Control of growth interface shape using vibroconvective stirring applied to vertical Bridgman growth

The ability of vibroconvective stirring to control the growth interface shape during vertical Bridgman growth was demonstrated using the coupled vibrational stirring (CVS) technique. CVS involves the application of low-frequency vibrations to the outside of the growth ampoule and produces strong flo...

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Published inJournal of crystal growth Vol. 282; no. 1; pp. 236 - 250
Main Authors Zawilski, Kevin T., Custodio, M. Claudia C., DeMattei, Robert C., Feigelson, Robert S.
Format Journal Article
LanguageEnglish
Published Amsterdam Elsevier B.V 15.08.2005
Elsevier
Subjects
A1. Convection
A1. Directional solidification
A1. Fluid flows
A1. Stirring
A2. Bridgman technique
B1. Oxides
Condensed matter: structure, mechanical and thermal properties
Cross-disciplinary physics: materials science; rheology
Exact sciences and technology
Materials science
Mechanical and acoustical properties of condensed matter
Mechanical and elastic waves, vibrations
Methods of crystal growth; physics of crystal growth
Physics
A2. Bridgman technique
A1. Stirring
B1. Oxides
A1. Directional solidification
A1. Convection
A1. Fluid flows
Fluctuations
Inorganic compounds
Growth rate
Lead titanates
Stirring
Growth interface
Transition element compounds
Surfaces
Vibrations
Flow(fluid)
Growth mechanism
Test method
Control method
Lead Niobates
Rate constant
Bridgman method
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Abstract The ability of vibroconvective stirring to control the growth interface shape during vertical Bridgman growth was demonstrated using the coupled vibrational stirring (CVS) technique. CVS involves the application of low-frequency vibrations to the outside of the growth ampoule and produces strong flows emanating from the fluid surface. Previous studies showed that the growth rate and interface shape fluctuations occurred under growth with a constant vibrational frequency. In order to eliminate these fluctuations, this paper examines methods to lower the vibrational frequency as growth progressed to maintain a constant fluid flow rate in the vicinity of the growth interface. These flow control methods were tested on two growth systems: NaNO 3 and lead magnesium niobate–lead titanate (PMNT). The previously observed fluctuations were greatly reduced when flows were appropriately controlled. Using this control method, CVS flows were then applied to reduce the concavity of the growth interface in the NaNO 3 system at fast growth rates (>10 mm/h).
AbstractList The ability of vibroconvective stirring to control the growth interface shape during vertical Bridgman growth was demonstrated using the coupled vibrational stirring (CVS) technique. CVS involves the application of low-frequency vibrations to the outside of the growth ampoule and produces strong flows emanating from the fluid surface. Previous studies showed that the growth rate and interface shape fluctuations occurred under growth with a constant vibrational frequency. In order to eliminate these fluctuations, this paper examines methods to lower the vibrational frequency as growth progressed to maintain a constant fluid flow rate in the vicinity of the growth interface. These flow control methods were tested on two growth systems: NaNO 3 and lead magnesium niobate–lead titanate (PMNT). The previously observed fluctuations were greatly reduced when flows were appropriately controlled. Using this control method, CVS flows were then applied to reduce the concavity of the growth interface in the NaNO 3 system at fast growth rates (>10 mm/h).
Author Feigelson, Robert S.
Custodio, M. Claudia C.
Zawilski, Kevin T.
DeMattei, Robert C.
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crossref_primary_10_1080_18811248_2011_9711813
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Issue 1
Keywords A2. Bridgman technique
A1. Stirring
B1. Oxides
A1. Directional solidification
A1. Convection
A1. Fluid flows
Fluctuations
Inorganic compounds
Growth rate
Lead titanates
Stirring
Growth interface
Transition element compounds
Surfaces
Vibrations
Flow(fluid)
Growth mechanism
Test method
Control method
Lead Niobates
Rate constant
Bridgman method
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Snippet The ability of vibroconvective stirring to control the growth interface shape during vertical Bridgman growth was demonstrated using the coupled vibrational...
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SubjectTerms A1. Convection
A1. Directional solidification
A1. Fluid flows
A1. Stirring
A2. Bridgman technique
B1. Oxides
Condensed matter: structure, mechanical and thermal properties
Cross-disciplinary physics: materials science; rheology
Exact sciences and technology
Materials science
Mechanical and acoustical properties of condensed matter
Mechanical and elastic waves, vibrations
Methods of crystal growth; physics of crystal growth
Physics
Title Control of growth interface shape using vibroconvective stirring applied to vertical Bridgman growth
URI https://dx.doi.org/10.1016/j.jcrysgro.2005.04.084
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