Ultrathin nanofiltration membrane with polydopamine-covalent organic framework interlayer for enhanced permeability and structural stability

Nanofiltration is a promising technology towards desalination and water purification. However, the pursuit for separation efficiency was hampered by the thick and less controllable selective layer. Herein, the ultrathin composite membranes with enhanced nanofiltration (NF) performance were achieved...

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Published in	Journal of membrane science Vol. 576; pp. 131 - 141
Main Authors	Wu, Mengyuan, Yuan, Jinqiu, Wu, Hong, Su, Yanlei, Yang, Hao, You, Xinda, Zhang, Runnan, He, Xueyi, Khan, Niaz Ali, Kasher, Roni, Jiang, Zhongyi
Format	Journal Article
Language	English
Published	Elsevier B.V 15.04.2019
Subjects	adsorption asymmetric membranes Covalent organic framework desalination dyes High flux hydrophilicity Interfacial polymerization nanofiltration Nanofiltration membrane permeability polyacrylonitrile polyamides polymerization porosity sodium sulfate solutes Structural stability water purification High flux Covalent organic framework Nanofiltration membrane Interfacial polymerization Structural stability
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Abstract	Nanofiltration is a promising technology towards desalination and water purification. However, the pursuit for separation efficiency was hampered by the thick and less controllable selective layer. Herein, the ultrathin composite membranes with enhanced nanofiltration (NF) performance were achieved by interfacial polymerization mediated by polydopamine (PDA)-covalent organic framework (COF) interlayer. The hybrid interlayer with exceptional surface hydrophilicity and high porosity controlled the adsorption/diffusion of amine monomers during the interfacial polymerization process and generated an ultrathin and dense polyamide (PA) layer, which was immensely reduced from 79 nm to 11 nm in thickness. The PA/PDA-COF/PAN nanofiltration membrane exhibited desirable desalination ratio (93.4% for Na2SO4) and dye rejection (94.5% for Orange GII), along with outstanding water permeation flux of 207.07 L m−2 h−1 MPa−1, 3 times higher than that of commercial NF membranes with similar solute rejection. Moreover, the hybrid interlayer significantly strengthened the interfacial interaction between the PA layer and the polyacrylonitrile (PAN) support, rendering the composite membrane with superior structural stability. The proposed strategy provided novel insight into the rational design of multifunctional interlayer to manipulate interfacial polymerization for high-performance PA membranes. [Display omitted] •The 11 nm-thick NF membranes were prepared on PDA-COF hybrid interlayer.•The hybrid interlayer controlled the adsorption/diffusion of amine monomers.•The PA/PDA-COF/PAN membrane showed highest water flux of 207.07 L m−2 h−1 MPa−1.•The TFC membranes exhibited high rejections to Na2SO4 (93.4%) and dyes (94.5–100%).•The PA/PDA-COF/PAN membrane showed satisfying structural stability.
AbstractList	Nanofiltration is a promising technology towards desalination and water purification. However, the pursuit for separation efficiency was hampered by the thick and less controllable selective layer. Herein, the ultrathin composite membranes with enhanced nanofiltration (NF) performance were achieved by interfacial polymerization mediated by polydopamine (PDA)-covalent organic framework (COF) interlayer. The hybrid interlayer with exceptional surface hydrophilicity and high porosity controlled the adsorption/diffusion of amine monomers during the interfacial polymerization process and generated an ultrathin and dense polyamide (PA) layer, which was immensely reduced from 79 nm to 11 nm in thickness. The PA/PDA-COF/PAN nanofiltration membrane exhibited desirable desalination ratio (93.4% for Na2SO4) and dye rejection (94.5% for Orange GII), along with outstanding water permeation flux of 207.07 L m−2 h−1 MPa−1, 3 times higher than that of commercial NF membranes with similar solute rejection. Moreover, the hybrid interlayer significantly strengthened the interfacial interaction between the PA layer and the polyacrylonitrile (PAN) support, rendering the composite membrane with superior structural stability. The proposed strategy provided novel insight into the rational design of multifunctional interlayer to manipulate interfacial polymerization for high-performance PA membranes. [Display omitted] •The 11 nm-thick NF membranes were prepared on PDA-COF hybrid interlayer.•The hybrid interlayer controlled the adsorption/diffusion of amine monomers.•The PA/PDA-COF/PAN membrane showed highest water flux of 207.07 L m−2 h−1 MPa−1.•The TFC membranes exhibited high rejections to Na2SO4 (93.4%) and dyes (94.5–100%).•The PA/PDA-COF/PAN membrane showed satisfying structural stability. Nanofiltration is a promising technology towards desalination and water purification. However, the pursuit for separation efficiency was hampered by the thick and less controllable selective layer. Herein, the ultrathin composite membranes with enhanced nanofiltration (NF) performance were achieved by interfacial polymerization mediated by polydopamine (PDA)-covalent organic framework (COF) interlayer. The hybrid interlayer with exceptional surface hydrophilicity and high porosity controlled the adsorption/diffusion of amine monomers during the interfacial polymerization process and generated an ultrathin and dense polyamide (PA) layer, which was immensely reduced from 79 nm to 11 nm in thickness. The PA/PDA-COF/PAN nanofiltration membrane exhibited desirable desalination ratio (93.4% for Na2SO4) and dye rejection (94.5% for Orange GII), along with outstanding water permeation flux of 207.07 L m−2 h−1 MPa−1, 3 times higher than that of commercial NF membranes with similar solute rejection. Moreover, the hybrid interlayer significantly strengthened the interfacial interaction between the PA layer and the polyacrylonitrile (PAN) support, rendering the composite membrane with superior structural stability. The proposed strategy provided novel insight into the rational design of multifunctional interlayer to manipulate interfacial polymerization for high-performance PA membranes.
Author	You, Xinda He, Xueyi Wu, Mengyuan Zhang, Runnan Jiang, Zhongyi Yang, Hao Yuan, Jinqiu Wu, Hong Su, Yanlei Khan, Niaz Ali Kasher, Roni
Author_xml	– sequence: 1 givenname: Mengyuan surname: Wu fullname: Wu, Mengyuan organization: Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China – sequence: 2 givenname: Jinqiu surname: Yuan fullname: Yuan, Jinqiu organization: Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China – sequence: 3 givenname: Hong surname: Wu fullname: Wu, Hong email: wuhong@tju.edu.cn organization: Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China – sequence: 4 givenname: Yanlei surname: Su fullname: Su, Yanlei organization: Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China – sequence: 5 givenname: Hao surname: Yang fullname: Yang, Hao organization: Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China – sequence: 6 givenname: Xinda surname: You fullname: You, Xinda organization: Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China – sequence: 7 givenname: Runnan surname: Zhang fullname: Zhang, Runnan organization: Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China – sequence: 8 givenname: Xueyi surname: He fullname: He, Xueyi organization: Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China – sequence: 9 givenname: Niaz Ali surname: Khan fullname: Khan, Niaz Ali organization: Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China – sequence: 10 givenname: Roni surname: Kasher fullname: Kasher, Roni organization: Department of Desalination and Water Treatment, Zuckerberg Institute for Water Research, Jacob Blaustein Institutes for Desert Research, Ben-Gurion University of the Negev, Sede Boqer Campus, 84990, Israel – sequence: 11 givenname: Zhongyi surname: Jiang fullname: Jiang, Zhongyi organization: Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Key Laboratory for Green Chemical Technology, School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China
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Snippet	Nanofiltration is a promising technology towards desalination and water purification. However, the pursuit for separation efficiency was hampered by the thick...
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SubjectTerms	adsorption asymmetric membranes Covalent organic framework desalination dyes High flux hydrophilicity Interfacial polymerization nanofiltration Nanofiltration membrane permeability polyacrylonitrile polyamides polymerization porosity sodium sulfate solutes Structural stability water purification
Title	Ultrathin nanofiltration membrane with polydopamine-covalent organic framework interlayer for enhanced permeability and structural stability
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