Structure of [Et 4N] 2[Mo 2(CO) 8(μ-SPh) 2] and structural chemistry of dinuclear molybdenum(0,I) carbonyl complexes containing thiolato bridges
The crystal and molecular structure of the dinuclear molybdenum(O) carbonyl complex containing thiophenyl bridges, [Et 4N] 2[Mo 2(CO) 8(μ-SPh) 2] ( 1) was determined from three-dimensional X-ray data. 1 crystallizes in the triclinic, space group P 1 with a=9.841(2), b=9.921(4), c=11.848(2) Å; α= 81....
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Published in | Inorganica Chimica Acta Vol. 157; no. 1; pp. 85 - 90 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
Published |
Lausanne
Elsevier B.V
01.03.1989
Elsevier Science |
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Abstract | The crystal and molecular structure of the dinuclear molybdenum(O) carbonyl complex containing thiophenyl bridges, [Et
4N]
2[Mo
2(CO)
8(μ-SPh)
2] (
1) was determined from three-dimensional X-ray data.
1 crystallizes in the triclinic, space group
P
1
with
a=9.841(2),
b=9.921(4),
c=11.848(2) Å; α= 81.80(3)°, β=85.64(2)°, γ=82.06(3)°;
V=1038.9- (6) Å
3;
Z=1;
R=0.068 for 3228 independent reflections with
I⩾3σ(
I). A planar MoS
2Mo bimetallic framework with a large Mo…Mo distance of 4.069- (1)·Å which obviously indicates the absence of MoMo bonding was contained in the centrosymmetric structure of the anion of
1, [Mo
2(CO)
8(μ- SPh)
2]
2−. Studying the structure of
1 and comparing
1 with [Et
4N]
2[Mo
2(CO)
8(μ-SCH
2CO
2Et)
2] (
2), Mo
2(CO)
8(μ-SCH
2CO
2Et)
2 (
3), Mo
2(CO)
6(μ-SCH
2- CO
2Et)
2(MeCN)
2 (
4) and Mo
2(CO)
6(μ-SPh)
2(Me- CN)
2 (
5), the structural chemistry of dinuclear molybdenum(O,I) carbonyl complexes containing thiolato bridges and the relevance to their properties and electrochemistry were discussed. |
---|---|
AbstractList | The crystal and molecular structure of the dinuclear molybdenum(O) carbonyl complex containing thiophenyl bridges, [Et
4N]
2[Mo
2(CO)
8(μ-SPh)
2] (
1) was determined from three-dimensional X-ray data.
1 crystallizes in the triclinic, space group
P
1
with
a=9.841(2),
b=9.921(4),
c=11.848(2) Å; α= 81.80(3)°, β=85.64(2)°, γ=82.06(3)°;
V=1038.9- (6) Å
3;
Z=1;
R=0.068 for 3228 independent reflections with
I⩾3σ(
I). A planar MoS
2Mo bimetallic framework with a large Mo…Mo distance of 4.069- (1)·Å which obviously indicates the absence of MoMo bonding was contained in the centrosymmetric structure of the anion of
1, [Mo
2(CO)
8(μ- SPh)
2]
2−. Studying the structure of
1 and comparing
1 with [Et
4N]
2[Mo
2(CO)
8(μ-SCH
2CO
2Et)
2] (
2), Mo
2(CO)
8(μ-SCH
2CO
2Et)
2 (
3), Mo
2(CO)
6(μ-SCH
2- CO
2Et)
2(MeCN)
2 (
4) and Mo
2(CO)
6(μ-SPh)
2(Me- CN)
2 (
5), the structural chemistry of dinuclear molybdenum(O,I) carbonyl complexes containing thiolato bridges and the relevance to their properties and electrochemistry were discussed. |
Author | Jiaxi, Lu Botao, Zhuang Liangren, Huang Yu, Yang Lingjie, He |
Author_xml | – sequence: 1 givenname: Zhuang surname: Botao fullname: Botao, Zhuang – sequence: 2 givenname: Huang surname: Liangren fullname: Liangren, Huang – sequence: 3 givenname: He surname: Lingjie fullname: Lingjie, He – sequence: 4 givenname: Yang surname: Yu fullname: Yu, Yang – sequence: 5 givenname: Lu surname: Jiaxi fullname: Jiaxi, Lu |
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CitedBy_id | crossref_primary_10_1016_S0277_5387_00_86648_6 crossref_primary_10_1002_chin_198922072 crossref_primary_10_1021_ic100186v crossref_primary_10_1016_0277_5387_96_00009_5 crossref_primary_10_1016_S0020_1693_00_83198_9 crossref_primary_10_1016_S0020_1693_00_83129_1 crossref_primary_10_1016_0022_0728_91_85364_U crossref_primary_10_1002_cjoc_20000180516 crossref_primary_10_1016_S0277_5387_00_83270_2 crossref_primary_10_1080_00958979308022749 crossref_primary_10_1016_S0020_1693_00_80591_5 crossref_primary_10_1016_S0020_1693_00_85982_4 crossref_primary_10_1016_S0277_5387_00_84744_0 crossref_primary_10_1016_S0022_328X_01_01173_1 crossref_primary_10_1016_j_jorganchem_2006_11_027 crossref_primary_10_1016_S0277_5387_00_83578_0 |
Cites_doi | 10.1007/BFb0111303 10.1039/cs9811000455 10.1002/cjoc.19860040403 10.1016/S0022-328X(00)98528-0 10.1021/ic00204a035 10.1016/0010-8545(87)85003-8 10.1021/ja00401a018 10.1021/ja00534a001 10.1016/S0020-1693(00)88350-4 10.1021/ja00894a010 10.1021/om00084a025 10.1021/ja00509a021 10.1002/anie.198507421 10.1021/ja00363a059 10.1021/ja00402a054 10.1021/ic00262a036 10.1016/S0277-5387(00)84934-7 10.1021/ic00161a001 10.1016/S0277-5387(00)84307-7 10.1021/ja00516a013 10.1016/S0020-1693(00)82155-6 10.1016/0022-328X(85)88027-X 10.1021/ja00728a041 10.1021/ic00131a029 |
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Copyright | 1989 1991 INIST-CNRS |
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Issue | 1 |
Keywords | Organic cation Molecular structure Organic ligand Transition metal Carbonyl Complexes Zerovalent metal Complexes Experimental study X ray diffraction Quaternary ammonium compound Molybdenum Carbonyl Complexes Mu complex Dinuclear complex Benzenic compound Crystalline structure |
Language | English |
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Snippet | The crystal and molecular structure of the dinuclear molybdenum(O) carbonyl complex containing thiophenyl bridges, [Et
4N]
2[Mo
2(CO)
8(μ-SPh)
2] (
1) was... |
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StartPage | 85 |
SubjectTerms | Carbonyl and nitrosyl compounds, and their complexes Condensed matter: structure, mechanical and thermal properties Exact sciences and technology Inorganic compounds Physics Structure of solids and liquids; crystallography Structure of specific crystalline solids |
Title | Structure of [Et 4N] 2[Mo 2(CO) 8(μ-SPh) 2] and structural chemistry of dinuclear molybdenum(0,I) carbonyl complexes containing thiolato bridges |
URI | https://dx.doi.org/10.1016/S0020-1693(00)83427-1 |
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