Ultrathin polyamide nanofiltration membranes with tunable chargeability for multivalent cation removal
Positively charged nanofiltration membranes are promising in water softening and heavy metal ion removal. However, facile modulation on their chargeability remains a great challenge. Here, we proposed a charged-monomer-engineered interfacial polymerization toward positively charged polyamide membran...
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| Published in | Journal of membrane science Vol. 642; p. 119971 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.02.2022
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Positively charged nanofiltration membranes are promising in water softening and heavy metal ion removal. However, facile modulation on their chargeability remains a great challenge. Here, we proposed a charged-monomer-engineered interfacial polymerization toward positively charged polyamide membranes. In particular, branched amino macromolecules (BAMs) with different charged group numbers and molecular sizes were selected as aqueous monomers, allowing for wide-range-tunable membrane chargeability. We found that larger BAMs tend to form intramolecularly crosslinked networks with more amino residues, conferring membrane chargeability up to +5.53 mC m−2. Besides, the slower diffusion of larger BAMs also led to ultrathin membranes down to 9.0 nm in thickness. The optimal composite nanofiltration membrane displayed a high rejection to multivalent cations (e.g., MgCl2 rejection of 98.7%) with ultrahigh pure water permeance of 31.5 L m−2 h−1 bar−1, which was around 2–10 times higher than that of the reported positively charged nanofiltration membranes. Our monomer design strategy for interfacial polymerization may evolve into a facile approach to constructing advanced charged membranes.
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•Ultrathin positively charged polyamide membranes were made by IP process.•The membrane chargeability was tuned by unreacted amino groups in PEI molecules.•The membrane thickness was reduced by decreasing the diffusion rate of PEI in IP.•The membrane exhibits 31.5 (L m−2 h−1 bar −1) water flux, 98.7% MgCl2 rejection. |
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| AbstractList | Positively charged nanofiltration membranes are promising in water softening and heavy metal ion removal. However, facile modulation on their chargeability remains a great challenge. Here, we proposed a charged-monomer-engineered interfacial polymerization toward positively charged polyamide membranes. In particular, branched amino macromolecules (BAMs) with different charged group numbers and molecular sizes were selected as aqueous monomers, allowing for wide-range-tunable membrane chargeability. We found that larger BAMs tend to form intramolecularly crosslinked networks with more amino residues, conferring membrane chargeability up to +5.53 mC m−2. Besides, the slower diffusion of larger BAMs also led to ultrathin membranes down to 9.0 nm in thickness. The optimal composite nanofiltration membrane displayed a high rejection to multivalent cations (e.g., MgCl2 rejection of 98.7%) with ultrahigh pure water permeance of 31.5 L m−2 h−1 bar−1, which was around 2–10 times higher than that of the reported positively charged nanofiltration membranes. Our monomer design strategy for interfacial polymerization may evolve into a facile approach to constructing advanced charged membranes.
[Display omitted]
•Ultrathin positively charged polyamide membranes were made by IP process.•The membrane chargeability was tuned by unreacted amino groups in PEI molecules.•The membrane thickness was reduced by decreasing the diffusion rate of PEI in IP.•The membrane exhibits 31.5 (L m−2 h−1 bar −1) water flux, 98.7% MgCl2 rejection. Positively charged nanofiltration membranes are promising in water softening and heavy metal ion removal. However, facile modulation on their chargeability remains a great challenge. Here, we proposed a charged-monomer-engineered interfacial polymerization toward positively charged polyamide membranes. In particular, branched amino macromolecules (BAMs) with different charged group numbers and molecular sizes were selected as aqueous monomers, allowing for wide-range-tunable membrane chargeability. We found that larger BAMs tend to form intramolecularly crosslinked networks with more amino residues, conferring membrane chargeability up to +5.53 mC m⁻². Besides, the slower diffusion of larger BAMs also led to ultrathin membranes down to 9.0 nm in thickness. The optimal composite nanofiltration membrane displayed a high rejection to multivalent cations (e.g., MgCl₂ rejection of 98.7%) with ultrahigh pure water permeance of 31.5 L m⁻² h⁻¹ bar⁻¹, which was around 2–10 times higher than that of the reported positively charged nanofiltration membranes. Our monomer design strategy for interfacial polymerization may evolve into a facile approach to constructing advanced charged membranes. |
| ArticleNumber | 119971 |
| Author | You, Xinda Li, Wenwen Li, Ya Wang, Zhen Shen, Jianliang Zhang, Runnan Jiang, Zhongyi Yang, Chao Su, Yanlei Li, Yafei |
| Author_xml | – sequence: 1 givenname: Zhen surname: Wang fullname: Wang, Zhen email: 17806242156@163.com organization: Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin, 300072, China – sequence: 2 givenname: Xinda surname: You fullname: You, Xinda email: xindayou@tju.edu.cn organization: Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin, 300072, China – sequence: 3 givenname: Chao orcidid: 0000-0002-5328-0355 surname: Yang fullname: Yang, Chao email: chaoyang@tju.edu.cn organization: Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin, 300072, China – sequence: 4 givenname: Wenwen surname: Li fullname: Li, Wenwen email: liwenwen@tju.edu.cn organization: Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin, 300072, China – sequence: 5 givenname: Yafei surname: Li fullname: Li, Yafei email: liyafei@gmail.com organization: Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin, 300072, China – sequence: 6 givenname: Ya surname: Li fullname: Li, Ya email: liya0822@tju.edu.cn organization: Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin, 300072, China – sequence: 7 givenname: Jianliang surname: Shen fullname: Shen, Jianliang email: shenjianliang@tju.edu.cn organization: Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin, 300072, China – sequence: 8 givenname: Runnan surname: Zhang fullname: Zhang, Runnan email: runnan.zhang@tju.edu.cn organization: Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin, 300072, China – sequence: 9 givenname: Yanlei surname: Su fullname: Su, Yanlei email: suyanlei@tju.edu.cn organization: Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin, 300072, China – sequence: 10 givenname: Zhongyi orcidid: 0000-0002-3813-9943 surname: Jiang fullname: Jiang, Zhongyi email: zhyjiang@tju.edu.cn organization: Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin, 300072, China |
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| Keywords | Ultrathin polyamide nanofilms Polyethyleneimine Interfacial polymerization Nanofiltration Positive charge |
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| Snippet | Positively charged nanofiltration membranes are promising in water softening and heavy metal ion removal. However, facile modulation on their chargeability... |
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| SubjectTerms | branched chain amino acids cation-exchange membranes electrical charges heavy metals Interfacial polymerization magnesium chloride metal ions nanocomposites Nanofiltration polyamides Polyethyleneimine polymerization Positive charge Ultrathin polyamide nanofilms water purification |
| Title | Ultrathin polyamide nanofiltration membranes with tunable chargeability for multivalent cation removal |
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