Comparison of PdCo/SBA-15 prepared by co-impregnation and sequential impregnation for Fischer–Tropsch synthesis

Properties and catalytic performance of bimetallic Pd–Co/SBA-15 prepared by co-impregnation (0.2Pd–10Co-CIP) and sequential impregnation (0.2Pd–10Co-SIP) for Fischer–Tropsch synthesis (FTS) were investigated. After calcination, Co3O4 was formed and located inside the channels of SBA-15 and on extern...

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Published inCatalysis communications Vol. 66; pp. 73 - 78
Main Authors Osakoo, Nattawut, Henkel, Robert, Loiha, Sirinuch, Roessner, Frank, Wittayakun, Jatuporn
Format Journal Article
LanguageEnglish
Published Elsevier B.V 05.06.2015
Subjects
Co-impregnation
Cobalt
Fischer–Tropsch synthesis
Palladium
SBA-15
Sequential impregnation
Co-impregnation
Palladium
Cobalt
SBA-15
Sequential impregnation
Fischer–Tropsch synthesis
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Abstract Properties and catalytic performance of bimetallic Pd–Co/SBA-15 prepared by co-impregnation (0.2Pd–10Co-CIP) and sequential impregnation (0.2Pd–10Co-SIP) for Fischer–Tropsch synthesis (FTS) were investigated. After calcination, Co3O4 was formed and located inside the channels of SBA-15 and on external surface. Compared to 0.2Pd–10Co-SIP, 0.2Pd–10Co-CIP had a smaller surface area, pore size, lower reduction temperature and less active sites due to larger particle sizes of Co3O4. From FTS testing, 0.2Pd–10Co-SIP provided higher and steadier conversions of CO and H2 as well as higher yield of C5–C9 products. [Display omitted] •Co-Pd/SBA-15 was prepared by co-impregnation (CIP) and sequential impregnation (SIP).•The reduced SIP catalyst had better Co dispersion.•Pd enhanced reduction of cobalt oxides and hydrogenation in FTS.•The SIP catalyst gave higher conversions of CO and H2.•The SIP catalyst gave higher selectivity and yield of C5–C9 products.
AbstractList Properties and catalytic performance of bimetallic Pd–Co/SBA-15 prepared by co-impregnation (0.2Pd–10Co-CIP) and sequential impregnation (0.2Pd–10Co-SIP) for Fischer–Tropsch synthesis (FTS) were investigated. After calcination, Co3O4 was formed and located inside the channels of SBA-15 and on external surface. Compared to 0.2Pd–10Co-SIP, 0.2Pd–10Co-CIP had a smaller surface area, pore size, lower reduction temperature and less active sites due to larger particle sizes of Co3O4. From FTS testing, 0.2Pd–10Co-SIP provided higher and steadier conversions of CO and H2 as well as higher yield of C5–C9 products. [Display omitted] •Co-Pd/SBA-15 was prepared by co-impregnation (CIP) and sequential impregnation (SIP).•The reduced SIP catalyst had better Co dispersion.•Pd enhanced reduction of cobalt oxides and hydrogenation in FTS.•The SIP catalyst gave higher conversions of CO and H2.•The SIP catalyst gave higher selectivity and yield of C5–C9 products.
Author Osakoo, Nattawut
Loiha, Sirinuch
Roessner, Frank
Henkel, Robert
Wittayakun, Jatuporn
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Keywords Co-impregnation
Palladium
Cobalt
SBA-15
Sequential impregnation
Fischer–Tropsch synthesis
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Snippet Properties and catalytic performance of bimetallic Pd–Co/SBA-15 prepared by co-impregnation (0.2Pd–10Co-CIP) and sequential impregnation (0.2Pd–10Co-SIP) for...
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SubjectTerms Co-impregnation
Cobalt
Fischer–Tropsch synthesis
Palladium
SBA-15
Sequential impregnation
Title Comparison of PdCo/SBA-15 prepared by co-impregnation and sequential impregnation for Fischer–Tropsch synthesis
URI https://dx.doi.org/10.1016/j.catcom.2015.03.020
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