, People’s Republic of China – sequence: 5 givenname: Peiyuan surname: Zhao fullname: Zhao, Peiyuan organization: Institute of New Catalytic Materials Science and Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), College of Chemistry, Nankai University, Tianjin 300071, People’s Republic of China – sequence: 6 givenname: Lan-Lan surname: Lou fullname: Lou, Lan-Lan organization: Institute of New Catalytic Materials Science and Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), College of Chemistry, Nankai University, Tianjin 300071, People’s Republic of China – sequence: 7 givenname: Shuangxi surname: Liu fullname: Liu, Shuangxi email: sxliu@nankai.edu.cn organization: Institute of New Catalytic Materials Science and Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education), College of Chemistry, Nankai University, Tianjin 300071, People’s Republic of China |
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| Keywords | Slow photon effect Water oxidation Visible light photodegradation Three-dimensionally ordered macroporous material Ag3PO4/3DOM-WO3 |
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•Ag3PO4/3DOM-WO3 photocatalysts were firstly reported.•Ag3PO4/3DOM-WO3 exhibited super high activity in degradation of organic... |
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| SubjectTerms | Ag3PO4/3DOM-WO3 Slow photon effect Three-dimensionally ordered macroporous material Visible light photodegradation Water oxidation |
| Title | Three-dimensionally ordered macroporous WO3 supported Ag3PO4 with enhanced photocatalytic activity and durability |
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