An integrated separation technology for high fluoride-containing wastewater treatment: Fluoride removal, membrane fouling behavior and control
The high concentration of fluoride in aqueous, which exacerbated by the discharged wastewater from semiconductor, electroplating, metallurgical and ceramics industries, has gone far beyond the World Health Organization (WHO) standard and seriously affected the health of human life. This study aims t...
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| Published in | Journal of cleaner production Vol. 349; p. 131225 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
15.05.2022
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| Subjects | |
| Online Access | Get full text |
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| Abstract | The high concentration of fluoride in aqueous, which exacerbated by the discharged wastewater from semiconductor, electroplating, metallurgical and ceramics industries, has gone far beyond the World Health Organization (WHO) standard and seriously affected the health of human life. This study aims to validate the deep removal of fluoride from high fluoride-containing wastewater by using an integrated precipitation/crystallization/ultrafiltration (UF)/reverse osmosis (RO) system. The system enables an extremely low residual fluoride concentration (down to 0.25 mg L−1) qualified WHO standard, which was much lower than those of other reported membrane-based processes. In particular, the application of crystallization rather than conventional coagulation/flocculation was demonstrated to be effective in reducing fluoride, turbidity and sludge water content. Membrane fouling analysis indicated that UF membrane scaling was attributed to the CaF2 particles deposition at recovery rates of 70%–90%. RO membrane fouling behaviors were identified at recovery rate of 50% (organic fouling), 70% (inorganic scaling occurred and organic fouling) and 80% (inorganic scaling and organic fouling). Meanwhile, UF/RO membrane scaling/fouling could be removed by pure water cleaning (UF) and Na2CO3/NaOH/HCl cleaning (RO). Results of this work shall provide useful information on the application of a precipitation/crystallization/UF/RO system to purify and recover high fluoride-containing wastewater.
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●A new integrated system for fluoride-containing wastewater treatment was developed.●Crystallization process reduced fluoride, turbidity and sludge water content.●UF/RO fouling behaviors were identified along the permeate recovery rates.●Residual fluoride in integrated system effluent qualified WHO standard. |
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| AbstractList | The high concentration of fluoride in aqueous, which exacerbated by the discharged wastewater from semiconductor, electroplating, metallurgical and ceramics industries, has gone far beyond the World Health Organization (WHO) standard and seriously affected the health of human life. This study aims to validate the deep removal of fluoride from high fluoride-containing wastewater by using an integrated precipitation/crystallization/ultrafiltration (UF)/reverse osmosis (RO) system. The system enables an extremely low residual fluoride concentration (down to 0.25 mg L⁻¹) qualified WHO standard, which was much lower than those of other reported membrane-based processes. In particular, the application of crystallization rather than conventional coagulation/flocculation was demonstrated to be effective in reducing fluoride, turbidity and sludge water content. Membrane fouling analysis indicated that UF membrane scaling was attributed to the CaF₂ particles deposition at recovery rates of 70%–90%. RO membrane fouling behaviors were identified at recovery rate of 50% (organic fouling), 70% (inorganic scaling occurred and organic fouling) and 80% (inorganic scaling and organic fouling). Meanwhile, UF/RO membrane scaling/fouling could be removed by pure water cleaning (UF) and Na₂CO₃/NaOH/HCl cleaning (RO). Results of this work shall provide useful information on the application of a precipitation/crystallization/UF/RO system to purify and recover high fluoride-containing wastewater. The high concentration of fluoride in aqueous, which exacerbated by the discharged wastewater from semiconductor, electroplating, metallurgical and ceramics industries, has gone far beyond the World Health Organization (WHO) standard and seriously affected the health of human life. This study aims to validate the deep removal of fluoride from high fluoride-containing wastewater by using an integrated precipitation/crystallization/ultrafiltration (UF)/reverse osmosis (RO) system. The system enables an extremely low residual fluoride concentration (down to 0.25 mg L−1) qualified WHO standard, which was much lower than those of other reported membrane-based processes. In particular, the application of crystallization rather than conventional coagulation/flocculation was demonstrated to be effective in reducing fluoride, turbidity and sludge water content. Membrane fouling analysis indicated that UF membrane scaling was attributed to the CaF2 particles deposition at recovery rates of 70%–90%. RO membrane fouling behaviors were identified at recovery rate of 50% (organic fouling), 70% (inorganic scaling occurred and organic fouling) and 80% (inorganic scaling and organic fouling). Meanwhile, UF/RO membrane scaling/fouling could be removed by pure water cleaning (UF) and Na2CO3/NaOH/HCl cleaning (RO). Results of this work shall provide useful information on the application of a precipitation/crystallization/UF/RO system to purify and recover high fluoride-containing wastewater. [Display omitted] ●A new integrated system for fluoride-containing wastewater treatment was developed.●Crystallization process reduced fluoride, turbidity and sludge water content.●UF/RO fouling behaviors were identified along the permeate recovery rates.●Residual fluoride in integrated system effluent qualified WHO standard. |
| ArticleNumber | 131225 |
| Author | Qiu, Yangbo Shao, Jiahui Ren, Long-Fei Xia, Lei Zhao, Yan |
| Author_xml | – sequence: 1 givenname: Yangbo surname: Qiu fullname: Qiu, Yangbo organization: School of Environmental Science and Engineering, Shanghai Jiao Tong University, No. 800 Dongchuan Road, Shanghai, 200240, PR China – sequence: 2 givenname: Long-Fei surname: Ren fullname: Ren, Long-Fei organization: School of Environmental Science and Engineering, Shanghai Jiao Tong University, No. 800 Dongchuan Road, Shanghai, 200240, PR China – sequence: 3 givenname: Jiahui surname: Shao fullname: Shao, Jiahui email: jhshao@sjtu.edu.cn organization: School of Environmental Science and Engineering, Shanghai Jiao Tong University, No. 800 Dongchuan Road, Shanghai, 200240, PR China – sequence: 4 givenname: Lei surname: Xia fullname: Xia, Lei organization: Division of Soil and Water Management, Department of Earth and Environmental Sciences, KU Leuven, Kasteelpark Arenberg 20 Bus 2459, 3001, Leuven, Belgium – sequence: 5 givenname: Yan orcidid: 0000-0003-3660-4669 surname: Zhao fullname: Zhao, Yan organization: Department of Chemical Engineering, KU Leuven, Celestijnenlaan 200F, B-3001, Leuven, Belgium |
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| SubjectTerms | coagulation crystallization flocculation fluorides High fluoride-containing wastewater humans Membrane fouling Precipitation/crystallization/UF/RO system Recovery rate semiconductors sludge turbidity ultrafiltration wastewater wastewater treatment water content World Health Organization |
| Title | An integrated separation technology for high fluoride-containing wastewater treatment: Fluoride removal, membrane fouling behavior and control |
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