C-Al2O3 coatings prepared by cathode plasma electrolytic deposition on TC4 substrate for better high temperature oxidation resistance
The Al2O3 coating prepared by cathode plasma electrolytic deposition (CPED) method usually has porous structure, which is not conductive to its application in the field of high temperature oxidation resistance. In this paper, carbon doped Al2O3 (C-Al2O3) coatings were prepared by adding glycerol to...
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| Published in | Surface & coatings technology Vol. 405; p. 126585 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Lausanne
Elsevier B.V
15.01.2021
Elsevier BV |
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| Abstract | The Al2O3 coating prepared by cathode plasma electrolytic deposition (CPED) method usually has porous structure, which is not conductive to its application in the field of high temperature oxidation resistance. In this paper, carbon doped Al2O3 (C-Al2O3) coatings were prepared by adding glycerol to the electrolytes, and coatings with reduced porosity and better high temperature oxidation resistance were obtained. SEM, EDS, XRD, XPS, high temperature oxidation test and first-principles calculation were used to study the structures and performances of the coatings. The results show that by adding glycerol to the electrolytes, the porosity of the obtained coatings is reduced. The doping of carbon (C) causes the XRD peaks of Al2O3 and XPS spectrum of Al2p and O1s.to shift to the left. The decrease in porosity is closely related to the increase in electrical conductivity of the coating caused by the doping of C, which reduces the band-gap of Al2O3. The coating with low C content shows the best high temperature oxidation resistance, while high C content coatings exhibit poorer high temperature oxidation resistance. Related mechanism is disclosed in the paper.
•C-Al2O3 coatings were deposited onto TC4 by CPED using glycerol as carbon source.•The presence of C leaded to a decreased porosity of the coatings.•Coatings with low C content showed the best high temperature oxidation resistance. |
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| AbstractList | The Al2O3 coating prepared by cathode plasma electrolytic deposition (CPED) method usually has porous structure, which is not conductive to its application in the field of high temperature oxidation resistance. In this paper, carbon doped Al2O3 (C-Al2O3) coatings were prepared by adding glycerol to the electrolytes, and coatings with reduced porosity and better high temperature oxidation resistance were obtained. SEM, EDS, XRD, XPS, high temperature oxidation test and first-principles calculation were used to study the structures and performances of the coatings. The results show that by adding glycerol to the electrolytes, the porosity of the obtained coatings is reduced. The doping of carbon (C) causes the XRD peaks of Al2O3 and XPS spectrum of Al2p and O1s.to shift to the left. The decrease in porosity is closely related to the increase in electrical conductivity of the coating caused by the doping of C, which reduces the band-gap of Al2O3. The coating with low C content shows the best high temperature oxidation resistance, while high C content coatings exhibit poorer high temperature oxidation resistance. Related mechanism is disclosed in the paper. The Al2O3 coating prepared by cathode plasma electrolytic deposition (CPED) method usually has porous structure, which is not conductive to its application in the field of high temperature oxidation resistance. In this paper, carbon doped Al2O3 (C-Al2O3) coatings were prepared by adding glycerol to the electrolytes, and coatings with reduced porosity and better high temperature oxidation resistance were obtained. SEM, EDS, XRD, XPS, high temperature oxidation test and first-principles calculation were used to study the structures and performances of the coatings. The results show that by adding glycerol to the electrolytes, the porosity of the obtained coatings is reduced. The doping of carbon (C) causes the XRD peaks of Al2O3 and XPS spectrum of Al2p and O1s.to shift to the left. The decrease in porosity is closely related to the increase in electrical conductivity of the coating caused by the doping of C, which reduces the band-gap of Al2O3. The coating with low C content shows the best high temperature oxidation resistance, while high C content coatings exhibit poorer high temperature oxidation resistance. Related mechanism is disclosed in the paper. •C-Al2O3 coatings were deposited onto TC4 by CPED using glycerol as carbon source.•The presence of C leaded to a decreased porosity of the coatings.•Coatings with low C content showed the best high temperature oxidation resistance. |
| ArticleNumber | 126585 |
| Author | He, Yedong Zhang, Jin Lian, Yong Zhang, Shuguang Zhao, Chao |
| Author_xml | – sequence: 1 givenname: Shuguang surname: Zhang fullname: Zhang, Shuguang – sequence: 2 givenname: Chao surname: Zhao fullname: Zhao, Chao – sequence: 3 givenname: Jin surname: Zhang fullname: Zhang, Jin email: zhangjin@ustb.edu.cn – sequence: 4 givenname: Yong surname: Lian fullname: Lian, Yong – sequence: 5 givenname: Yedong surname: He fullname: He, Yedong |
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| CitedBy_id | crossref_primary_10_1016_j_matchar_2022_112061 crossref_primary_10_1016_j_ijrmhm_2024_106563 crossref_primary_10_1016_j_surfcoat_2022_128719 crossref_primary_10_3390_coatings12050580 crossref_primary_10_1016_j_msea_2023_145967 crossref_primary_10_3390_ma14164567 crossref_primary_10_1016_j_mcat_2023_113407 crossref_primary_10_1016_j_vacuum_2021_110522 crossref_primary_10_1016_j_surfin_2022_102413 crossref_primary_10_1016_j_corcom_2021_10_002 crossref_primary_10_1016_j_ceramint_2023_12_053 crossref_primary_10_1016_j_surfcoat_2022_128127 crossref_primary_10_1109_TPS_2021_3091830 crossref_primary_10_1016_j_fusengdes_2022_113134 |
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| Keywords | Cathode plasma electrolytic deposition Glycerol High temperature oxidation resistance Decrease porosity C-Al2O3 coatings |
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| SubjectTerms | Aluminum oxide C-Al2O3 coatings Carbon Cathode plasma electrolytic deposition Cathodes Cathodic coating (process) Coatings Decrease porosity Doping Electrical resistivity Electrodeposition Electrolytes First principles Glycerol High temperature High temperature oxidation resistance Oxidation Oxidation resistance Oxidation tests Porosity Substrates X ray photoelectron spectroscopy |
| Title | C-Al2O3 coatings prepared by cathode plasma electrolytic deposition on TC4 substrate for better high temperature oxidation resistance |
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