Facile green synthesis of ZnO–CdWO4 nanoparticles and their potential as adsorbents to remove organic dye
In this work, ZnO–CdWO4 nanoparticles have been synthesized by the ecofriendly green method with lemon leaf extract to favorably anchor functional groups on their surface. The prepared ZnO–CdWO4 nanoparticles are used as adsorbent to treat Congo red (CR) dye after characterization through FT-IR, UV–...
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| Published in | Environmental pollution (1987) Vol. 271; p. 116401 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
15.02.2021
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| Subjects | |
| Online Access | Get full text |
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| Abstract | In this work, ZnO–CdWO4 nanoparticles have been synthesized by the ecofriendly green method with lemon leaf extract to favorably anchor functional groups on their surface. The prepared ZnO–CdWO4 nanoparticles are used as adsorbent to treat Congo red (CR) dye after characterization through FT-IR, UV–Vis, TEM, SEM-EDX, and HRTEM techniques. The equilibrium partition coefficient and adsorption capacity values for CR by ZnO–CdWO4 are estimated as 21.4 mg g−1 μM−1 and 5 mg g−1, respectively (at an initial dye concentration of 10 mg L−1). The adsorption process is found as exothermic and spontaneous, as determined by the ΔG°, ΔS°, and ΔH° values. The Boyd plot has been used as a confirmatory tool to fit the adsorption kinetics data along with intraparticle diffusion and pseudo-second-order models. Based on this research, ZnO–CdWO4 nanoparticles are validated as an effective adsorbent for CR dye in aqueous solutions.
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•ZnO–CdWO4 was prepared using the Lemon leaf extract for CR adsorption application.•The diameters of ZnO–CdWO4 particles were in the range between 10 and 40 nm.•The adsorption process was exothermic and spontaneous with the capacity of 5 mg g−1.•The partition coefficient of CR by ZnO–CdWO4 was estimated as 21.4 mg g−1 μM−1. |
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| AbstractList | In this work, ZnO–CdWO4 nanoparticles have been synthesized by the ecofriendly green method with lemon leaf extract to favorably anchor functional groups on their surface. The prepared ZnO–CdWO4 nanoparticles are used as adsorbent to treat Congo red (CR) dye after characterization through FT-IR, UV–Vis, TEM, SEM-EDX, and HRTEM techniques. The equilibrium partition coefficient and adsorption capacity values for CR by ZnO–CdWO4 are estimated as 21.4 mg g−1 μM−1 and 5 mg g−1, respectively (at an initial dye concentration of 10 mg L−1). The adsorption process is found as exothermic and spontaneous, as determined by the ΔG°, ΔS°, and ΔH° values. The Boyd plot has been used as a confirmatory tool to fit the adsorption kinetics data along with intraparticle diffusion and pseudo-second-order models. Based on this research, ZnO–CdWO4 nanoparticles are validated as an effective adsorbent for CR dye in aqueous solutions.
[Display omitted]
•ZnO–CdWO4 was prepared using the Lemon leaf extract for CR adsorption application.•The diameters of ZnO–CdWO4 particles were in the range between 10 and 40 nm.•The adsorption process was exothermic and spontaneous with the capacity of 5 mg g−1.•The partition coefficient of CR by ZnO–CdWO4 was estimated as 21.4 mg g−1 μM−1. |
| ArticleNumber | 116401 |
| Author | Siddiqui, Sharf Ilahi Chaudhry, Saif Ali Fatima, Bushra Ahmad, Rabia Kim, Ki-Hyun Nirala, Ranjeet Kumar Vikrant, Kumar |
| Author_xml | – sequence: 1 givenname: Bushra surname: Fatima fullname: Fatima, Bushra organization: Department of Chemistry, Jamia Millia Islamia, New Delhi, 110025, India – sequence: 2 givenname: Sharf Ilahi surname: Siddiqui fullname: Siddiqui, Sharf Ilahi organization: Department of Chemistry, Jamia Millia Islamia, New Delhi, 110025, India – sequence: 3 givenname: Ranjeet Kumar surname: Nirala fullname: Nirala, Ranjeet Kumar organization: Centre for Interdisciplinary Research in Basic Sciences, Jamia Millia Islamia, New Delhi, 110025, India – sequence: 4 givenname: Kumar surname: Vikrant fullname: Vikrant, Kumar organization: Department of Civil & Environmental Engineering, Hanyang University, 222 Wangsimni-Ro, Seoul, 04763, Republic of Korea – sequence: 5 givenname: Ki-Hyun surname: Kim fullname: Kim, Ki-Hyun email: kkim61@hanyang.ac.kr organization: Department of Civil & Environmental Engineering, Hanyang University, 222 Wangsimni-Ro, Seoul, 04763, Republic of Korea – sequence: 6 givenname: Rabia surname: Ahmad fullname: Ahmad, Rabia organization: Department of Chemistry, Jamia Millia Islamia, New Delhi, 110025, India – sequence: 7 givenname: Saif Ali surname: Chaudhry fullname: Chaudhry, Saif Ali organization: Department of Chemistry, Jamia Millia Islamia, New Delhi, 110025, India |
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| Keywords | Lemon leaf extract Congo red Kinetics Adsorption Isotherms ZnO–CdWO4 composite |
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