Alloying behavior and deformation twinning in a CoNiFeCrAl0.6Ti0.4 high entropy alloy processed by spark plasma sintering
► CoNiFeCrAl0.6Ti0.4 high entropy alloy has been synthesized via MA and SPS. ► Deformation twinning possibly occurred during MA or SPS. ► This alloy exhibits excellent mechanical properties. ► The fracture mechanism of this alloy is intergranular fracture and plastic fracture. Inequi-atomic CoNiFeCr...
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| Published in | Journal of alloys and compounds Vol. 553; pp. 316 - 323 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Kidlington
Elsevier B.V
15.03.2013
Elsevier |
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| Abstract | ► CoNiFeCrAl0.6Ti0.4 high entropy alloy has been synthesized via MA and SPS. ► Deformation twinning possibly occurred during MA or SPS. ► This alloy exhibits excellent mechanical properties. ► The fracture mechanism of this alloy is intergranular fracture and plastic fracture.
Inequi-atomic CoNiFeCrAl0.6Ti0.4 high entropy alloy has been designed and fabricated by mechanical alloying (MA) and spark plasma sintering (SPS). Alloying behavior, microstructure, phase evolution and mechanical properties of CoNiFeCrAl0.6Ti0.4 alloy were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscope (TEM), as well as by an Instron testing system. During MA, a supersaturated solid solution consisting of a FCC phase and a metastable BCC phase was formed. Two FCC phases (named FCC1 and FCC2) and a new BCC phase were observed after SPS. During SPS, the metastable BCC phase transformed into the FCC2 phase and the new BCC phase. Meanwhile, the FCC1 phase was the initial FCC phase which was formed during MA. Moreover, nanoscale twins obviously presented only in partial FCC1 phase after SPS. Deformation twinning may be occurred during MA or SPS. The sintered alloy with a high relative density of 98.83% exhibits excellent comprehensive mechanical properties. The yield stress, compressive strength, compression ratio and Vickers hardness of the alloy are 2.08, 2.52GPa, 11.5% and 573 HV, respectively. The fracture mechanism of CoNiFeCrAl0.6Ti0.4 high entropy alloy is mainly performed at intergranular fracture and plastic fracture mode. |
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| AbstractList | Inequi-atomic CoNiFeCrAl0.6Ti0.4 high entropy alloy has been designed and fabricated by mechanical alloying (MA) and spark plasma sintering (SPS). Alloying behavior, microstructure, phase evolution and mechanical properties of CoNiFeCrAl0.6Ti0.4 alloy were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscope (TEM), as well as by an Instron testing system. During MA, a supersaturated solid solution consisting of a FCC phase and a metastable BCC phase was formed. Two FCC phases (named FCC1 and FCC2) and a new BCC phase were observed after SPS. During SPS, the metastable BCC phase transformed into the FCC2 phase and the new BCC phase. Meanwhile, the FCC1 phase was the initial FCC phase which was formed during MA. Moreover, nanoscale twins obviously presented only in partial FCC1 phase after SPS. Deformation twinning may be occurred during MA or SPS. The sintered alloy with a high relative density of 98.83% exhibits excellent comprehensive mechanical properties. The yield stress, compressive strength, compression ratio and Vickers hardness of the alloy are 2.08, 2.52 GPa, 11.5% and 573 HV, respectively. The fracture mechanism of CoNiFeCrAl0.6Ti0.4 high entropy alloy is mainly performed at intergranular fracture and plastic fracture mode. ► CoNiFeCrAl0.6Ti0.4 high entropy alloy has been synthesized via MA and SPS. ► Deformation twinning possibly occurred during MA or SPS. ► This alloy exhibits excellent mechanical properties. ► The fracture mechanism of this alloy is intergranular fracture and plastic fracture. Inequi-atomic CoNiFeCrAl0.6Ti0.4 high entropy alloy has been designed and fabricated by mechanical alloying (MA) and spark plasma sintering (SPS). Alloying behavior, microstructure, phase evolution and mechanical properties of CoNiFeCrAl0.6Ti0.4 alloy were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscope (TEM), as well as by an Instron testing system. During MA, a supersaturated solid solution consisting of a FCC phase and a metastable BCC phase was formed. Two FCC phases (named FCC1 and FCC2) and a new BCC phase were observed after SPS. During SPS, the metastable BCC phase transformed into the FCC2 phase and the new BCC phase. Meanwhile, the FCC1 phase was the initial FCC phase which was formed during MA. Moreover, nanoscale twins obviously presented only in partial FCC1 phase after SPS. Deformation twinning may be occurred during MA or SPS. The sintered alloy with a high relative density of 98.83% exhibits excellent comprehensive mechanical properties. The yield stress, compressive strength, compression ratio and Vickers hardness of the alloy are 2.08, 2.52GPa, 11.5% and 573 HV, respectively. The fracture mechanism of CoNiFeCrAl0.6Ti0.4 high entropy alloy is mainly performed at intergranular fracture and plastic fracture mode. |
| Author | Chen, Weiping Fu, Zhiqiang Zhu, Dezhi Fang, Sicong Zhang, Dayue Xiao, Huaqiang |
| Author_xml | – sequence: 1 givenname: Zhiqiang surname: Fu fullname: Fu, Zhiqiang email: kopyhit@163.com organization: School of Mechanical and Automotive Engineering, South China University of Technology, Guangzhou, Guangdong 510640, China – sequence: 2 givenname: Weiping surname: Chen fullname: Chen, Weiping organization: School of Mechanical and Automotive Engineering, South China University of Technology, Guangzhou, Guangdong 510640, China – sequence: 3 givenname: Sicong surname: Fang fullname: Fang, Sicong organization: School of Mechanical and Automotive Engineering, South China University of Technology, Guangzhou, Guangdong 510640, China – sequence: 4 givenname: Dayue surname: Zhang fullname: Zhang, Dayue organization: School of Metallurgy and Materials, University of Birmingham, Edgbaston, Birmingham B15 2TT, United Kingdom – sequence: 5 givenname: Huaqiang surname: Xiao fullname: Xiao, Huaqiang organization: School of Mechanical and Automotive Engineering, South China University of Technology, Guangzhou, Guangdong 510640, China – sequence: 6 givenname: Dezhi surname: Zhu fullname: Zhu, Dezhi organization: School of Mechanical and Automotive Engineering, South China University of Technology, Guangzhou, Guangdong 510640, China |
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| Keywords | High entropy alloys Deformation twinning Spark plasma sintering Mechanical alloying high entropy alloy Scanning electron microscopy Nanodefect Mechanical twin Aluminium alloy X ray diffraction Intergranular fracture Tensile strength Metastable phase Phase transformation Plasticity Yield strength Microstructure Supersaturated solid solution Fracture mode |
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| Snippet | ► CoNiFeCrAl0.6Ti0.4 high entropy alloy has been synthesized via MA and SPS. ► Deformation twinning possibly occurred during MA or SPS. ► This alloy exhibits... Inequi-atomic CoNiFeCrAl0.6Ti0.4 high entropy alloy has been designed and fabricated by mechanical alloying (MA) and spark plasma sintering (SPS). Alloying... |
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| SubjectTerms | Alloy systems Alloying Applied sciences Body centered cubic lattice Condensed matter: structure, mechanical and thermal properties Deformation twinning Elasticity. Plasticity Entropy Exact sciences and technology Fatigue, brittleness, fracture, and cracks High entropy alloys Mechanical alloying Mechanical and acoustical properties of condensed matter Mechanical properties and methods of testing. Rheology. Fracture mechanics. Tribology Mechanical properties of solids Metals. Metallurgy Nanostructure Phase transformations Physics Scanning electron microscopy Spark plasma sintering |
| Title | Alloying behavior and deformation twinning in a CoNiFeCrAl0.6Ti0.4 high entropy alloy processed by spark plasma sintering |
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