Magnetically assembled electrodes based on Pt, RuO2-IrO2-TiO2 and Sb-SnO2 for electrochemical oxidation of wastewater featured by fluctuant Cl- concentration
Magnetically assembled electrode (MAE) flexibly attracts magnetic particles (auxiliary electrodes, AEs) on a main electrode (ME) by the magnetic force, where the role of ME is always ignored. In this study, Ti/Pt, Ti/RuO2-IrO2-TiO2 and Ti/Sb-SnO2 were selected as the ME for comparison in treating sy...
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| Published in | Journal of hazardous materials Vol. 421; p. 126803 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
05.01.2022
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| Subjects | |
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| Abstract | Magnetically assembled electrode (MAE) flexibly attracts magnetic particles (auxiliary electrodes, AEs) on a main electrode (ME) by the magnetic force, where the role of ME is always ignored. In this study, Ti/Pt, Ti/RuO2-IrO2-TiO2 and Ti/Sb-SnO2 were selected as the ME for comparison in treating synthetic wastewater (acid red G or phenol) with variable Cl- content. The effects of ME type, loading amount of Fe3O4/Sb-SnO2 AEs, and Cl- concentration were investigated, followed by varied electrochemical characterizations. Results show that AEs played a vital role in electrode activity and selectivity, and MEs also exerted an unignorable influence on the performance of the MAEs. Among the three MEs, Ti/RuO2-IrO2-TiO2 has the best OER/CER ability, activating more extra active sites with same AEs loading amount, leading to higher organics degradation efficiency under chlorine-free condition. However, this MAE is featured by the noticeable accumulation of intermediate products under chlorine-free condition even if 0.3 g·cm−2 of AEs are loaded. All electrodes’ performances were enhanced in the presence of Cl-. With high concentration chloride (0.5 M NaCl), the accumulation of intermediate products was reduced significantly, especially on Ti/RuO2-IrO2-TiO2 based MAE, and no chlorinated compound was identified. Finally, the structure-activity relationships of these MAEs were proposed.
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•A new anode architecture was organized by magnetic force.•Main electrodes with different OER/CER activity were compared.•Magnetic particles could effectively increase the less accessible active sites.•The structure-activity relationships under variable Cl- content were discussed. |
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| AbstractList | Magnetically assembled electrode (MAE) flexibly attracts magnetic particles (auxiliary electrodes, AEs) on a main electrode (ME) by the magnetic force, where the role of ME is always ignored. In this study, Ti/Pt, Ti/RuO2-IrO2-TiO2 and Ti/Sb-SnO2 were selected as the ME for comparison in treating synthetic wastewater (acid red G or phenol) with variable Cl- content. The effects of ME type, loading amount of Fe3O4/Sb-SnO2 AEs, and Cl- concentration were investigated, followed by varied electrochemical characterizations. Results show that AEs played a vital role in electrode activity and selectivity, and MEs also exerted an unignorable influence on the performance of the MAEs. Among the three MEs, Ti/RuO2-IrO2-TiO2 has the best OER/CER ability, activating more extra active sites with same AEs loading amount, leading to higher organics degradation efficiency under chlorine-free condition. However, this MAE is featured by the noticeable accumulation of intermediate products under chlorine-free condition even if 0.3 g·cm−2 of AEs are loaded. All electrodes’ performances were enhanced in the presence of Cl-. With high concentration chloride (0.5 M NaCl), the accumulation of intermediate products was reduced significantly, especially on Ti/RuO2-IrO2-TiO2 based MAE, and no chlorinated compound was identified. Finally, the structure-activity relationships of these MAEs were proposed.
[Display omitted]
•A new anode architecture was organized by magnetic force.•Main electrodes with different OER/CER activity were compared.•Magnetic particles could effectively increase the less accessible active sites.•The structure-activity relationships under variable Cl- content were discussed. |
| ArticleNumber | 126803 |
| Author | Xu, Hao Zhang, Yuanyuan Shao, Dan Yan, Wei Zhang, Cuiping Tan, Guoqiang Rao, Yongfang |
| Author_xml | – sequence: 1 givenname: Yuanyuan surname: Zhang fullname: Zhang, Yuanyuan organization: School of Materials Science and Engineering, Shaanxi Key Laboratory of Green Preparation and Functionalization for Inorganic Materials, Shaanxi University of Science & Technology, Xi’an 710021, China – sequence: 2 givenname: Cuiping surname: Zhang fullname: Zhang, Cuiping organization: School of Materials Science and Engineering, Shaanxi Key Laboratory of Green Preparation and Functionalization for Inorganic Materials, Shaanxi University of Science & Technology, Xi’an 710021, China – sequence: 3 givenname: Dan surname: Shao fullname: Shao, Dan email: shaodan@sust.edu.cn organization: School of Materials Science and Engineering, Shaanxi Key Laboratory of Green Preparation and Functionalization for Inorganic Materials, Shaanxi University of Science & Technology, Xi’an 710021, China – sequence: 4 givenname: Hao surname: Xu fullname: Xu, Hao email: xuhao@mail.xjtu.edu.cn organization: Department of Environmental Engineering, Xi’an Jiaotong University, Xi’an 710049, China – sequence: 5 givenname: Yongfang surname: Rao fullname: Rao, Yongfang organization: Department of Environmental Engineering, Xi’an Jiaotong University, Xi’an 710049, China – sequence: 6 givenname: Guoqiang surname: Tan fullname: Tan, Guoqiang organization: School of Materials Science and Engineering, Shaanxi Key Laboratory of Green Preparation and Functionalization for Inorganic Materials, Shaanxi University of Science & Technology, Xi’an 710021, China – sequence: 7 givenname: Wei surname: Yan fullname: Yan, Wei organization: Department of Environmental Engineering, Xi’an Jiaotong University, Xi’an 710049, China |
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