Morphology, composition and selectivity of nickel/titanium oxide nanoflakes grown on a superelastic nickel/titanium alloy fiber substrate for highly efficient solid-phase microextraction of aromatic compounds

Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes (NiO/TiO 2 NFs) was carried out on superelastic nickel/titanium alloy (NiTi) wires for solid-phase microextraction. The resulting fiber coatings were characterized by scanning electron microscopy and energy dispersive X-ray spect...

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Published in	Analytical methods Vol. 11; no. 9; pp. 1237 - 1247
Main Authors	Du, Junliang, Wang, Feifei, Wang, Zhuo, Wang, Xuemei, Du, Xinzhen
Format	Journal Article
Language	English
Published	Cambridge Royal Society of Chemistry 28.02.2019
Subjects	alloys Aromatic compounds Chemical composition Coatings Composition Correlation coefficient Correlation coefficients detection limit elemental composition Energy dispersive X ray spectroscopy energy-dispersive X-ray analysis Fiber coatings Fibers High performance liquid chromatography Hydrothermal reactions Intermetallic compounds Liquid chromatography Morphology Nickel Nickel base alloys nickel oxide Nickel oxides Nickel titanides Polycyclic aromatic hydrocarbons Recyclability Reproducibility Scanning electron microscopy Selectivity Sodium hydroxide Solid phase methods solid phase microextraction Solid phases Stability Substrates Titanium Titanium alloys Titanium base alloys titanium dioxide Titanium oxide Titanium oxides Ultraviolet radiation Water analysis Water sampling X-ray spectroscopy
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Abstract	Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes (NiO/TiO 2 NFs) was carried out on superelastic nickel/titanium alloy (NiTi) wires for solid-phase microextraction. The resulting fiber coatings were characterized by scanning electron microscopy and energy dispersive X-ray spectroscopy. Control of the NaOH concentration was found to be an effective route to manipulate the morphology and composition of NiO-based nanoflakes grown on the NiTi fiber substrates via a hydrothermal reaction. At higher concentrations of NaOH, pristine NiO nanoflakes (NiONFs) were in situ grown on the NiTi fiber substrates for the first time. Their extraction performance was evaluated using typical aromatic compounds by high-performance liquid chromatography with UV detection. The results clearly demonstrate that the extraction selectivity is subject to the surface elemental composition of the nanoflake coatings and the extraction capability greatly depends on their surface morphology. In view of the good extraction selectivity of the NiONF coating for the selected polycyclic aromatic hydrocarbons (PAHs), the key experimental parameters were optimized. Under the optimum conditions, the calibration curves were linear in the range of 0.05-100 μg L −1 with correlation coefficients greater than 0.999. Limits of detection were 0.009-0.036 μg L −1 . Furthermore, the intra-day and inter-day repeatability of the proposed method with the single fiber varied from 3.7% to 5.3% and from 5.4% to 5.8%, respectively. The fiber-to-fiber reproducibility ranged from 5.8% to 8.6%. The proposed method was suitable for selective enrichment and determination of target PAHs from real water samples. Moreover, the fabricated fibers showed precisely controllable growth of NiONFs and a long-term recyclability of 150 cycles. Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes was carried out on superelastic nickel/titanium alloy wires for solid-phase microextraction.
AbstractList	Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes (NiO/TiO 2 NFs) was carried out on superelastic nickel/titanium alloy (NiTi) wires for solid-phase microextraction. The resulting fiber coatings were characterized by scanning electron microscopy and energy dispersive X-ray spectroscopy. Control of the NaOH concentration was found to be an effective route to manipulate the morphology and composition of NiO-based nanoflakes grown on the NiTi fiber substrates via a hydrothermal reaction. At higher concentrations of NaOH, pristine NiO nanoflakes (NiONFs) were in situ grown on the NiTi fiber substrates for the first time. Their extraction performance was evaluated using typical aromatic compounds by high-performance liquid chromatography with UV detection. The results clearly demonstrate that the extraction selectivity is subject to the surface elemental composition of the nanoflake coatings and the extraction capability greatly depends on their surface morphology. In view of the good extraction selectivity of the NiONF coating for the selected polycyclic aromatic hydrocarbons (PAHs), the key experimental parameters were optimized. Under the optimum conditions, the calibration curves were linear in the range of 0.05-100 μg L −1 with correlation coefficients greater than 0.999. Limits of detection were 0.009-0.036 μg L −1 . Furthermore, the intra-day and inter-day repeatability of the proposed method with the single fiber varied from 3.7% to 5.3% and from 5.4% to 5.8%, respectively. The fiber-to-fiber reproducibility ranged from 5.8% to 8.6%. The proposed method was suitable for selective enrichment and determination of target PAHs from real water samples. Moreover, the fabricated fibers showed precisely controllable growth of NiONFs and a long-term recyclability of 150 cycles. Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes was carried out on superelastic nickel/titanium alloy wires for solid-phase microextraction. Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes (NiO/TiO 2 NFs) was carried out on superelastic nickel/titanium alloy (NiTi) wires for solid-phase microextraction. The resulting fiber coatings were characterized by scanning electron microscopy and energy dispersive X-ray spectroscopy. Control of the NaOH concentration was found to be an effective route to manipulate the morphology and composition of NiO-based nanoflakes grown on the NiTi fiber substrates via a hydrothermal reaction. At higher concentrations of NaOH, pristine NiO nanoflakes (NiONFs) were in situ grown on the NiTi fiber substrates for the first time. Their extraction performance was evaluated using typical aromatic compounds by high-performance liquid chromatography with UV detection. The results clearly demonstrate that the extraction selectivity is subject to the surface elemental composition of the nanoflake coatings and the extraction capability greatly depends on their surface morphology. In view of the good extraction selectivity of the NiONF coating for the selected polycyclic aromatic hydrocarbons (PAHs), the key experimental parameters were optimized. Under the optimum conditions, the calibration curves were linear in the range of 0.05–100 μg L −1 with correlation coefficients greater than 0.999. Limits of detection were 0.009–0.036 μg L −1 . Furthermore, the intra-day and inter-day repeatability of the proposed method with the single fiber varied from 3.7% to 5.3% and from 5.4% to 5.8%, respectively. The fiber-to-fiber reproducibility ranged from 5.8% to 8.6%. The proposed method was suitable for selective enrichment and determination of target PAHs from real water samples. Moreover, the fabricated fibers showed precisely controllable growth of NiONFs and a long-term recyclability of 150 cycles. Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes (NiO/TiO2NFs) was carried out on superelastic nickel/titanium alloy (NiTi) wires for solid-phase microextraction. The resulting fiber coatings were characterized by scanning electron microscopy and energy dispersive X-ray spectroscopy. Control of the NaOH concentration was found to be an effective route to manipulate the morphology and composition of NiO-based nanoflakes grown on the NiTi fiber substrates via a hydrothermal reaction. At higher concentrations of NaOH, pristine NiO nanoflakes (NiONFs) were in situ grown on the NiTi fiber substrates for the first time. Their extraction performance was evaluated using typical aromatic compounds by high-performance liquid chromatography with UV detection. The results clearly demonstrate that the extraction selectivity is subject to the surface elemental composition of the nanoflake coatings and the extraction capability greatly depends on their surface morphology. In view of the good extraction selectivity of the NiONF coating for the selected polycyclic aromatic hydrocarbons (PAHs), the key experimental parameters were optimized. Under the optimum conditions, the calibration curves were linear in the range of 0.05–100 μg L−1 with correlation coefficients greater than 0.999. Limits of detection were 0.009–0.036 μg L−1. Furthermore, the intra-day and inter-day repeatability of the proposed method with the single fiber varied from 3.7% to 5.3% and from 5.4% to 5.8%, respectively. The fiber-to-fiber reproducibility ranged from 5.8% to 8.6%. The proposed method was suitable for selective enrichment and determination of target PAHs from real water samples. Moreover, the fabricated fibers showed precisely controllable growth of NiONFs and a long-term recyclability of 150 cycles. Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes (NiO/TiO₂NFs) was carried out on superelastic nickel/titanium alloy (NiTi) wires for solid-phase microextraction. The resulting fiber coatings were characterized by scanning electron microscopy and energy dispersive X-ray spectroscopy. Control of the NaOH concentration was found to be an effective route to manipulate the morphology and composition of NiO-based nanoflakes grown on the NiTi fiber substrates via a hydrothermal reaction. At higher concentrations of NaOH, pristine NiO nanoflakes (NiONFs) were in situ grown on the NiTi fiber substrates for the first time. Their extraction performance was evaluated using typical aromatic compounds by high-performance liquid chromatography with UV detection. The results clearly demonstrate that the extraction selectivity is subject to the surface elemental composition of the nanoflake coatings and the extraction capability greatly depends on their surface morphology. In view of the good extraction selectivity of the NiONF coating for the selected polycyclic aromatic hydrocarbons (PAHs), the key experimental parameters were optimized. Under the optimum conditions, the calibration curves were linear in the range of 0.05–100 μg L⁻¹ with correlation coefficients greater than 0.999. Limits of detection were 0.009–0.036 μg L⁻¹. Furthermore, the intra-day and inter-day repeatability of the proposed method with the single fiber varied from 3.7% to 5.3% and from 5.4% to 5.8%, respectively. The fiber-to-fiber reproducibility ranged from 5.8% to 8.6%. The proposed method was suitable for selective enrichment and determination of target PAHs from real water samples. Moreover, the fabricated fibers showed precisely controllable growth of NiONFs and a long-term recyclability of 150 cycles.
Author	Wang, Feifei Du, Junliang Wang, Xuemei Wang, Zhuo Du, Xinzhen
AuthorAffiliation	College of Chemistry and Chemical Engineering Northwest Normal University Department of Chemistry and Chemical Engineering Mianyang Normal University
AuthorAffiliation_xml	– name: College of Chemistry and Chemical Engineering – name: Department of Chemistry and Chemical Engineering – name: Mianyang Normal University – name: Northwest Normal University
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Snippet	Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes (NiO/TiO 2 NFs) was carried out on superelastic nickel/titanium alloy (NiTi) wires for... Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes (NiO/TiO2NFs) was carried out on superelastic nickel/titanium alloy (NiTi) wires for... Direct in situ hydrothermal growth of nickel/titanium oxide nanoflakes (NiO/TiO₂NFs) was carried out on superelastic nickel/titanium alloy (NiTi) wires for...
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SubjectTerms	alloys Aromatic compounds Chemical composition Coatings Composition Correlation coefficient Correlation coefficients detection limit elemental composition Energy dispersive X ray spectroscopy energy-dispersive X-ray analysis Fiber coatings Fibers High performance liquid chromatography Hydrothermal reactions Intermetallic compounds Liquid chromatography Morphology Nickel Nickel base alloys nickel oxide Nickel oxides Nickel titanides Polycyclic aromatic hydrocarbons Recyclability Reproducibility Scanning electron microscopy Selectivity Sodium hydroxide Solid phase methods solid phase microextraction Solid phases Stability Substrates Titanium Titanium alloys Titanium base alloys titanium dioxide Titanium oxide Titanium oxides Ultraviolet radiation Water analysis Water sampling X-ray spectroscopy
Title	Morphology, composition and selectivity of nickel/titanium oxide nanoflakes grown on a superelastic nickel/titanium alloy fiber substrate for highly efficient solid-phase microextraction of aromatic compounds
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