Hydrogen adsorption/absorption on Pd/Pt(1 1 1) multilayers
One to 20 monolayers of Pd were deposited on Pt(1 1 1) and their electrochemical behavior was studied by cyclic voltammetry and impedance spectroscopy. The hydrogen adsorption and absorption is more reversible at deposits on Pt(1 1 1) as compared to Au(1 1 1), probably due to less strain and/or elec...
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| Published in | Journal of electroanalytical chemistry (Lausanne, Switzerland) Vol. 621; no. 1; pp. 62 - 68 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
01.09.2008
Elsevier Science |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1572-6657 1873-2569 |
| DOI | 10.1016/j.jelechem.2008.04.019 |
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| Abstract | One to 20 monolayers of Pd were deposited on Pt(1
1
1) and their electrochemical behavior was studied by cyclic voltammetry and impedance spectroscopy. The hydrogen adsorption and absorption is more reversible at deposits on Pt(1
1
1) as compared to Au(1
1
1), probably due to less strain and/or electronic effects. The quantity of hydrogen adsorbed/absorbed at 10
ML are however comparable at both supports. The charge transfer resistance is lower at 1 Pd ML in perchloric and sulfuric acids than for thicker layers, and it is lower at Pd/Pt(1
1
1) than at Pd/Au(1
1
1). The adsorption pseudocapacitance reaches a maximum at 0.214
V in sulfuric acid for 1
ML and there are two peaks at 0.214
V and 0.255
V for thicker layers. Crystal violet increases the reversibility of hydrogen absorption and inhibits hydrogen adsorption although some residual adsorption remains. |
|---|---|
| AbstractList | One to 20 monolayers of Pd were deposited on Pt(1
1
1) and their electrochemical behavior was studied by cyclic voltammetry and impedance spectroscopy. The hydrogen adsorption and absorption is more reversible at deposits on Pt(1
1
1) as compared to Au(1
1
1), probably due to less strain and/or electronic effects. The quantity of hydrogen adsorbed/absorbed at 10
ML are however comparable at both supports. The charge transfer resistance is lower at 1 Pd ML in perchloric and sulfuric acids than for thicker layers, and it is lower at Pd/Pt(1
1
1) than at Pd/Au(1
1
1). The adsorption pseudocapacitance reaches a maximum at 0.214
V in sulfuric acid for 1
ML and there are two peaks at 0.214
V and 0.255
V for thicker layers. Crystal violet increases the reversibility of hydrogen absorption and inhibits hydrogen adsorption although some residual adsorption remains. |
| Author | Duncan, Hugues Lasia, Andrzej |
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| Keywords | Hydrogen absorption Pd thin layers Kinetics Pt Poison effect Hydrogen adsorption Crystal orientation Hydrogen Basic dye Acidic solution Sulfuric acid Electrodes Cyclic voltammetry Absorption Platinum Inhibition Platinoid Modified material Multilayer Electrode poisoning Triarylmethane dye Transition metal Palladium Single crystal Thickness Perchloric acid Adsorption Medium effect Methylrosanilinium chloride Electrochemical impedance spectroscopy |
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| Snippet | One to 20 monolayers of Pd were deposited on Pt(1
1
1) and their electrochemical behavior was studied by cyclic voltammetry and impedance spectroscopy. The... |
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| SubjectTerms | Chemistry Electrochemistry Electrodes: preparations and properties Exact sciences and technology General and physical chemistry Hydrogen absorption Hydrogen adsorption Kinetics Other electrodes Pd thin layers Poison effect |
| Title | Hydrogen adsorption/absorption on Pd/Pt(1 1 1) multilayers |
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