N-doped porous carbon derived from macadamia nut shell for CO2 adsorption
Selective adsorption and converting CO2 upon efficient solid-based adsorbents is critical for net-zero accomplishment. Herein, we develop an advisable strategy to prepare nitrogen-enriched porous carbons using the macadamia nutshell (MNS) as a carbon precursor, KOH as the activator and melamine as t...
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| Published in | Fuel processing technology Vol. 249; p. 107854 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.10.2023
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0378-3820 |
| DOI | 10.1016/j.fuproc.2023.107854 |
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| Abstract | Selective adsorption and converting CO2 upon efficient solid-based adsorbents is critical for net-zero accomplishment. Herein, we develop an advisable strategy to prepare nitrogen-enriched porous carbons using the macadamia nutshell (MNS) as a carbon precursor, KOH as the activator and melamine as the nitrogen agent, respectively. The as-prepared porous carbons exhibit an enhanced specific surface area of 1731 m2/g and high microporosity with abundant nitrogen functional groups and structural defects. The CO2 uptake of 6.61 and 4.35 mmol g−1 were achieved at 0 and 25 °C, respectively, under 1 bar. More importantly, these biomass-based nitrogen-doped carbons possess various CO2 adsorption merits such as quick adsorption kinetics, high CO2/N2 selectivity, medium heat of adsorption, outstanding uninterrupted recyclability and good dynamic CO2 capture capacity. The present study provides an advanced protocol to design nitrogen-doped porous Carbon via a facile route toward the capture of CO2, which offers excellent progress in sustainable chemistry and engineering.
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•N-doped porous carbons were synthesized from biomass waste.•Macadamia nut shell as the precursor, melamine as the N source, KOH as the activator.•The obtained carbon exhibits high CO2 adsorption capacity, 6.61 mmol g−1 at 0 °C and 1 bar.•The adsorbents also possess many good CO2 adsorption properties.•Synergetic effect of narrow microporosity and N functionalities determines CO2 uptake. |
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| AbstractList | Selective adsorption and converting CO2 upon efficient solid-based adsorbents is critical for net-zero accomplishment. Herein, we develop an advisable strategy to prepare nitrogen-enriched porous carbons using the macadamia nutshell (MNS) as a carbon precursor, KOH as the activator and melamine as the nitrogen agent, respectively. The as-prepared porous carbons exhibit an enhanced specific surface area of 1731 m2/g and high microporosity with abundant nitrogen functional groups and structural defects. The CO2 uptake of 6.61 and 4.35 mmol g−1 were achieved at 0 and 25 °C, respectively, under 1 bar. More importantly, these biomass-based nitrogen-doped carbons possess various CO2 adsorption merits such as quick adsorption kinetics, high CO2/N2 selectivity, medium heat of adsorption, outstanding uninterrupted recyclability and good dynamic CO2 capture capacity. The present study provides an advanced protocol to design nitrogen-doped porous Carbon via a facile route toward the capture of CO2, which offers excellent progress in sustainable chemistry and engineering.
[Display omitted]
•N-doped porous carbons were synthesized from biomass waste.•Macadamia nut shell as the precursor, melamine as the N source, KOH as the activator.•The obtained carbon exhibits high CO2 adsorption capacity, 6.61 mmol g−1 at 0 °C and 1 bar.•The adsorbents also possess many good CO2 adsorption properties.•Synergetic effect of narrow microporosity and N functionalities determines CO2 uptake. Selective adsorption and converting CO₂ upon efficient solid-based adsorbents is critical for net-zero accomplishment. Herein, we develop an advisable strategy to prepare nitrogen-enriched porous carbons using the macadamia nutshell (MNS) as a carbon precursor, KOH as the activator and melamine as the nitrogen agent, respectively. The as-prepared porous carbons exhibit an enhanced specific surface area of 1731 m²/g and high microporosity with abundant nitrogen functional groups and structural defects. The CO₂ uptake of 6.61 and 4.35 mmol g⁻¹ were achieved at 0 and 25 °C, respectively, under 1 bar. More importantly, these biomass-based nitrogen-doped carbons possess various CO₂ adsorption merits such as quick adsorption kinetics, high CO₂/N₂ selectivity, medium heat of adsorption, outstanding uninterrupted recyclability and good dynamic CO₂ capture capacity. The present study provides an advanced protocol to design nitrogen-doped porous Carbon via a facile route toward the capture of CO₂, which offers excellent progress in sustainable chemistry and engineering. |
| ArticleNumber | 107854 |
| Author | Huang, Jiamei Demir, Muslum Yu, Qiyun Wang, Linlin Altay, Bilge Nazli Bai, Jiali Kilic, Murat Hu, Xin |
| Author_xml | – sequence: 1 givenname: Jiali surname: Bai fullname: Bai, Jiali organization: Key Laboratory of the Ministry of Education for Advanced Catalysis Materials, Zhejiang Normal University, Jinhua, Zhejiang 321004, PR China – sequence: 2 givenname: Jiamei surname: Huang fullname: Huang, Jiamei organization: Key Laboratory of the Ministry of Education for Advanced Catalysis Materials, Zhejiang Normal University, Jinhua, Zhejiang 321004, PR China – sequence: 3 givenname: Qiyun surname: Yu fullname: Yu, Qiyun organization: Key Laboratory of the Ministry of Education for Advanced Catalysis Materials, Zhejiang Normal University, Jinhua, Zhejiang 321004, PR China – sequence: 4 givenname: Muslum surname: Demir fullname: Demir, Muslum organization: Department of Chemical Engineering, Osmaniye Korkut Ata University, Osmaniye 80000, Türkiye – sequence: 5 givenname: Murat surname: Kilic fullname: Kilic, Murat organization: Department of Chemical Engineering, Eskişehir Technical University, Eskişehir 26555, Türkiye – sequence: 6 givenname: Bilge Nazli surname: Altay fullname: Altay, Bilge Nazli organization: College of Engineering Technology, Print and Graphic Media Science, Rochester Institute of Technology, Rochester, NY 14623, United States – sequence: 7 givenname: Xin surname: Hu fullname: Hu, Xin email: huxin@zjnu.cn organization: Key Laboratory of the Ministry of Education for Advanced Catalysis Materials, Zhejiang Normal University, Jinhua, Zhejiang 321004, PR China – sequence: 8 givenname: Linlin surname: Wang fullname: Wang, Linlin email: wanglinlin@zjnu.cn organization: Key Laboratory of Urban Rail Transit Intelligent Operation and Maintenance Technology and Equipment of Zhejiang Province, College of Engineering, Zhejiang Normal University, Jinhua, Zhejiang 321004, PR China |
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| Keywords | N-doped Porous carbons Macadamia nutshell Biomass waste CO2 adsorption |
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| Snippet | Selective adsorption and converting CO2 upon efficient solid-based adsorbents is critical for net-zero accomplishment. Herein, we develop an advisable strategy... Selective adsorption and converting CO₂ upon efficient solid-based adsorbents is critical for net-zero accomplishment. Herein, we develop an advisable strategy... |
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| SubjectTerms | adsorbents adsorption Biomass waste carbon carbon dioxide CO2 adsorption fuels green chemistry heat hulls Macadamia macadamia nuts Macadamia nutshell melamine N-doped nitrogen Porous carbons surface area technology |
| Title | N-doped porous carbon derived from macadamia nut shell for CO2 adsorption |
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